IP Library Patent Application 13957724
Patent Application
App. No. 13/957,724

SWEETENER CRYSTALS AND METHOD OF MAKING

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Patent No.
US None
App. No.
13/957,724
Abstract

A sweetening composition comprising a crystalline matrix wherein the crystalline matrix comprises a high intensity sweetener and a carrier/substrate, and wherein the composition has a bulk density of about 0.4 g/cc to about 1.0 g/cc.

Claims (44)

1 . A sweetening composition comprising:

a crystalline matrix wherein the crystalline matrix comprises a high intensity sweetener and a carrier/substrate, and wherein the composition has a bulk density of about 0.4 g/cc to about 1.0 g/cc.

2 . The composition of claim 1 , wherein the composition has a bulk density of about 0.5 g/cc to about 0.85 g/cc.

3 . The composition of claim 1 , wherein the high intensity sweetener is selected from the group consisting of aspartame, acesulfame, alitame, brazzein, cyclamic acid, dihydrochalcones, extract of Dioscorophyllum cumminsii , extract of the fruit of Pentadiplandra brazzeana , glycyrrhizin, hernandulcin, monatin, monellin, mogroside, neotame, neohesperidin, saccharin, sucralose, stevia extracts, luo han guo, agave, Thaumatin katemfe fruit ( Thaumatococcus daniellii ), Hernandulcin-lippia duclis, and combinations thereof.

4 . The composition of claim 1 , wherein the high intensity sweetener is luo han guo.

5 . The composition of claim 1 , wherein the carrier/substrate is selected from the group consisting of a monosaccharide, a disaccharide, a polysaccharide, a sugar alcohol, a low-intensity sweetener and mixtures thereof.

6 . The composition of claim 1 , wherein the carrier/substrate is glucose, fructose, galactose, xylose, ribose, sucrose, lactulose, lactose, maltose, trehalose, cellobiose, kojibiose, nigerose, isomaltose, β,β-trehalose, α,β-trehalose, sophorose, laminaribiose, gentiobiose, turanose, maltulose, palatinose, gentiobiulose, mannobiose, melibiose, melibiulose, rutinose, rutinulose, xylobiose, erythritol, glycol, glycerol, threitol, arabitol, xylitol, ribitol, mannitol, sorbitol, dulcitol, iditol, isomalt, maltitol, lactitol, polyglycitol, maltodextrin and mixtures thereof.

7 . The composition of claim 1 , wherein the sweetening composition has less than 0.25 kcal per gram of SES.

8 . The composition of claim 1 , wherein the sweetening composition has less than 0.5 kcal per gram of SES.

9 . The composition of claim 1 , wherein the sweetening composition has a ratio of carrier/substrate to high intensity sweetener is from about 1:1 to about 99.9:0.1.

10 . The composition of claim 1 , wherein the sweetening composition has a ratio of carrier/substrate to high intensity sweetener is from about 10:1 to about 90:1.

11 . The composition of claim 1 , wherein the sweetening composition has a ratio of carrier/substrate to high intensity sweetener is from about 25:1 to about 50:1.

12 . The composition of claim 1 , wherein the sweetening composition has a ratio of carrier/substrate to high intensity sweetener is from about 30:1 to about 40:1.

13 . The composition of claim 1 , wherein the composition has a particle size from about 250 microns to about 2000 microns.

14 . The composition of claim 1 , wherein the composition has a particle size from about 300 microns to about 850 microns.

15 . The composition of claim 1 , wherein the resulting sweetening composition has a white color with a sparkling sheen.

16 . The composition of claim 1 , wherein the resulting sweetening composition has a color ranging from light brown to dark brown.

17 . The composition of claim 1 , wherein the resulting sweetening composition has a natural taste.

18 . The composition of claim 1 , wherein the resulting sweetening composition has an improved stability.

19 . The composition of claim 1 , wherein the resulting sweetening composition is a 1:1 volume replacement for sugar.

20 . A method of making a sweetening composition comprising the steps of:

(a) combining a high intensity sweetener, a carrier/substrate, and water, thus forming a mixture or solution;

(b) heating the mixture or solution; and

(c) cooling the mixture, thereby forming co-crystals.

21 . The method of claim 20 , further comprising a drying step in combination with or after the cooling step.

22 . The method of claim 20 , further comprising a resting step in combination with or after the cooling step.

23 . The method of claim 20 , wherein the high intensity sweetener is selected from the group consisting of aspartame, acesulfame, alitame, brazzein, cyclamic acid, dihydrochalcones, extract of Dioscorophyllum cumminsii , extract of the fruit of Pentadiplandra brazzeana , glycyrrhizin, hernandulcin, monatin, monellin, mogroside, neotame, neohesperidin, saccharin, sucralose, stevia extracts, luo han guo, agave, Thaumatin katemfe fruit ( Thaumatococcus daniellii ), Hernandulcin-lippia duclis, and combinations thereof.

24 . The method of claim 20 , wherein the carrier/substrate is selected from the group consisting of a monosaccharide, a disaccharide, a polysaccharide, a sugar alcohol, a low-intensity sweetener and mixtures thereof.

25 . The method of claim 20 , wherein the carrier/substrate is glucose, fructose, galactose, xylose, ribose, sucrose, lactulose, lactose, maltose, trehalose, cellobiose, kojibiose, nigerose, isomaltose, β,β-trehalose, α,β-trehalose, sophorose, laminaribiose, gentiobiose, turanose, maltulose, palatinose, gentiobiulose, mannobiose, melibiose, melibiulose, rutinose, rutinulose, xylobiose, erythritol, glycol, glycerol, threitol, arabitol, xylitol, ribitol, mannitol, sorbitol, dulcitol, iditol, isomalt, maltitol, lactitol, polyglycitol, maltodextrin and mixtures thereof.

26 . The method of claim 20 , wherein the high intensity sweetener, carrier/substrate is heated to a temperature of about 40° C. to about 110° C.

27 . The method of claim 20 , wherein the high intensity sweetener, carrier/substrate is heated to a temperature of about 60° C. to about 100° C.

28 . The method of claim 20 , wherein the high intensity sweetener, carrier/substrate is heated to a temperature of about 90° C.

29 . A method of making a sweetening composition comprising the steps of:

(a) combining a high intensity sweetener, a carrier/substrate, and water, thus forming a mixture or solution;

(b) mixing the mixture or solution; and

(c) cooling the mixture, thereby forming co-crystals.

30 . The method of claim 29 , further comprising a drying step in combination with or after the cooling step.

31 . The method of claim 29 , further comprising a resting step in combination with or after the cooling step.

32 . The method of claim 29 , wherein the high intensity sweetener is selected from the group consisting of aspartame, acesulfame, alitame, brazzein, cyclamic acid, dihydrochalcones, extract of Dioscorophyllum cumminsii, extract of the fruit of Pentadiplandra brazzeana , glycyrrhizin, hernandulcin, monatin, monellin, mogroside, neotame, neohesperidin, saccharin, sucralose, stevia extracts, luo han guo, agave, Thaumatin katemfe fruit ( Thaumatococcus daniellii ), Hernandulcin-lippia duclis, and combinations thereof.

33 . The method of claim 29 , wherein the carrier/substrate is selected from the group consisting of a monosaccharide, a disaccharide, a polysaccharide, a sugar alcohol, a low-intensity sweetener and mixtures thereof.

34 . The method of claim 29 , wherein the carrier/substrate is glucose, fructose, galactose, xylose, ribose, sucrose, lactulose, lactose, maltose, trehalose, cellobiose, kojibiose, nigerose, isomaltose, β,β-trehalose, α,β-trehalose, sophorose, laminaribiose, gentiobiose, turanose, maltulose, palatinose, gentiobiulose, mannobiose, melibiose, melibiulose, rutinose, rutinulose, xylobiose, erythritol, glycol, glycerol, threitol, arabitol, xylitol, ribitol, mannitol, sorbitol, dulcitol, iditol, isomalt, maltitol, lactitol, polyglycitol, maltodextrin and mixtures thereof.

35 . The method of claim 29 , wherein the high intensity sweetener, carrier/substrate and water are heated to a temperature of about 40° C. to about 110° C.

36 . The method of claim 29 , wherein the high intensity sweetener, carrier/substrate and water are heated to a temperature of about 60° C. to about 100° C.

37 . The method of claim 29 , wherein the high intensity sweetener, carrier/substrate and water are heated to a temperature of about 90° C.

Assignments (6)
RELEASE OF SECURITY INTEREST Recorded May 3, 2021
From: COOPERATIEVE RABOBANK U.A.
To: HEARTLAND CONSUMER PRODUCTS LLC; TC HEARTLAND LLC
Reel/Frame 056113/0471 →
RELEASE OF SECURITY INTEREST Recorded May 3, 2021
From: COOPERATIEVE RABOBANK U.A.
To: HEARTLAND CONSUMER PRODUCTS LLC; TC HEARTLAND LLC
Reel/Frame 056116/0001 →
SECURITY INTEREST Recorded Dec 7, 2018
From: HEARTLAND CONSUMER PRODUCTS LLC; TC HEARTLAND LLC
To: COOPERATIEVE RABOBANK U.A., NEW YORK BRANCH, AS ADMINISTRATIVE AGENT
Reel/Frame 047712/0601 →
SECURITY INTEREST Recorded Nov 2, 2015
From: TC HEARTLAND LLC; HEARTLAND CONSUMER PRODUCTS LLC
To: COOPERATIEVE CENTRALE RAIFFEISEN-BOERENLEENBANK B.A., "RABOBANK NEDERLAND", NEW YORK BRANCH, AS ADMINISTRATIVE AGENT
Reel/Frame 037020/0929 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 29, 2015
From: MCNEIL NUTRITIONALS, LLC
To: HEARTLAND CONSUMER PRODUCTS LLC
Reel/Frame 036912/0615 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 23, 2013
From: LIAO, SHYHYUAN; PANARISI, JR., JOSEPH R.
To: MCNEIL NUTRITIONALS, LLC.
Reel/Frame 031070/0515 →