IP Library Granted Patent US 8,746,376
Granted Patent B2
US 8,746,376 · App. 13/722,250 · Granted Jun 10, 2014

Rotary drill bit including polycrystalline diamond cutting elements

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Quick Facts
Patent No.
US 8,746,376
App. No.
13/722,250
Granted
Jun 10, 2014
Kind
B2
Abstract

Embodiments relate to methods of fabricating PCD materials by subjecting a mixture that exhibits a broad diamond particle size distribution to an HPHT process, PCD materials so-formed, and PDCs including a polycrystalline diamond table comprising such PCD materials. In an embodiment, a PCD material includes a plurality of bonded diamond grains that exhibit a substantially unimodal diamond grain size distribution characterized, at least in part, by a parameter θ that is less than about 1.0. θ = x 6 · σ , where x is the average grain size of the substantially unimodal diamond grain size distribution, and σ is the standard deviation of the substantially unimodal diamond grain size distribution.

Claims (57)

1. A drill bit, comprising:

a bit body configured to engage a subterranean formation, the bit body including a plurality of blades, each of the plurality of blades including a plurality of polycrystalline diamond cutting elements, at least one of the plurality of polycrystalline diamond cutting elements including a polycrystalline diamond material including:

a plurality of bonded diamond grains, the plurality of bonded diamond grains exhibiting a substantially unimodal diamond grain size distribution characterized, at least in part, by a parameter θ that is about 0.25 to about 1.0; and

wherein:

θ

=

x

6

·

σ

;

x is the average grain size of the substantially unimodal diamond grain size distribution, and is about 5 μm to about 30 μm; and

σ is the standard deviation of the substantially unimodal diamond grain size distribution.

2. The drill bit of claim 1 wherein the parameter θ is about 0.3 to about 0.9.

3. The drill bit of claim 1 wherein the parameter θ is about 0.3 to about 0.7.

4. The drill bit of claim 1 wherein the parameter θ is about 0.5 to about 0.7.

5. The drill bit of claim 1 wherein the parameter θ is about 0.3 to about 0.4.

6. The drill bit of claim 1 wherein σ is about 2 μm to about 15 μm.

7. The drill bit of claim 1 wherein σ is about 4 μm to about 10 μm, and the parameter θ is about 0.3 to about 0.7.

8. The drill bit of claim 1 wherein the polycrystalline diamond material exhibits a thermal stability that is at least about as thermally stable as a partially leached polycrystalline diamond material having a leach depth of about 60 μm to about 70 μm and a different diamond grain size distribution.

9. The drill bit of claim 1 wherein the at least one of the plurality of polycrystalline diamond cutting elements includes a substrate bonded to the polycrystalline diamond material.

10. The drill bit of claim 9 wherein the substrate comprises a cemented carbide material.

11. The drill bit of claim 1 wherein the polycrystalline diamond material is leached to a selected depth.

12. A drill bit, comprising:

a bit body configured to engage a subterranean formation, the bit body including a plurality of blades, each of the plurality of blades including a plurality of polycrystalline diamond cutting elements, at least one of the plurality of polycrystalline diamond cutting elements including a polycrystalline diamond material including:

a plurality of bonded diamond grains, the plurality of bonded diamond grains exhibiting a substantially unimodal diamond grain size distribution characterized, at least in part, by a parameter θ that is about 0.3 to about 0.7; and

wherein:

θ

=

x

6

·

σ

;

x is the average grain size of the substantially unimodal diamond grain size distribution and is about 10 μm to about 20 μm; and

σ is the standard deviation of the substantially unimodal diamond grain size distribution.

13. The drill bit of claim 12 wherein the parameter θ is about 0.5 to about 0.7.

14. The drill bit of claim 12 wherein the parameter θ is about 0.3 to about 0.4.

15. The drill bit of claim 12 wherein x is about 12 μm to about 15 μm and σ is about 6 μm to about 8.5 μm.

16. The drill bit of claim 12 wherein σ is about 4 μm to about 10 μm.

17. The drill bit of claim 12 wherein the polycrystalline diamond material is leached to a selected depth.

18. A drill bit, comprising:

a bit body configured to engage a subterranean formation, the bit body including a plurality of blades, each of the plurality of blades including a plurality of polycrystalline diamond cutting elements, at least one of the plurality of polycrystalline diamond cutting elements including a polycrystalline diamond material including:

a plurality of bonded diamond grains defining a plurality of interstitial regions, the plurality of bonded diamond grains exhibiting a substantially unimodal diamond grain size distribution characterized, at least in part, by a parameter θ that is about 0.3 to about 0.9;

wherein:

θ

=

x

6

·

σ

;

x is the average grain size of the substantially unimodal diamond grain size distribution and is about 10 μm to about 20 μm;

σ is the standard deviation of the substantially unimodal diamond grain size distribution; and

a catalyst material is disposed in at least a portion of the plurality of interstitial regions.

19. The drill bit of claim 18 wherein the polycrystalline diamond material is leached to a selected depth.

20. The drill bit of claim 18 wherein the catalyst material includes a metal-solvent catalyst or a carbonate catalyst.

Assignments (5)
SECURITY INTEREST Recorded Jul 18, 2025
From: US SYNTHETIC CORPORATION
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 074973/0089 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: ACE DOWNHOLE, LLC; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; APERGY BMCS ACQUISITION CORP.; NORRISEAL-WELLMARK, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
Reel/Frame 060305/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: ACE DOWNHOLE, LLC; APERGY BMCS ACQUISITION CORP.; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 053790/0001 →
SECURITY AGREEMENT Recorded May 9, 2018
From: APERGY (DELAWARE) FORMATION, INC.; APERGY BMCS ACQUISITION CORP.; APERGY ENERGY AUTOMATION, LLC; HARBISON-FISCHER, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 046117/0015 →