IP Library Granted Patent US 8,802,863
Granted Patent B2
US 8,802,863 · App. 13/699,451 · Granted Aug 12, 2014

Amino alcohol cationic lipids for oligonucleotide delivery

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Quick Facts
Patent No.
US 8,802,863
App. No.
13/699,451
Granted
Aug 12, 2014
Kind
B2
Abstract

The instant invention provides for novel cationic lipids that can be used in combination with other lipid components such as cholesterol and PEG-lipids to form lipid nanoparticles with oligonucleotides. It is an object of the instant invention to provide a cationic lipid scaffold that is more efficacious than traditional cationic lipids. The present invention employs amino alcohols to enhance the efficiency of in vivo delivery of siRNA.

Claims (21)

1. A lipid of Formula A:

wherein:

R 1 and R 2 are independently selected from H, (C 1 -C 6 )alkyl, heterocyclyl and polyamine, wherein said alkyl, heterocyclyl and polyamine are optionally substituted with one to three substituents selected from R′, or R 1 and R 2 can be taken together with the nitrogen to which they are attached to form a monocyclic heterocycle with 4-7 members optionally containing, in addition to the nitrogen, one or two additional heteroatoms selected from N, O and S, said monocyclic heterocycle is optionally substituted with one to three substituents selected from R′;

R 3 is selected from H and (C 1 -C 6 )alkyl, wherein said alkyl is optionally substituted with one to three substituents selected from R′, or R 3 can be taken together with R 1 to form a monocyclic heterocycle with 4-7 members optionally containing, in addition to the nitrogen, one or two additional heteroatoms selected from N, O and S, said monocyclic heterocycle is optionally substituted with one to three substituents selected from R′;

R′ is independently selected from halogen, R″, OR″, SR″, CN, CO 2 R″ and CON(R″) 2 ;

R″ is independently selected from H and (C 1 -C 6 )alkyl, wherein said alkyl is optionally substituted with halogen and OH;

L 1 is C 4 -C 22 alkenyl, said alkenyl is optionally substituted with R′; and

L 2 is selected from C 4 -C 22 alkyl and C 4 -C 22 alkenyl, said alkyl and alkenyl are optionally substituted with R′;

or any pharmaceutically acceptable salt or stereoisomer thereof.

2. A lipid of Formula A according to claim 1 , wherein:

R 1 and R 2 are each H;

R 3 is H;

L 1 is C 4 -C 22 alkenyl; and

L 2 is selected from C 4 -C 22 alkyl and C 4 -C 22 alkenyl;

or any pharmaceutically acceptable salt or stereoisomer thereof.

3. A lipid which is selected from:

2-amino-3-[(9Z,12Z)-octadeca-9,12-dien-1-yloxy]-2-{[(9Z,12Z)-octadeca-9,12-dien-1-yloxy]methyl)}propan-1-ol (Compound 1);

2-amino-3-[(9Z)-octadec-9-en-1-yloxy]-2-{[(9Z)-octadec-9-en-1-yloxy]methyl}propan-1-ol (Compound 2);

2-amino-3-[(9Z,12Z)-octadeca-9,12-dien-1-yloxy]-2-[(octyloxy)methyl]propan-1-ol (Compound 3); and

2-(dimethylamino)-3-[(9Z,12Z)-octadeca-9,12-dien-1-yloxy]-2-{[(9Z,12Z)-octadeca-9,12-dien-1-yloxy]methyl}propan-1-ol (Compound 4) or any pharmaceutically acceptable salt or stereoisomer thereof.

4. A lipid particle comprising a lipid according to claim 1 .

Assignments (2)
SECURITY INTEREST Recorded Oct 1, 2025
From: ALNYLAM PHARMACEUTICALS, INC.; SIRNA THERAPEUTICS, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 072996/0337 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 26, 2014
From: MERCK SHARP & DOHME CORP.
To: SIRNA THERAPEUTICS, INC.
Reel/Frame 032531/0541 →