IP Library Granted Patent US 9,446,078
Granted Patent B2
US 9,446,078 · App. 13/925,993 · Granted Sep 20, 2016

Sterilized and decellularized extracellular matrix for treating cardiac arrhythmia

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Quick Facts
Patent No.
US 9,446,078
App. No.
13/925,993
Granted
Sep 20, 2016
Kind
B2
Abstract

Disclosed herein are compositions and methods for treating or preventing a cardiac arrhythmia in a subject.

Claims (30)

1. A composition for treating a cardiac arrhythmia, comprising:

a non-immunogenic regenerative biomaterial construct comprising sterilized and decellularized ECM derived from xenogeneic small intestine submucosa (SIS) tissue,

said ECM comprising a decellularization level of at least 96%,

said regenerative biomaterial construct being configured to be directly delivered to damaged myocardial tissue of a subject's heart,

said regenerative biomaterial construct being further configured to modulate electrical said subject's heart by inducing myofibroblast proliferation and angiogenesis of said damaged myocardial tissue and, thereby, positive remodeling of said damaged myocardial tissue, when said regenerative biomaterial construct is administered to said damaged myocardial tissue,

said regenerative construct being formed in vitro by a sterilization and decellularization process comprising (i) introducing said ECM into a reactor pressure vessel, (ii) introducing sterilant comprising carbon dioxide (CO2) into said reactor pressure vessel at a first controlled pressurization rate, (iii) pressurizing said reactor pressure vessel at a pressure in the range of approximately 1000-3500 psi and at a temperature in the range of 25°-60° C., (iv) maintaining said ECM in contact with said CO2 at said vessel pressure and temperature for a minimum first processing time no less than 20 minutes said steps of introducing said CO2 into said vessel interior space and maintaining said vessel pressure and temperature being performed contemporaneously during a maximum processing time no greater than 60 minutes, and (v) depressurizing said reactor pressure vessel at a depressurizing rate in the range of 725-1450 psi/min,

wherein said ECM exhibits a significantly altered collagen structure and significantly reduced glycosaminoglycan (GAG) and xenogeneic antigen content compared to a non-sterilized and non-decellularized ECM derived from xenogeneic small intestine submucosa (SIS) tissue, and

wherein said ECM comprises a post-processing dry weight TGF-β content of at least 2.8 pg/mg and bFGF content of at least 19 pg/mg.

2. A composition for treating a cardiac arrhythmia, comprising:

a non-immunogenic regenerative biomaterial construct comprising sterilized and decellularized ECM derived from xenogeneic small intestine submucosa (SIS) tissue,

said ECM comprising a decellularization level of at least 96%,

said regenerative biomaterial construct being configured to be directly delivered to damaged myocardial tissue of a subject's heart,

said regenerative biomaterial construct being further configured to modulate electrical activity of said subject's heart by inducing myofibroblast proliferation and angiogenesis of said damaged myocardial tissue and, thereby, positive remodeling of said dan1aged myocardial tissue, when said regenerative biomaterial construct is administered to said damaged myocardial tissue,

said regenerative construct being formed in vitro by a sterilization and decellularization process comprising (i) introducing said ECM into a reactor pressure vessel, (ii) introducing a sterilant comprising carbon dioxide (CO2) into said reactor pressure vessel at a first controlled pressurization rate, (iii) pressurizing said reactor pressure vessel at a pressure in the range of approximately 1000-3500 psi and at a temperature in the range of 25°-60° C., (iv) maintaining said ECM in contact with said CO2 at said vessel pressure and temperature for a minimum first processing time no less than 20 minutes, said steps of introducing said CO2 into said vessel interior space and maintaining said vessel pressure and temperature being performed contemporaneously during a maximum processing time no greater than 60 minutes, (v) rapidly depressurizing said reactor pressure vessel at a depressurizing rate in the range of 725-1450 psi/min, and (vi) introducing a non-native biologically active agent into said interior space of said reactor vessel during said rapid depressurization step,

wherein said ECM exhibits a significantly altered collagen structure and significantly reduced glycosaminoglycan (GAG) and xenogeneic antigen content compared to a non-sterilized and non-decellularized ECM derived from xenogeneic small intestine submucosa (SIS) tissue, and wherein said non-native biologically active agent is incorporated into said ECM.

3. The composition of claim 2 , wherein said non-native biologically active agent comprises a statin, said statin comprising cerivastatin.

4. The composition of claim 2 , wherein said non-native biologically active agent comprises an anti-arrhythmic agent, said anti-arrhythmic agent comprising propranolol.

5. The composition of claim 2 , wherein said non-native biologically active agent comprises an antibiotic.

6. The composition of claim 2 , wherein said cardiac arrhythmia comprises atrial fibrillation.

7. A composition for treating a cardiac arrhythlnia, comprising:

a non-immunogenic regenerative biomaterial construct comprising sterilized and decellularized ECM derived from xenogeneic small intestine submucosa (SIS) tissue,

said ECM comprising a decellularization level of at least 96%,

said regenerative biomaterial construct being configured to be directly delivered to damaged myocardial tissue of a subject's heart,

said regenerative biomaterial construct being further configured to modulate electrical activity of said subject's heart by inducing myofibroblast proliferation and angiogenesis of said damaged myocardial tissue and, thereby, positive remodeling of said damaged myocardial tissue, when said regenerative biomaterial construct is administered to said damaged myocardial tissue,

said regenerative construct being formed in vitro by a sterilization and decellularization process comprising (i) introducing said ECM into a reactor pressure vessel, (ii) introducing a sterilant comprising carbon dioxide (CO2) into said reactor pressure vessel at a first controlled pressurization rate, (iii) pressurizing said reactor pressure vessel at a pressure in the range of approximately 1000-3500 psi and at a temperature in the range of 25°-60° C., (iv) maintaining said ECM in contact with said CO2 at said vessel pressure and temperature for a minimum first processing time no less than 20 minutes, said steps of introducing said CO2 into said vessel interior space and maintaining said vessel pressure and temperature being performed contemporaneously during a maximum processing time no greater than 60 minutes, (v) rapidly depressurizing said reactor pressure vessel at a depressurizing rate in the range of 725-1450 psi/min, and (vi) introducing a supplemental native biologically active agent into said interior space of said reactor vessel during said rapid depressurization step,

wherein said ECM exhibits a significantly altered collagen structure and significantly reduced glycosaminoglycan (GAG) and xenogeneic antigen content compared to a non-sterilized and non-decellularized ECM derived from xenogeneic small intestine submucosa (SIS) tissue, and

wherein said supplemental native biologically active agent is incorporated into said ECM.

8. The composition of claim 7 , wherein said supplemental native biologically active agent comprises a cytokine, said cytokine comprising interleukin-10.

9. The composition of claim 7 , wherein said supplemental native biologically active agent comprises a growth factor, said growth factor comprising transforming growth factor-β (TGF-β).

10. The composition of claim 7 , wherein said cardiac arrhythmia comprises atrial fibrillation.

Assignments (10)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 12, 2025
From: CORMATRIX CARDIOVASCULAR, INC.
To: CORVIVO CARDIOVASCULAR, INC.
Reel/Frame 070482/0001 →
CHANGE OF NAME Recorded Sep 15, 2023
From: AZIYO MED, LLC
To: ELUTIA MED LLC
Reel/Frame 064923/0704 →
CHANGE OF NAME Recorded Sep 15, 2023
From: AZIYO BIOLOGICS, INC.
To: ELUTIA INC.
Reel/Frame 064923/0361 →
RELEASE OF SECURITY INTEREST Recorded Aug 12, 2022
From: AZIYO BIOLOGICS, INC.; AZIYO MED, LLC
To: MIDCAP FINANCIAL TRUST
Reel/Frame 061161/0001 →
RELEASE OF SECURITY INTEREST Recorded Aug 12, 2022
From: AZIYO BIOLOGICS, INC.; AZIYO MED, LLC
To: MIDCAP FUNDING IV TRUST
Reel/Frame 061164/0532 →
SEURITY INTEREST (TERM) Recorded Aug 2, 2017
From: AZIYO BIOLOGICS, INC.; AZIYO MED, LLC
To: MIDCAP FINANCIAL TRUST, AS AGENT
Reel/Frame 043413/0942 →
SECURITY INTEREST (REVOLVING) Recorded Aug 2, 2017
From: AZIYO BIOLOGICS, INC.; AZIYO MED, LLC
To: MIDCAP FINANCIAL TRUST, AS AGENT
Reel/Frame 043414/0001 →
RELEASE OF SECURITY INTEREST Recorded Jun 2, 2017
From: MIDCAP FINANCIAL TRUST
To: CORMATRIX CARDIOVASCULAR, INC.
Reel/Frame 042669/0559 →
SECURITY INTEREST Recorded Sep 30, 2015
From: CORMATRIX CARDIOVASCULAR, INC.
To: MIDCAP FINANCIAL TRUST
Reel/Frame 036732/0103 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 6, 2013
From: MATHENY, ROBERT G
To: CORMATRIX CARDIOVASCULAR, INC.
Reel/Frame 030746/0050 →