IP Library Granted Patent US 9,351,937
Granted Patent B2
US 9,351,937 · App. 13/954,184 · Granted May 31, 2016

Controlled release pharmaceutical formulations of nitazoxanide

Inventors: Jean-Francois Rossignol (St. Petersburg, FL); Marc Ayers (Tampa, FL)
Assignee: Romark Laboratories L.C.
A61K9/2086A61K9/209A61K9/28A61K9/284A61K9/2853A61K31/426A61K31/7056A61K38/21
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Quick Facts
Patent No.
US 9,351,937
App. No.
13/954,184
Granted
May 31, 2016
Kind
B2
Abstract

Solid dosage formulations of nitazoxanide or a nitazoxanide analog are provided that comprise a controlled release portion and an immediate release portion. The pharmaceutical composition is typically in the form of a bilayer solid oral dosage form comprising (a) a first layer comprising a first quantity of nitazoxanide or analog thereof in a controlled release formulation; and (b) a second layer comprising a second quantity of nitazoxanide or analog thereof in an immediate release formulation. Method of using the formulations in the treatment of hepatitis C are also provided.

Claims (28)

1. A method of reducing one or more side-effects associated with treatment with nitazoxanide or tizoxanide in a patient, the method comprising administering to the patient a therapeutically effective amount of a pharmaceutical composition in the form of a solid dosage form, the composition comprising (a) a first portion comprising a first quantity of nitazoxanide, tizoxanide or a pharmaceutically acceptable salt or ester thereof in a controlled release formulation; and (b) a second portion comprising a second quantity of nitazoxanide, tizoxanide or a pharmaceutically acceptable salt or ester thereof in an immediate release formulation, wherein the one or more side effects is selected from abdominal pain, diarrhea, flatulence and nausea.

2. The method of claim 1 , wherein the first and second quantities of nitazoxanide, tizoxanide or a pharmaceutically acceptable salt or ester thereof are each nitazoxanide.

3. The method of claim 2 , wherein the first portion further comprises a low viscosity polymer.

4. The method of claim 2 , wherein the ratio of the first quantity of nitazoxanide to the second quantity of nitazoxanide is about 2.5:1 to about 4:1.

5. The method of claim 2 , wherein

the first quantity of nitazoxanide comprises about 500 mg of nitazoxanide; and

the second quantity of nitazoxanide comprises about 175 mg of nitazoxanide in an immediate release formulation.

6. The method of claim 2 , wherein the solid dosage form is a bilayer tablet wherein:

the first portion (a) forms a first layer comprising about 500 mg of nitazoxanide in a controlled release formulation, and further comprising a low-viscosity hydroxypropylmethylcellulose;

the second portion (b) forms a second layer comprising about 175 mg of nitazoxanide in an immediate release formulation, the second layer deposited on top of and compressed with the first layer to form a core tablet.

7. The method of claim 6 , wherein the tablet further comprises an outer coating (c) applied to the core tablet.

8. The method of claim 2 , wherein the solid oral dosage form is a tablet.

9. The method of claim 2 , wherein the solid oral dosage form is a capsule.

10. The method of claim 9 , wherein the first portion (a) is in the form of controlled-release granules containing the first quantity of nitazoxanide, and the second portion (b) is in the form of immediate-release granules containing the second quantity of nitazoxanide.

11. A method for increasing the bioavailability of nitazoxanide or an analogue thereof in a patient, the method comprising administering to the patient a therapeutically effective amount of a pharmaceutical composition in the form of a solid dosage form, the composition comprising (a) a first portion comprising a first quantity of nitazoxanide, tizoxanide or a pharmaceutically acceptable salt or ester thereof in a controlled release formulation; and (b) a second portion comprising a second quantity of nitazoxanide, tizoxanide or a pharmaceutically acceptable salt or ester thereof in an immediate release formulation.

12. The method of claim 11 , wherein the first and second quantities of nitazoxanide, tizoxanide or a pharmaceutically acceptable salt or ester thereof are each nitazoxanide.

13. The method of claim 12 , wherein the first portion further comprises a low viscosity polymer.

14. The method of claim 12 , wherein the ratio of the first quantity of nitazoxanide to the second quantity of nitazoxanide or an analogue thereof is about 2.5:1 to about 4:1.

15. The method of claim 12 , wherein

the first quantity of nitazoxanide comprises about 500 mg of nitazoxanide; and

the second quantity of nitazoxanide comprises about 175 mg of nitazoxanide in an immediate release formulation.

16. The method of claim 12 , wherein the solid dosage form is a bilayer tablet wherein:

the first portion (a) forms a first layer comprising about 500 mg of nitazoxanide in a controlled release formulation, and further comprising a low-viscosity hydroxypropylmethylcellulose;

the second portion (b) forms a second layer comprising about 175 mg of nitazoxanide in an immediate release formulation, the second layer deposited on top of and compressed with the first layer to form a core tablet.

17. The method of claim 16 , wherein the tablet further comprises an outer coating (c) applied to the core tablet.

18. The method of claim 12 , wherein the solid oral dosage form is a tablet.

19. The method of claim 12 , wherein the solid oral dosage form is a capsule.

20. The method of claim 19 , wherein the first portion (a) is in the form of controlled-release granules containing the first quantity of nitazoxanide, and the second portion (b) is in the form of immediate-release granules containing the second quantity of nitazoxanide.

Assignments (5)
SECURITY INTEREST Recorded Nov 16, 2019
From: ROMARK BIOSCIENCES S.À R.L. LLC; ROMARK LABORATORIES, L.C.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 051030/0613 →
SECURITY INTEREST Recorded Jul 2, 2018
From: ROMARK BIOSCIENCES S.À R.L. LLC; ROMARK LABORATORIES, L.C.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 046254/0524 →
SECURITY INTEREST Recorded Dec 22, 2017
From: ROMARK BIOSCIENCES S.À R.L. LLC; ROMARK LABORATORIES, L.C.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 044472/0001 →
RELEASE OF SECURITY INTEREST Recorded Mar 6, 2015
From: U.S. BANK NATIONAL ASSOCIATION
To: ROMARK LABORATORIES, L.C.; ROMARK MANUFACTURING, LLC; LAPICOR, N.V.
Reel/Frame 035108/0474 →
SECURITY AGREEMENT Recorded Sep 4, 2013
From: ROMARK LABORATORIES, L.C.; ROMARK MANUFACTURING, LLC; LAPICOR, N.V.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 031156/0923 →
Continuity (3)
Division 12656704 · Feb 12, 2010
Provisional Application 61202285 · Feb 13, 2009
Related Publication 20140065215A1 · Mar 6, 2014