IP Library Granted Patent US 9,095,582
Granted Patent B2
US 9,095,582 · App. 13/893,344 · Granted Aug 4, 2015

Substituted aryloxazoles and their use

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Quick Facts
Patent No.
US 9,095,582
App. No.
13/893,344
Granted
Aug 4, 2015
Kind
B2
Abstract

The present application relates to novel substituted aryloxazole derivatives, to processes for their preparation, to their use for the treatment and/or prophylaxis of diseases and to their use for preparing medicaments for the treatment and/or prophylaxis of diseases, preferably for the treatment and/or prevention of cardiovascular and metabolic disorders.

Claims (60)

1. A compound of the formula (I)

in which

A represents O or S,

R 1 represents hydrogen or (C 1 -C 4 )-alkyl,

R 2 represents hydrogen or (C 1 -C 4 )-alkyl which may be substituted by hydroxyl, (C 1 -C 4 )-alkoxy or up to three times by fluorine

or

R 1 and R 2 are attached to one another and together with the carbon atom to which they are attached form a cyclopropane or cyclobutane ring,

R 3 represents hydrogen, halogen or (C 1 -C 4 )-alkyl,

R 4 and R 5 together with the nitrogen atom to which they are attached form a pyrrolidino ring which may be mono- or disubstituted by identical or different substituents from the group consisting of (C 1 -C 4 )-alkyl, hydroxyl, oxo and (C 1 -C 4 )-alkoxy,

and either (i)

R 6 represents (C 6 -C 10 )-aryl which may be mono- to trisubstituted by identical or different substituents from the group consisting of halogen, nitro, cyano, (C 1 -C 4 )-alkyl, trifluoromethyl, hydroxyl, (C 1 -C 4 )-alkoxy, difluoromethoxy, trifluoromethoxy, mono-(C 1 -C 4 )-alkylaminocarbonyl, (C 1 -C 4 )-alkoxycarbonyl and carboxyl,

and

R 7 represents hydrogen, fluorine, chlorine, (C 1 -C 4 )-alkyl, trifluoromethyl, (C 1 -C 4 )-alkoxycarbonyl, carboxyl or phenyl, where

(C 1 -C 4 )-alkyl may be substituted by hydroxyl or (C 1 -C 4 )-alkoxy

and

phenyl may be substituted by halogen, cyano, (C 1 -C 4 )-alkyl or trifluoromethyl,

or (ii)

R 6 represents hydrogen or (C 1 -C 4 )-alkyl

and

R 7 represents phenyl which may be mono- or disubstituted by identical or different substituents from the group consisting of halogen, cyano, (C 1 -C 4 )-alkyl and trifluoromethyl,

or a salt thereof.

2. The compound of claim 1 in which

A represents O or S,

R 1 represents hydrogen or methyl,

R 2 represents hydrogen, methyl, hydroxymethyl, methoxymethyl or trifluoromethyl,

R 3 represents hydrogen, fluorine or methyl,

R 4 and R 5 together with the nitrogen atom to which they are attached form a pyrrolidino ring which may be mono- or disubstituted by identical or different substituents from the group consisting of methyl, hydroxyl and/or methoxy,

and either (i)

R 6 represents phenyl, which may be mono- to trisubstituted by identical or different substituents from the group consisting of fluorine, chlorine, cyano, (C 1 -C 4 )-alkyl, trifluoromethyl, (C 1 -C 4 )-alkoxy, trifluoromethoxy, mono-(C 1 -C 4 )-alkylaminocarbonyl, (C 1 -C 4 )-alkoxycarbonyl and carboxyl,

and

R 7 represents hydrogen, (C 1 -C 4 )-alkyl, trifluoromethyl, (C 1 -C 4 )-alkoxycarbonyl, carboxyl or phenyl which may be substituted by fluorine or chlorine,

or (ii)

R 6 represents hydrogen

and

R 7 represents phenyl which may be mono- or disubstituted by identical or different substituents from the group consisting of fluorine, chlorine, cyano, methyl and trifluoromethyl,

or a salt thereof.

3. The compound of claim 1 in which

A represents O or S,

R 1 represents hydrogen or methyl,

R 2 represents hydrogen, methyl, hydroxymethyl or trifluoromethyl,

R 3 represents hydrogen or fluorine,

R 4 and R 5 together with the nitrogen atom to which they are attached form a pyrrolidino ring, which may be substituted by hydroxyl,

R 6 represents phenyl which may be mono- or disubstituted by identical or different substituents from the group consisting of fluorine, chlorine, methyl, trifluoromethyl, methoxy and carboxyl,

and

R 7 represents hydrogen, methyl, trifluoromethyl, methoxycarbonyl or carboxyl,

or a salt thereof.

4. A process for preparing compounds of formula (I) as defined in claim 1 comprising:

reacting a compound of formula (II)

in which A, R 1 , R 2 , R 3 , R 4 and R 5 have the meaning given in claim 1 ,

and

R 8 represents hydrogen or a temporary hydroxyl protective group

in an inert solvent in the presence of a base with a compound of formula (III)

in which R 6 and R 7 have the meanings given in claim 1 and

Q represents halogen, mesylate, tosylate or triflate,

or alternatively, if A represents O, reacting a compound of formula (IV)

in which R 1 , R 2 , R 3 , R 4 , R 5 and R 8 each have the meanings given above

in an inert solvent in the presence of a base with a compound of formula (V)

in which R 6 and R 7 have the meaning given in claim 1 ,

removing any protective groups present, and optionally reacting the resulting compound of formula (I) with a base or acid to produce a salt thereof.

5. A pharmaceutical composition comprising a compound of claim 1 and one or more inert nontoxic pharmaceutically suitable auxiliaries.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 9, 2014
From: BAYER SCHERING PHARMA AKTIENGESELLSCHAFT
To: BAYER PHARMA AKTIENGESELLSCHAFT
Reel/Frame 033283/0004 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 2, 2014
From: BAYER PHARMA AKTIENGESELLSCHAFT
To: BAYER INTELLECTUAL PROPERTY GMBH
Reel/Frame 033230/0119 →
CHANGE OF NAME Recorded Jul 1, 2014
From: BAYER SCHERING PHARMA AG
To: BAYER PHARMA AKTIENGESELLSCHAFT
Reel/Frame 033265/0193 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 9, 2014
From: NELL, PETER, DR.; HUBSCH, WALTER, DR.; ALBRECHT-KUPPER, BARBARA, DR.; KELDENICH, JOERG, DR.; VAKALOPOULOS, ALEXANDROS, DR.; SUSSMEIER, FRANK; ZIMMERMANN, KATJA, DR.; LANG, DIETER, DR.; MEIBOM, DANIEL, DR.
To: BAYER SCHERING PHARMA AKTIENGESELLSCHAFT
Reel/Frame 033058/0113 →