IP Library Granted Patent US 9,163,314
Granted Patent B2
US 9,163,314 · App. 13/643,375 · Granted Oct 20, 2015

CMP slurry composition for tungsten

Inventors: Jea-Gun Park (Seongnam-si, KR); Jin-Hyung Park (Ulsan, KR); Jae-Hyung Lim (Seoul, KR); Jong-Young Cho (Seoul, KR); Ho Choi (Seoul, KR); Hee-Sub Hwang (Seoul, KR)
Assignee: INDUSTRIAL BANK OF KOREA
C23F1/30C09G1/02C23F3/06
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Quick Facts
Patent No.
US 9,163,314
App. No.
13/643,375
Granted
Oct 20, 2015
Kind
B2
Abstract

The present invention relates to a CMP slurry composition for polishing tungsten comprising a abrasive and a polishing chemical, wherein the abrasive comprises colloidal silica dispersed in ultra-pure water, and the polishing chemical comprises hydrogen peroxide, ammonium persulfate and iron nitrate. The slurry composition is not discolored and has good etching selectivity, so as to be applied to a CMP process.

Claims (10)

1. A Chemical Mechanical Polishing (CMP) slurry composition for polishing tungsten consisting of;

an abrasive and a polishing chemical to inhibit discoloration and to adjust etching selectivity by decreasing a polishing rate of titanium nitride and increasing a polishing rate of tungsten,

wherein

the abrasive consists of colloidal silica dispersed in ultra-pure water;

the polishing chemical consists of hydrogen peroxide in an amount of 0.5-2 weight%, ammonium persulfate in an amount of 0.05-1 weight% and iron nitrate in an amount of 0.01-0.1 weight%;

etching selectivity of tungsten and titanium nitride is 1:1.5-2 and etching selectivity of tungsten and an oxide film is 2:1 or more;

the amount of the colloidal silica is 2-4 weight%;

pH of the composition is 2-4; and

the polishing rate of titanium nitride is decreased and the polishing rate of tungsten is increased as increasing the concentration of ammonium persulfate.

2. The CMP slurry composition of claim 1 , wherein the etching selectivity of tungsten and titanium nitride is 1:1.8 and the etching selectivity of tungsten and an oxide film is 2.1:1 at ammonium persulfate of 0.05 weight% and iron nitrate of 0.1 weight%.

Assignments (7)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 3, 2022
From: SHIN-ETSU CHEMICAL CO., LTD.
To: UBMATERIALS INC.
Reel/Frame 059318/0078 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 24, 2017
From: INDUSTRIAL BANK OF KOREA
To: SHIN-ETSU CHEMICAL CO., LTD.
Reel/Frame 042089/0699 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 6, 2015
From: UBMATERIALS INC.
To: INDUSTRIAL BANK OF KOREA
Reel/Frame 034904/0474 →
LICENSE Recorded Feb 3, 2015
From: UB MATERIALS, INC.
To: SHIN-ETSU CHEMICAL CO., LTD.
Reel/Frame 034874/0855 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 9, 2014
From: UBMATERIALS INC.
To: UBMATERIALS INC.
Reel/Frame 032178/0525 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 9, 2014
From: UBPRECISION CO., LTD.
To: UBMATERIALS INC.
Reel/Frame 032189/0755 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 25, 2012
From: PARK, JEA-GUN; PARK, JIN-HYUNG; LIM, JAE-HYUNG; CHO, JONG-YOUNG; CHOI, HO; HWANG, HEE-SUB
To: UBPRECISION CO., LTD.
Reel/Frame 029196/0593 →
Priority Claims (2)
KR 10-2011-0081207 · Aug 16, 2011 · national
KR 10-2011-0117872 · Nov 11, 2011 · national
Continuity (1)
Related Publication 20130214199A1 · Aug 22, 2013