IP Library Granted Patent US 8,778,262
Granted Patent B2
US 8,778,262 · App. 13/782,407 · Granted Jul 15, 2014

Alloy having reduced inclusions

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Quick Facts
Patent No.
US 8,778,262
App. No.
13/782,407
Granted
Jul 15, 2014
Kind
B2
Abstract

One aspect is an alloy consisting of niobium, zirconium, tantalum, and tungsten. The alloy is formed with a melt metallurgical route such that all four metals solidify as a homogeneous alloy having no inclusions more than 10 μm in size.

Claims (39)

1. An alloy consisting of niobium, zirconium, tantalum, and tungsten, wherein the alloy is formed with a melt metallurgical route such that all four metals solidify as a homogeneous alloy having no inclusions more than 10 μm in size and characterized in that the alloy comprises no mono-element inclusions.

2. The alloy of claim 1 characterized in that formation of the alloy employs the powder metallurgical and melt metallurgical routes sequentially such that the alloy has no inclusions more than 4 μm in size.

3. The alloy of claim 1 characterized in that formation of the alloy employs melting the alloy by means of the melt metallurgical route at least three times such that the alloy has no inclusions more than 0.2 μm in size such that the inclusion have negligible influence on fatigue resistance of the alloy.

4. The alloy of claim 1 characterized in that formation of the alloy employs grinding of each of the niobium, zirconium, tantalum, and tungsten such that all inclusions in the alloy are between 10 μm and 10 nm.

5. The alloy of claim 1 characterized in that formation of the alloy employs multiple melt metallurgical routes such that all inclusions in the alloy are between 10 μm and 10 nm.

6. The alloy of claim 5 characterized in that formation of the alloy employs multiple melt metallurgical routes such that all inclusions in the alloy are less than 0.1 μm.

7. The alloy of claim 1 characterized by the alloy comprising the following fractions of the metals:

0.5 wt-% to 10 wt-% zirconium,

0.5 wt-% to 9 wt-% tungsten,

20 wt-% to 40 wt-% tantalum, and

the remainder being accounted for by the niobium fraction.

8. The alloy of claim 1 characterized by the alloy comprising the following fractions of the metals:

0.5 wt-% to 2.3 wt-% zirconium,

2.5 wt-% to 4.5 wt-% tungsten,

24 wt-% to 32 wt-% tantalum, and

the remainder being the niobium fraction.

9. The alloy of claim 1 characterized by the alloy comprising the following fractions of the metals:

1.3 wt-% zirconium,

3.5 wt-% tungsten,

28 wt-% tantalum, and

the remainder being accounted for by the niobium fraction.

10. An implantable medical device, characterized by the implantable device being made up, at least in part, of an alloy consisting of niobium, zirconium, tantalum, and tungsten, wherein the alloy is formed with a melt metallurgical route and a melt metallurgical route such that all four metals solidify as a homogeneous alloy having no inclusions more than 10 μm in size and characterized in that the alloy comprises no mono-elemental inclusions.

11. The implantable medical device of claim 10 characterized in that formation of the alloy employs the powder metallurgical and melt metallurgical routes sequentially such that the alloy has no inclusions more than 4 μm in size.

12. The implantable medical device of claim 10 characterized in that formation of the alloy employs melting the alloy by means of the melt metallurgical route at least three times such that the alloy has no inclusions more than 0.2 μm in size such that the inclusion have negligible influence on fatigue resistance of the alloy.

13. The implantable medical device of claim 10 characterized in that formation of the alloy employs grinding of each of the niobium, zirconium, tantalum, and tungsten such that all inclusions in the alloy are between 10 μm and 10 nm.

14. The implantable medical device of claim 10 characterized in that formation of the alloy employs multiple melt metallurgical routes such that all inclusions of the alloy are between 10 μm and 10 nm.

15. The implantable medical device of claim 10 characterized by the alloy comprising the following fractions of the metals:

0.5 wt-% to 10 wt-% zirconium,

0.5 wt-% to 9 wt-% tungsten,

20 wt-% to 40 wt-% tantalum, and

the remainder being accounted for by the niobium fraction.

16. The implantable medical device according to claim 10 characterized by the implantable medical device being a stent or a precursor product of a stent or an electrode or a cardiac pacemaker casing or a cable or an electrical lead.

17. An alloy consisting of a first metal, a second metal, a third metal, and a fourth metal, characterized in that the first metal, the second metal, the third metal, and the fourth metal are selected from the group consisting of the metals, niobium, zirconium, tantalum, and tungsten; and such that all four metals solidify as a homogeneous alloy having no inclusions more than 10 μm in size; and

characterized in that the alloy is generated by:

grinding a first metal to form a first metal powder and grinding a second metal to form a second metal powder;

mixing the first metal powder and the second metal powder to form a first blended powder;

generating a first blended body from the blended powder by means of a powder metallurgical route; and

generating the alloy by melting the first blended body and a third metal and a fourth metal by means of a melt metallurgical route; and

characterized in that the alloy comprises no mono-elemental inclusions.

Assignments (2)
CHANGE OF NAME Recorded Nov 6, 2015
From: HERAEUS PRECIOUS METALS GMBH & CO. KG
To: HERAEUS DEUTSCHLAND GMBH & CO. KG
Reel/Frame 037056/0430 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 11, 2013
From: SCHIEFER, HERWIG; VOGT, CHRISTOPH; SPECHT, HEIKO; TROETZSCHEL, JENS
To: HERAEUS PRECIOUS METALS GMBH & CO. KG
Reel/Frame 031185/0706 →