IP Library Granted Patent US 9,346,149
Granted Patent B1
US 9,346,149 · App. 13/734,354 · Granted May 24, 2016

Polycrystalline diamond compacts and applications therefor

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Quick Facts
Patent No.
US 9,346,149
App. No.
13/734,354
Granted
May 24, 2016
Kind
B1
Abstract

Embodiments relate to polycrystalline diamond compacts (“PDCs”) including a polycrystalline diamond (“PCD”) table having a diamond grain size distribution selected for improving leachability. In an embodiment, a PDC includes a PCD table bonded to a substrate. The PCD table includes diamond grains exhibiting diamond-to-diamond bonding therebetween. The diamond grains includes a first amount being about 30 to about 65 volume % of the diamond grains and a second amount being about 18 to about 65 volume % of the diamond grains. The first amount exhibits a first average grain size of about 8 μm to about 22 μm. The second amount exhibits a second average grain size that is greater than the first average grain size and is about 15 μm to about 50 μm. Other embodiments are directed methods of forming PDCs, and various applications for such PDCs in rotary drill bits, bearing apparatuses, and wire-drawing dies.

Claims (39)

1. A polycrystalline diamond compact, comprising:

a substrate; and

a polycrystalline diamond table bonded to the substrate, the polycrystalline diamond table including a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween, the plurality of diamond grains including:

a first amount being about 35 volume % to about 45 volume % of the plurality of diamond grains, the first amount exhibiting a first average grain size of about 8 μm to about 14 μm; and

a second amount being about 55 volume % to about 65 volume % of the plurality of diamond grains, the second amount exhibiting a second average grain size that is greater than the first average grain size and is about 15 μm to about 50 μm.

2. The polycrystalline diamond compact of claim 1 wherein the first average grain size is about 10 μm to about 12 μm and the second average grain size is about 18 μm to about 22 μm.

3. The polycrystalline diamond compact of claim 1 wherein the first amount is about 38 volume % to about 42 volume % and the second amount is about 58 volume % to about 62 volume %.

4. The polycrystalline diamond compact of claim 3 wherein the first average grain size is about 10 μm to about 12 μm and the second average grain size is about 18 μm to about 22 μm.

5. The polycrystalline diamond compact of claim 1 wherein the polycrystalline diamond table includes boron in a range from greater than 0 weight % to about 5 weight %.

6. The polycrystalline diamond compact of claim 5 wherein the range is from greater than 0 weight % to about 0.2 weight %.

7. The polycrystalline diamond compact of claim 1 wherein the polycrystalline diamond table is integrally formed with the substrate.

8. The polycrystalline diamond compact of claim 1 wherein the polycrystalline diamond table includes at least one exterior surface and a leached region extending inwardly from of the at least one exterior surface to a depth of greater than 250 μm.

9. A rotary drill bit, comprising:

a bit body including a leading end structure configured to facilitate drilling a subterranean formation and having one or more blades; and

a plurality of cutting elements mounted to the one or more blades, at least one of the plurality of cutting elements including:

a substrate; and

a polycrystalline diamond table bonded to the substrate, the polycrystalline diamond table including a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween, the plurality of diamond grains including:

a first amount exhibiting a first average grain size of about 8 μm to about 14 μm; and

a second amount exhibiting a second average grain size that is greater than the first average grain size and is about 15 μm to about 50 μm;

wherein the first amount is about 35 volume % to about 45 volume % and the second amount is about 55 volume % to about 65 volume %; or the first amount is about 55 volume % to about 65 volume % and the second amount is about 35 volume % to about 45 volume %.

10. A polycrystalline diamond compact, comprising:

a substrate; and

a polycrystalline diamond table bonded to the substrate, the polycrystalline diamond table including a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween, the plurality of diamond grains including:

a first amount being about 55 volume % to about 65 volume % of the plurality of diamond grains, the first amount exhibiting a first average grain size of about 8 μm to about 14 μm; and

a second amount being about 35 volume % to about 45 volume % of the plurality of diamond grains, the second amount exhibiting a second average grain size that is greater than the first average grain size and is about 20 μm to about 40 μm;

wherein a ratio of the first average grain size to the second average grain size is about 0.3 to about 0.7.

11. A polycrystalline diamond compact, comprising:

a substrate; and

a polycrystalline diamond table bonded to the substrate, the polycrystalline diamond table including a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween, the plurality of diamond grains including:

a first amount being about 55 volume % to about 65 volume % of the plurality of diamond grains, the first amount exhibiting a first average grain size of about 8 μm to about 14 μm; and

a second amount being about 35 volume % to about 45 volume % of the plurality of diamond grains, the second amount exhibiting a second average grain size that is greater than the first average grain size and is about 15 μm to about 50 μm.

12. The polycrystalline diamond compact of claim 11 wherein the first average grain size is about 10 μm to about 12 μm and the second average grain size is about 18 μm to about 22 μm.

13. The polycrystalline diamond compact of claim 11 wherein the first amount is about 58 volume % to about 62 volume % and the second amount is about 38 volume % to about 42 volume %.

14. The polycrystalline diamond compact of claim 13 wherein the first average grain size is about 10 μm to about 12 μm and the second average grain size is about 18 μm to about 22 μm.

15. The polycrystalline diamond compact of claim 11 wherein the first amount is about 60 volume % and the second amount is about 40 volume %, and wherein the first average grain size is about 12 μm and the second average grain size is about 20 μm.

16. The polycrystalline diamond compact of claim 11 wherein the polycrystalline diamond table includes boron in an amount from greater than 0 weight % to about 5 weight %.

17. The polycrystalline diamond compact of claim 16 wherein the amount is from greater than 0 weight % to about 0.2 weight %.

18. The polycrystalline diamond compact of claim 11 wherein the polycrystalline diamond table is integrally formed with the substrate.

19. The polycrystalline diamond compact of claim 11 wherein the polycrystalline diamond table includes at least one exterior surface and a leached region extending inwardly from of the at least one exterior surface to a depth of greater than 250 μm.

Assignments (6)
SECURITY INTEREST Recorded Jul 18, 2025
From: US SYNTHETIC CORPORATION
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 074973/0089 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: ACE DOWNHOLE, LLC; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; APERGY BMCS ACQUISITION CORP.; NORRISEAL-WELLMARK, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
Reel/Frame 060305/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: ACE DOWNHOLE, LLC; APERGY BMCS ACQUISITION CORP.; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 053790/0001 →
SECURITY AGREEMENT Recorded May 9, 2018
From: APERGY (DELAWARE) FORMATION, INC.; APERGY BMCS ACQUISITION CORP.; APERGY ENERGY AUTOMATION, LLC; HARBISON-FISCHER, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 046117/0015 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 4, 2013
From: LINFORD, BRANDON PAUL; KNUTESON, CODY WILLIAM
To: US SYNTHETIC CORPORATION
Reel/Frame 029569/0384 →