R-T-B sintered magnet manufacturing method
View Patent ↗[Problem] To provide a heavy rare-earth element RH diffusion process that contributes greatly to mass production. [Solution] A method for producing a sintered magnet includes the steps of: providing a sintered R-T-B based magnet body; providing an RH diffusion source which is made of at least one of a fluoride, an oxide and an oxyfluoride that each include Dy and/or Tb; loading the sintered R-T-B based magnet body and the RH diffusion source into a process chamber so that the magnet body and the diffusion source are movable relative to each other and are readily brought close to, or into contact with, each other; and performing an RH diffusion process in which the sintered R-T-B based magnet body and the RH diffusion source are heated to a processing temperature of 800° C. through 950° C. while being moved either continuously or discontinuously in the process chamber.
1. A method for producing a sintered R-T-B based magnet, the method comprising the steps of:
providing a sintered R-T-B based magnet body;
providing an RH diffusion source which is made of at least one of a fluoride, an oxide and an oxyfluoride that each include Dy and/or Tb;
loading the sintered R-T-B based magnet body and the RH diffusion source into a process chamber so that the magnet body and the diffusion source are movable relative to each other and are readily brought close to, or into contact with, each other; and
performing an RH diffusion process in which the sintered R-T-B based magnet body and the RH diffusion source are heated to a processing temperature of 800° C. through 950° C. while being moved either continuously or discontinuously in the process chamber so that the magnet body and the diffusion source are moved relative to each other and are brought close to, or into contact with, each other; wherein
in the RH diffusion process, the process chamber is heated by a heater that is arranged around an outer periphery of the process chamber, the sintered R-T-B based magnet body and the RH diffusion source that are loaded into the process chamber are also heated, and the temperature of the sintered R-T-B based magnet body and the RH diffusion source is maintained within a range of 800° C. to 950° C.;
the RH diffusion process step is carried out using a stirring aid member loaded into the process chamber; and
the stirring aid member is made of zirconia, silicon nitride, silicon carbide, boron nitride, or a ceramic that includes any combination of zirconia, silicon nitride, silicon carbide, boron nitride.