Method for producing R-T-B sintered magnet
View Patent ↗[Problem] To provide a highly efficient manufacturing method including an RH supply-diffusion process by which the number of magnets processed at a time can be increased without allowing sintered R-T-B based magnets to stick to holding members. [Solution] A method for producing a sintered R-T-B based magnet including the steps of: forming a stack of RH diffusion sources and sintered R-T-B based magnet bodies by stacking the diffusion sources and the magnet bodies alternately with a holding member having openings interposed; and carrying out an RH supply-diffusion process by loading the stack into a process vessel and creating an atmosphere with a pressure of 0.1 Pa to 50 Pa and a temperature of 800° C. to 950° C. within the process vessel.
1. A method for producing a sintered R-T-B based magnet, the method comprising the steps of:
forming a stack of RH diffusion sources (which are made of a metal or alloy, of which at least 80 at % is a heavy rare-earth element RH that is at least one of Dy and Tb) and sintered R-T-B based magnet bodies (where R is at least one of the rare-earth elements and T is at least one of the transition metal elements and always includes Fe) by stacking the diffusion sources and the magnet bodies alternately with a holding member having openings interposed;
carrying out an RH supply-diffusion process by loading the stack into a process vessel and creating an atmosphere with a pressure of 0.3 Pa to 50 Pa and a temperature of 800° C. to 950° C. within the process vessel, wherein throughout the RH supply-diffusion process, the pressure is maintained between 0.3 Pa to 50 Pa and the temperature is maintained between 800° C. to 950° C.; and
carrying out an RH diffusion process by creating an atmosphere with a pressure of 200 Pa to 2 kPa and a temperature of 800° C. to 950° C. in the process vessel after the RH supply-diffusion process has been carried out, wherein throughout the RH diffusion process, the pressure is maintained between 200 Pa to 2 kPa and the temperature is maintained between 800° C. to 950° C.
2. The method of claim 1 , wherein the holding member has a thickness of 0.1 mm to 4 mm.
3. The method of claim 1 , further comprising decreasing the temperature in the process vessel to 500° C. at a cooling rate of 1° C. per minute to 15° C. per minute after either the RH supply-diffusion process or the RH diffusion process has been carried out.
4. The method of claim 1 , wherein the process vessel is evacuated using a rotary pump with or without a mechanical booster pump.