Lubricant composition
View Patent ↗1-[Di(4-octylphenyl)aminomethyl]tolutriazole is prepared in a mineral oil wherein the reaction also contains between 0.1 and 5% by weight of a polyacrylate polymer dissolved in a mineral oil. The liquid product shows increased storage stability with respect to crystallization of the 1-[di(4-octylphenyl)aminomethyl]tolutriazole when the polyacrylate polymer is added during the reaction to prepare the 1-[Di(4-octylphenyl)aminomethyl]tolutriazole. This product can be utilized in a lubricant composition as an antioxidant and corrosion inhibitor.
1. A method for reducing crystallization of 1-[Di(4-octylphenyl)aminomethyl]tolutriazole, comprising the steps of:
bringing a first component consisting of 1-[Di(4-octylphenyl)aminomethyl]tolutriazole in process oil to a processing temperature between about 80-100° C.,
adding to the first component a second component consisting of polyacrylate polymer in mineral oil to give about 0.1 to about 5.0 wt. % polyacrylate polymer as part of a total composition of the first component and second component,
stirring the total composition for at least 10 minutes while maintaining the processing temperature, and
storing the total composition at room temperature.
2. The method of claim 1 , wherein the polyacrylate polymer in mineral oil is added to give about 0.5-1.0 wt. %.
3. The method of claim 1 , wherein the 1-[Di(4-octylphenyl)aminomethyl]tolutriazole is diluted at between 40-60% by weight in the process oil.
4. The method of claim 3 , wherein the dilution is about 50% by weight.
5. The method of claim 1 , further comprising, after the final step, adding the composition to a lubricating composition at about 0.1-3 wt % as part of the lubricating composition.
6. A tolutriazole blend formed by bringing a first component consisting of 1-[Di(4-octylphenyl)aminomethyl]tolutriazole in process oil to a processing temperature between about 80-100° C., adding to the first component a second component consisting of polyacrylate polymer in mineral oil to give about 0.1 to 5.0 wt. % polyacrylate polymer as part of a total composition of the first and second components, and stirring the total composition for at least 10 minutes while maintaining the processing temperature.
7. The method of claim 5 , wherein the polyacrylate polymer in mineral oil is added to give about 0.5-1.0 wt. %.
8. The method of claim 5 , wherein the 1-[Di(4-octylphenyl)aminomethyl]tolutriazole is diluted at between 40-60% by weight in the process oil.
9. The method of claim 8 , wherein the dilution is about 50% by weight.