IP Library Granted Patent US 9,333,532
Granted Patent B2
US 9,333,532 · App. 13/810,678 · Granted May 10, 2016

Method for producing a material including a substrate provided with a coating

Inventor: Andriy Kharchenko (Palaiseau, FR)
Assignee: SAINT-GOBAIN GLASS FRANCE
B05D5/12C03C17/36C03C17/366C03C17/3618C03C17/3626C03C17/3644C03C17/3652B05D5/00C03C2218/32C03C2218/328C03C2218/355
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Quick Facts
Patent No.
US 9,333,532
App. No.
13/810,678
Granted
May 10, 2016
Kind
B2
Abstract

The subject of the invention is a process for obtaining a material comprising a substrate provided on at least one of its faces with a permanent coating comprising at least one thin film, said process comprising the following steps: said permanent coating is deposited on at least one of the faces of said substrate; then a temporary coating is deposited directly on top of said permanent coating, said temporary coating comprising, as the layer closest to the substrate, at least one thin film soluble in a solvent, surmounted by at least one functional layer; then the substrate thus coated is subjected to a heat treatment; and then said coated substrate is treated with said solvent so as to remove said temporary coating from the surface of said substrate.

Claims (22)

1. A process for obtaining a material comprising a substrate comprising, on a face thereof, a permanent coating comprising a thin film, the process comprising:

depositing the permanent coating on a face of the substrate, to obtain a first coated substrate; then

depositing a temporary coating directly on top of the permanent coating, wherein the temporary coating comprises, as a layer closest to the substrate, a thin film soluble in a solvent, surmounted by a functional layer configured to absorb laser radiation having a wavelength of between 600 and 1200 nm, thereby obtaining a second coated substrate; then

heat treating the second coated substrate by rapid annealing with laser radiation having a wavelength of between 600 and 1200 nm and a surface power level greater than 20 kW/cm 2 absorbed by the functional layer, thereby improving the crystallization of a thin film of the permanent coating; and then,

contacting the second coated substrate with a solvent, thereby removing the temporary coating from the surface of the substrate, and wherein the process does not comprise heating the substrate to any temperature above 100° C.

2. The process of claim 1 , wherein the substrate is a glass or glass-ceramic sheet.

3. The process of claim 2 , wherein the substrate is a glass sheet.

4. The process of claim 2 , wherein the substrate is a glass-ceramic sheet.

5. The process of claim 1 , wherein the permanent coating comprises a thin film comprising a transparent electrically conductive oxide, silver, or titanium dioxide.

6. The process of claim 1 , wherein the solvent is water-based.

7. The process of claim 6 , wherein the thin film soluble in a solvent comprises a metal halide or a metal sulfate soluble in water.

8. The process of claim 7 , wherein the water-soluble thin film comprises a metal halide.

9. The process of claim 7 , wherein the water-soluble thin film comprises a metal sulfate.

10. The process of claim 1 , wherein the permanent coating comprises a thin film comprising a transparent electrically conductive oxide.

11. The process of claim 1 , wherein the permanent coating comprises a thin film comprising silver.

12. The process of claim 1 , wherein the permanent coating comprises a thin film comprising titanium dioxide.

13. The process of claim 1 , wherein the functional layer is a metal or metal nitride layer.

14. The process of claim 1 , wherein the functional layer is a metallic titanium layer.

15. The process of claim 1 , wherein the functional layer is a graphite layer.

16. The process of claim 1 , wherein, between depositing the temporary coating and contacting the second coated substrate with a solvent, a duration of the heat treating is one second or less.

17. The process of claim 1 , wherein the permanent coating is transparent.

18. The process of claim 1 , wherein the functional layer is configured to absorb laser radiation having a wavelength of between 700 and 1200 nm, and wherein heat treating the second coated substrate by rapid annealing is with laser radiation having a wavelength of between 700 and 1200 nm and a surface power level of greater than 20 kW/cm 2 absorbed by the functional layer, thereby improving the crystallization of a thin film of the permanent coating.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 24, 2013
From: KHARCHENKO, ANDRIY
To: SAINT-GOBAIN GLASS FRANCE
Reel/Frame 029685/0768 →
Priority Claims (1)
FR 10 56165 · Jul 27, 2010 · national
Continuity (1)
Related Publication 20130115468A1 · May 9, 2013