IP Library Granted Patent US 9,175,096
Granted Patent B2
US 9,175,096 · App. 13/706,684 · Granted Nov 3, 2015

Regioselectively substituted cellulose esters produced in a halogenated ionic liquid process and products produced therefrom

Inventors: Charles Michael Buchanan (Bluff City, TN); Norma Lindsey Buchanan (Bluff City, TN); Michael Eugene Donelson (Kingsport, TN); Maryna Grigorievna Gorbunova (Kingsport, TN); Thauming Kuo (Kingsport, TN); Bin Wang (Kingsport, TN)
Assignee: EASTMAN CHEMICAL COMPANY
C08B1/003C08B3/04C08B3/06C08B3/08C08B3/10C08B3/16C08J5/18G02B5/3083C08J2301/08G02F1/13363G02F2413/11
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Quick Facts
Patent No.
US 9,175,096
App. No.
13/706,684
Granted
Nov 3, 2015
Kind
B2
Abstract

This invention relates to novel compositions comprising regioselectively substituted cellulose esters. One aspect of the invention relates to processes for preparing regioselectively substituted cellulose esters from cellulose dissolved in ionic liquids. Another aspect of the invention relates to the utility of regioselectively substituted cellulose esters in applications such as protective and compensation films for liquid crystalline displays.

Claims (9)

1. A film comprising at least one regioselectively substituted cellulose ester with a RDS ratio of C 6 >C 3 >C 2 , wherein said regioselectively substituted cellulose ester is prepared from cellulose having an α-cellulose content of at least 95 percent by weight.

2. The film according to claim 1 wherein the ring RDS ratio of the regioselectively substituted cellulose ester for C 6 /C 3 or C 6 /C 2 is at least 1.05.

3. The film according to claim 1 wherein the product of the ring RDS ratio of the regioselectively substituted cellulose ester for C 6 /C 3 or C 6 /C 2 times the total DS is at least 2.9.

4. The film according to claim 1 wherein said regioselectively substituted cellulose ester has a ring RDS ratio for C 6 /C 3 or C 6 /C 2 is at least 1.05, and the product of the ring RDS ratio for C 6 /C 3 or C 6 /C 2 times the total DS is at least 2.9.

5. The film according to claim 1 wherein said regioselectively substituted cellulose ester has a carbonyl RDS ratio of at least one acyl substituent for C 6 /C 3 or C 6 /C 2 of at least 1.3.

6. The film according to claim 1 wherein the product of the carbonyl RDS ratio of at least one acyl substituent for C 6 /C 3 or C 6 /C 2 times the DS of the acyl substituent for said regioselectively substituted cellulose ester is at least 2.3.

7. The film according to claim 1 wherein the product of the carbonyl RDS ratio for C 6 /C 3 or C 6 /C 2 times the DS of the acyl substituent for said regioselectively substituted cellulose ester is at least 2.5.

8. The film according to claim 1 wherein the carbonyl RDS ratio of at least one acyl substituent for C 6 /C 3 or C 6 /C 2 for said regioselectively substituted cellulose ester is at least 1.3 and the product of the carbonyl RDS ratio for C 6 /C 3 or C 6 /C 2 times the acyl DS for said regioselectively substituted cellulose ester is at least 2.3.

9. A film according to claim 1 wherein said film is photographic film, protective film, or compensation film.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 7, 2015
From: BUCHANAN, CHARLES MICHAEL; BUCHANAN, NORMA LINDSEY; DONELSON, MICHAEL EUGENE; GORBUNOVA, MARYNA GRIGORIEVNA; KUO, THAUMING; WANG, BIN
To: EASTMAN CHEMICAL COMPANY
Reel/Frame 035350/0362 →
Continuity (5)
Continuation 12539812 · Aug 12, 2009
Continuation In Part 12189415 · Aug 11, 2008
Provisional Application 61026280 · Feb 13, 2006
Provisional Application 61088423 · Aug 13, 2008
Related Publication 20130190485A1 · Jul 25, 2013