PROCESS FOR PHASE SEPARATION OR EXTRACTION AND DEVICE SUITABLE THEREFOR
The present invention relates to a device for separating two immiscible phases and/or for extracting one phase with another phase (phase separation or extraction device), comprising at least one vessel for receiving the at least two phases, at least one pipe for supplying a fluid to the vessel, at least one pipe for discharging a fluid from the vessel, and at least one arrangement comprising a transparent disk for observing the separation operation or the extraction operation, wherein at least the side of the transparent disk that faces the phases to be separated or extracted consists of sapphire (sapphire glass) or mica ( mica disk), and to the use of such a device in the preparation of di- and polyamines of the diphenylmethane series.
1 . A device for separating at least two immiscible phases or for extracting one phase with another phase comprising:
a) at least one vessel for receiving the phases to be separated or extracted,
b) at least one pipe for supplying a first fluid to the vessel,
c) at least one pipe for discharging a second fluid from the vessel, and
d) at least one means for observing the vessel's contents during phase separation or extraction comprising:
(i) a transparent disk composed of sapphire or mica on the disk's side that faces the phases to be separated or extracted.
2 . The device of claim 1 in which the transparent disk is composed completely of sapphire or mica.
3 . The device of claim 1 in which only the side of the transparent disk that faces the phases to be separated or extracted is composed of sapphire.
4 . The device of claim 1 in which the disk of the observation means is a composite of sapphire or mica and another transparent material selected from the group consisting of borosilicate glass and quartz glass.
5 . The device of claim 4 in which at least the side of the transparent disk that faces the phases to be separated or extracted consists of sapphire.
6 . A process for the separation of at least two immiscible phases or extraction of one phase with another phase comprising supplying a fluid composed of at least two phases to the device of claim 1 .
7 . The process of claim 6 in which the fluid composed of at least two phases was generated during production of di- and polyamines of the diphenylmethane series.
8 . The process of claim 1 fluid composed of at least two phases is separated into an aqueous phase and an organic phase containing di- and polyamines of the diphenylmethane series.
9 . The process of claim 8 in which the aqueous phase is alkaline.
10 . The process of claim 8 in which the aqueous phase has a pH value of from 8.0 to 14.
11 . The process of claim 6 in which the device is used to extract an organic phase containing di- and polyamines of the diphenylmethane series with an aqueous phase.
12 . The process of claim 6 in which the device is used to extract an aqueous phase containing di- and polyamines of the diphenylmethane series with an organic, aniline-containing phase.