IP Library Granted Patent US 9,884,027
Granted Patent B2
US 9,884,027 · App. 13/740,913 · Granted Feb 6, 2018

Nanofiber scaffolds for biological structures

Inventor: Jed K. Johnson (London, OH)
Assignee: NANOFIBER SOLUTIONS, INC.
A61K9/70A61K35/12A61K47/32A61L27/3804A61L27/54A61L27/60A61L2300/252A61L2300/406A61L2300/41A61L2300/414
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Quick Facts
Patent No.
US 9,884,027
App. No.
13/740,913
Granted
Feb 6, 2018
Kind
B2
Abstract

A system for manufacturing an artificial construct suitable for transplantation into a biological organism that includes a two or three three-dimensional preform that is based on the actual two or three-dimensional structure of a native mammalian tissue; and an electrospinning apparatus, wherein the electrospinning apparatus is operative to deposit at least one layer of polymer fibers on the preform to form a polymer scaffold, and wherein the orientation of the fibers in the scaffold relative to one another is substantially parallel.

Claims (26)

1. A synthetic construct consisting of:

a single layer of electrospun polymer fibers, wherein at least about 75% of the fibers have a fiber angle within about 10° of parallel;

wherein the single layer has a shape of a patch and a thickness from about 0.2 mm to about 3 mm.

2. The synthetic construct of claim 1 , wherein the electrospun polymer fibers comprise a natural polymer selected from the group consisting of collagen, gelatin, fibronectin, hyaluronic acid, and combinations thereof.

3. The synthetic construct of claim 1 , wherein about 92% of the electrospun polymer fibers have a fiber angle within about10° of parallel.

4. The synthetic construct of claim 1 , wherein the electrospun polymer fibers comprise a polymer selected from the group consisting of polyethylene terephthalate, polycaprolactone, polylactic acid, polyglycolic acid, polyetherketoneketone, polyurethane, polycarbonate, polyamide, and combinations thereof.

5. A system comprising:

a rotatable preform based on a structure of a native mammalian tissue; and

an electrospinning apparatus comprising at least one anti-static bar;

wherein the at least one anti-static bar is positioned from about 0.5 inches to about 3 inches away from the rotatable preform.

6. The system of claim 5 , wherein the electrospinning apparatus includes a fiberization tip.

7. A method of making a synthetic construct, the method comprising:

creating an electronic field of about 1-40 kV proximate to a fiberization tip;

positioning a first ground within a preform;

positioning at least one anti-static device from about 0.5 inches to about 3 inches away from the preform;

rotating the preform in a rotation direction at a rotation rate;

extruding from the fiberization tip at a flow rate a polymer solution comprising a polymer and a solvent; and

depositing by electrospinning a plurality of polymer fibers on the preform, wherein at least about 75 % of the electrospun polymer fibers deposited have a fiber angle within about 10° from the rotation direction of the preform.

8. The method of claim 7 , wherein the solvent is selected from the group consisting of acetone, dimethylformamide, trifluoroactic acid, hexafluoroisopropanol, acetic acid, dim ethylacetamine, chloroform, dichloromethane, water, ionic compounds, and combinations thereof.

9. The method of claim 7 , wherein the at least one anti-static device is an anti-static bar.

10. The method of claim 7 , wherein the rotation rate is about 15.7 meters per second.

11. The method of claim 7 , wherein the percentage of the electrospun polymer fibers having a fiber angle within about 10 degrees of the rotation direction of the preform is selected from the group consisting of about 75%, about 91%, about 92%, and about 98%.

12. The method of claim 7 , wherein the preform further comprises a second ground.

13. The method of claim 12 , wherein the depositing by electrospinning further comprises alternating a ground between the first ground and the second ground.

14. The method of claim 7 , wherein the flow rate is about 1.0 ml/h.

15. The method of claim 7 , wherein the polymer is selected from the group consisting of polyethylene terephthalate, silicone, polyurethane, polycarbonate, polyether ketone, polycaprolactone, polylactic acid, polyglycolic acid, and combinations thereof.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 4, 2022
From: NANOFIBER SOLUTIONS, LLC
To: NFS IP HOLDINGS, LLC
Reel/Frame 061882/0663 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 22, 2020
From: JOHNSON, JED K.
To: NANOFIBER SOLUTIONS, LLC
Reel/Frame 052458/0796 →
CHANGE OF NAME Recorded Mar 21, 2019
From: NANOFIBER SOLUTIONS, INC.
To: NANOFIBER SOLUTIONS, LLC
Reel/Frame 048680/0973 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 5, 2018
From: JOHNSON, JED K.
To: NANOFIBER SOLUTIONS, INC.
Reel/Frame 045993/0097 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 21, 2015
From: JOHNSON, JED K.
To: NANOFIBER SOLUTIONS, INC.
Reel/Frame 034765/0826 →
Continuity (2)
Provisional Application 61585869 · Jan 12, 2012
Related Publication 20140030315A1 · Jan 30, 2014