IP Library Granted Patent US 9,096,767
Granted Patent B2
US 9,096,767 · App. 13/669,640 · Granted Aug 4, 2015

Curable solid inks containing cyclohexyl-based crystalline gellants

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Quick Facts
Patent No.
US 9,096,767
App. No.
13/669,640
Granted
Aug 4, 2015
Kind
B2
Abstract

Disclosed herein are curable solid inks which are solid at room temperature and molten at an elevated temperature at which the molten ink is applied to a substrate. In particular, the curable solid ink of the present embodiments comprises a cyclohexyl-based crystalline gellant that impart self-leveling capabilities to the inks, where the cyclohexyl-based crystalline gellant have a structure of Formula I: wherein each X, Y, p, q, R 1 , R 2 , R 3 , and R 4 are as defined herein.

Claims (32)

1. A self-leveling curable solid ink comprising:

a curable wax;

a cyclohexyl-based crystalline gellant having the following formula:

wherein each X and Y is independently CH 2 or O; each p and q is independently from about 8 to about 20; each R 1 , R 2 , R 3 , and R 4 is independently H or lower alkyl;

wherein the cyclohexyl-based crystalline gellant has a tan δ above about 0.08, and a melting point of above about 90° C.

2. The self-leveling curable solid ink of claim 1 , wherein the cyclohexyl-based crystalline gellant having a tan δ of from about 0.8 to about 2.

3. The self-leveling curable solid ink of claim 1 , wherein the cyclohexyl-based crystalline gellant having a melting point of from about 90° C. to about 150° C.

4. The self-leveling curable solid ink of claim 1 , wherein the cyclohexyl-based crystalline gellant has a G′ at room temperature of from about 1 Pa to about 100 Pa and a G″ at room temperature of from about 1 Pa to about 100 Pa.

5. The self-leveling curable solid ink of claim 1 , wherein the cyclohexyl-based crystalline gellant has a melting temperature of from about 90° C. to about 150° C.

6. The self-leveling curable solid ink of claim 1 , wherein the self-leveling curable solid ink having a gel point of from about 35° C. to about 70° C.

7. The self-leveling curable solid ink of claim 1 , wherein the cyclohexyl-based crystalline gellant is present in the curable solid ink in an amount of from about 1 percent to about 50 percent.

8. The self-leveling curable solid ink of claim 1 , wherein the cyclohexyl-based crystalline gellant is present in the curable solid ink in an amount of from about 5 percent to about 10 percent.

9. The self-leveling curable solid ink of claim 1 , wherein both X and Y are CH 2 .

10. The self-leveling curable solid ink of claim 1 , wherein p is from about 10 to about 18.

11. The self-leveling curable solid ink of claim 1 , wherein q is from about 10 to about 18.

12. The self-leveling curable solid ink of claim 1 , wherein both R 3 and R 4 are methyl.

13. The self-leveling curable solid ink of claim 1 , wherein each one of R 1 and each one of R 2 is H.

14. A self-leveling curable solid ink comprising

a curable wax;

a cyclohexyl-based crystalline gellant; and

a photoinitiator;

wherein the cyclohexyl-based crystalline gellant has the following formula:

wherein each X and Y is independently CH 2 or O; each p and q is independently from about 8 to about 20; each R 1 , R 2 , R 3 and R 4 is independently H or lower alkyl; and

wherein the cyclohexyl-based crystalline gellant has a tan δ above about 0.08, and a melting point of above about 90° C.

15. The self-leveling curable solid ink of claim 14 , wherein the cyclohexyl-based crystalline gellant has a melting point of from about 90° C. to about 150° C.

16. The self-leveling curable solid ink of claim 14 , wherein the cyclohexyl-based crystalline gellant has a tan δ of from about 0.8 to about 2.

17. The self-leveling curable solid ink of claim 14 , wherein the cyclohexyl-based crystalline has a G′ at room temperature of from about 1 Pa to about 100 Pa and a G″ at room temperature of from about 1 Pa to about 100 Pa.

18. A self-leveling curable solid ink comprising

a curable wax; and

a cyclohexyl-based crystalline gellant;

wherein the cyclohexyl-based crystalline gellant has the following formula:

19. The self-leveling curable solid ink of claim 18 , wherein the cyclohexyl-based crystalline gellant has the following formula:

Assignments (12)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 6, 2025
From: XEROX CORPORATION
To: GENESEE VALLEY INNOVATIONS, LLC
Reel/Frame 073842/0479 →
SECOND LIEN NOTES PATENT SECURITY AGREEMENT Recorded Jul 2, 2025
From: XEROX CORPORATION
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 071785/0550 →
FIRST LIEN NOTES PATENT SECURITY AGREEMENT Recorded Apr 11, 2025
From: XEROX CORPORATION
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 070824/0001 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT RF 064760/0389 Recorded Feb 13, 2024
From: CITIBANK, N.A., AS COLLATERAL AGENT
To: XEROX CORPORATION
Reel/Frame 068261/0001 →
SECURITY INTEREST Recorded Feb 13, 2024
From: XEROX CORPORATION
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 066741/0001 →
SECURITY INTEREST Recorded Nov 20, 2023
From: XEROX CORPORATION
To: JEFFERIES FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 065628/0019 →
SECURITY INTEREST Recorded Jun 22, 2023
From: XEROX CORPORATION
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 064760/0389 →
RELEASE OF SECURITY INTEREST IN PATENTS AT R/F 062740/0214 Recorded May 18, 2023
From: CITIBANK, N.A., AS AGENT
To: XEROX CORPORATION
Reel/Frame 063694/0122 →
SECURITY INTEREST Recorded Nov 10, 2022
From: XEROX CORPORATION
To: CITIBANK, N.A., AS AGENT
Reel/Frame 062740/0214 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNOR JEFFREY BANNING'S NAME PREVIOUSLY RECORDED ON REEL 029247 FRAME 0052. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Sep 3, 2013
From: CHOPRA, NAVEEN; KEOSHKERIAN, BARKEV; VANBESIEN, DARYL; ELIYAHU, JENNY; DRAPPEL, STEPHAN; BANNING, JEFFREY
To: XEROX CORPORATION
Reel/Frame 031156/0054 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 3, 2013
From: CHAPPELL, JAMES M.; XU, FUSHENG; MCCONVILLE, PAUL J.
To: XEROX CORPORATION
Reel/Frame 031129/0509 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 6, 2012
From: CHOPRA, NAVEEN; KEOSHKERIAN, BARKEV; VANBESIEN, DARYL; ELIYAHU, JENNY; DRAPPEL, STEPHAN; BANNING, JEFF
To: XEROX CORPORATION
Reel/Frame 029247/0052 →