IP Library Granted Patent US 8,974,611
Granted Patent B2
US 8,974,611 · App. 13/815,075 · Granted Mar 10, 2015

Methods of producing deformed metal articles

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Quick Facts
Patent No.
US 8,974,611
App. No.
13/815,075
Granted
Mar 10, 2015
Kind
B2
Abstract

A method of making metal articles as well as sputtering targets is described, which involves deforming an ingot to preferred dimensions. In addition, products made by the process of the present invention are further described.

Claims (31)

1. A BCC metal having a texture gradient uniformity factor (H) of 0.3 or less wherein said BCC metal is a plate and is ingot-derived from melt feedstock.

2. The BCC metal of claim 1 , wherein said texture gradient uniformity factor is from about 0.1 to 0.2.

3. The BCC metal of claim 1 , wherein said texture gradient uniformity factor is from about 0.12 to about 0.17.

4. The BCC metal of claim 1 , wherein said BCC metal is tantalum.

5. The BCC metal of claim 1 , wherein the uniformity factor varies no more than ±0.1 throughout the BCC metal.

6. The BCC metal of claim 1 , wherein said BCC metal is tantalum or niobium, and having a metal purity of at least 99.95% of said BCC metal, and having an average grain size of 150 microns or less.

7. The BCC metal of claim 6 , wherein at least 95% of all grains present have a grain size of 100 microns or less.

8. The BCC metal of claim 6 , wherein said BCC metal has a degree random or times random of texture throughout the plate which varies no more than 5 degrees or times random.

9. The BCC metal of claim 6 , wherein said BCC metal has a degree random or times random of texture throughout the plate which varies no more than 2 degrees or times random.

10. The BCC metal of claim 1 , wherein said BCC metal is tantalum or niobium, and having a metal purity of at least 99.95% of said BCC metal, and having an average grain size of 5 to 50 microns.

11. The BCC metal of claim 10 , wherein at least 95% of all grains present have a grain size of 75 microns or less.

12. The BCC metal of claim 10 , wherein said BCC metal has a degree random or times random of texture throughout the plate which varies no more than 5 degrees or times random.

13. The BCC metal of claim 10 , wherein said BCC metal has a degree random or times random of texture throughout the plate which varies no more than 2 degrees or times random.

14. A BCC metal having a texture gradient banding factor (B) of 0.1 or less wherein said BCC metal is a plate and is ingot-derived from melt feedstock, and wherein said BCC metal has a texture gradient uniformity factor (H) of 0.2 or less.

15. The BCC metal of claim 14 , wherein said texture gradient banding factor is from about 0.01 to about 0.075.

16. The BCC metal of claim 14 , wherein said texture gradient banding factor is from about 0.02 to about 0.05.

17. The BCC metal of claim 14 , wherein said texture gradient uniformity factor is from about 0.1 to 0.2.

18. The BCC metal of claim 14 , wherein said texture gradient uniformity factor is from about 0.12 to about 0.17.

19. The BCC metal of claim 14 , wherein said BCC metal is tantalum.

20. The BCC metal of claim 14 , having a metal purity of at least 99.95% of said BCC metal.

21. The BCC metal of claim 14 , wherein said BCC metal has an average grain size of about 75 microns or less.

22. The BCC metal of claim 14 , wherein said BCC metal is tantalum and has a primary (111) texture throughout the thickness of the BCC metal.

23. The BCC metal of claim 14 , wherein the texture gradient banding factor varies no more than ±0.05 throughout the BCC metal.

24. The BCC metal of claim 14 , wherein said BCC metal is tantalum or niobium, and having a metal purity of at least 99.95% of said BCC metal, and having an average grain size of 150 microns or less.

25. The BCC metal of claim 24 , wherein at least 95% of all grains present have a grain size of 100 microns or less.

26. The BCC metal of claim 24 , wherein said BCC metal has a degree random or times random of texture throughout the plate which varies no more than 5 degrees or times random.

27. The BCC metal of claim 24 , wherein said BCC metal has a degree random or times random of texture throughout the plate which varies no more than 2 degrees or times random.

28. The BCC metal of claim 14 , wherein said BCC metal is tantalum or niobium, and having a metal purity of at least 99.95% of said BCC metal, and having an average grain size of 5 to 50 microns.

29. The BCC metal of claim 28 , wherein at least 95% of all grains present have a grain size of 75 microns or less.

30. The BCC metal of claim 28 , wherein said BCC metal has a degree random or times random of texture throughout the plate which varies no more than 5 degrees or times random.

31. The BCC metal of claim 28 , wherein said BCC metal has a degree random or times random of texture throughout the plate which varies no more than 2 degrees or times random.

Assignments (5)
RELEASE OF SECURITY INTERESTS Recorded Jul 9, 2019
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: GLOBAL ADVANCED METALS USA, INC.
Reel/Frame 049705/0929 →
SECURITY INTEREST Recorded Jul 7, 2014
From: TAL HOLDINGS, LLC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 033279/0731 →
SECURITY INTEREST Recorded May 1, 2014
From: GLOBAL ADVANCED METALS USA, INC.
To: TAL HOLDINGS, LLC.
Reel/Frame 032798/0117 →
SECURITY AGREEMENT Recorded Apr 29, 2014
From: GLOBAL ADVANCED METALS USA, INC.
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 032816/0878 →
RELEASE OF SECURITY INTEREST Recorded Apr 9, 2014
From: CABOT CORPORATION
To: GLOBAL ADVANCED METALS USA, INC.
Reel/Frame 032764/0791 →