Method for sintering
The present invention provides a method for sintering, comprising in the following order the steps of: providing a body in the green state or in the pre-sintered state on a support; providing a load on at least one spacer on the support such that the load is located above said body in the green state or in the pre-sintered state without contacting the body; heat treating the body in the green state or in the pre-sintered state at a temperature above the decomposition temperature of organic components contained in the green body and below the softening temperature or decomposition temperature of the spacer; heat treating the body in the green state or in the pre-sintered state at a temperature above the softening point or decomposition temperature of the spacer and below a sintering temperature such that the load contacts the body, and—sintering the body in the green state or pre-sintered state.
1. A method for sintering, said method comprising, in the following order, the steps of:
providing a body in the green state or in the pre-sintered state on a support;
providing a load on at least one spacer on the support such that the load is located above said body in the green state or in the pre-sintered state without contacting the body, wherein the load and the support are formed from the same material;
heat treating the body in the green state or in the pre-sintered state at a temperature above the decomposition temperature of organic components contained in the green body and below the softening temperature or decomposition temperature of the spacer, wherein the heat treatment is carried out at a temperature of from 350 to 450° C. for 0.5 to 5 hours;
heat treating the body in the green state or in the pre-sintered state at a temperature above the softening point or decomposition temperature of the spacer and below a sintering temperature such that the load contacts the body, wherein the heat treatment is carried out at a temperature of from 500 to 800° C. for 0.5 to 5 hours; and
sintering the body in the green state or pre-sintered state at a temperature of from 950° C. to 1500° C. for 0.5 to 5 hours,
wherein the at least one spacer is selected from carbon materials, polymeric materials and mixtures thereof.
2. The method of claim 1 , wherein the at least one spacer is provided in form of a rod, coil, brick or spring.
3. The method of claim 1 , wherein the support is a ceramic support.
4. The method of claim 3 , wherein the ceramic support is selected from alumina, zirconia or zirconia coated alumina.
5. The method of claim 1 , wherein the load is a flat plate.
6. The method of claim 5 , wherein the load is formed of a ceramic material.
7. The method of claim 6 , wherein the load is selected from alumina, zirconia or zirconia coated alumina.
8. The method of claim 1 , wherein the method comprises the provision of a body comprising at least two layers in the green state or pre-sintered state on a support.