IP Library Granted Patent US 10,514,372
Granted Patent B2
US 10,514,372 · App. 13/972,772 · Granted Dec 24, 2019

Digital rock analysis systems and methods that reliably predict a porosity-permeability trend

Inventors: Giuseppe De Prisco (Houston, TX); Jonas Toelke (Houston, TX)
Assignee: Halliburton Energy Services, Inc.
G01N33/24G01N15/08
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Quick Facts
Patent No.
US 10,514,372
App. No.
13/972,772
Granted
Dec 24, 2019
Kind
B2
Abstract

The pore structure of rocks and other materials can be determined through microscopy and subjected to digital simulation to determine the properties of fluid flows through the material. To determine a porosity-permeability over an extended range even when working from a small model, some disclosed method embodiments obtain a three-dimensional pore/matrix model of a sample; measure a distribution of porosity-related parameter variation as a function of subvolume size; measure a connectivity-related parameter as a function of subvolume size; derive a reachable porosity range as a function of subvolume size based at least in part on the distribution of porosity-related parameter variation and the connectivity-related parameter; select a subvolume size offering a maximum reachable porosity range; find permeability values associated with the maximum reachable porosity range; and display said permeability values as a function of porosity.

Claims (41)

1. A method that comprises:

scanning a sample using an electron microscope to obtain an image of the sample;

processing the image to derive a three-dimensional pore/matrix model;

measuring, by a processor, a distribution of porosity-related parameter variation for the pore/matrix model as a function of subvolume size;

measuring, by the processor, a pore connectivity-related parameter for the pore/matrix model as a function of subvolume size;

determining, by a processor, a reachable porosity for subvolumes in the model where the distribution of porosity-related parameter variation of the subvolumes is below a variation threshold and the pore connectivity-related parameter of the subvolumes is below a connectivity threshold;

adjusting, by the processor, either or both of the variation threshold or the connectivity threshold to determine the subvolumes offering a maximum reachable porosity;

determining, by the processor, porosity and permeability values associated with the determined subvolumes; and

displaying said permeability values as a function of porosity.

2. The method of claim 1 , further comprising determining an integral scale based at least in part on said distribution of porosity-related parameter variation as a function of subvolume size.

3. The method of claim 2 , further comprising determining a percolation scale based at least in part on the connectivity-related parameter as a function of subvolume size.

4. The method of claim 1 , further comprising determining, by the processor, porosities possessed by the subvolumes and selecting, by the processor, a subvolume size offering a maximum reachable porosity range from the determined porosities by determining that at least one of an integral scale or a percolation scale are to the same size as a dimension of the pore/matrix model.

5. The method of claim 1 , wherein the sample is a physical rock sample.

6. The method of claim 1 , wherein measuring the distribution of porosity-related parameter variation for the pore/matrix model as a function of the size of the subvolume further comprises wherein the porosity-related parameter variation comprises a standard deviation of porosity of slices of the subvolume and the slices are divided perpendicular to a flow direction of the subvolumes.

7. The method of claim 6 , further comprising measuring a distribution of standard deviation of pore surface to volume ratio.

8. The method of claim 1 , wherein said determining a reachable porosity for subvolumes includes:

screening out subvolumes having porosity-related parameter variation above the variation threshold;

screening out subvolumes having a connectivity-related parameter value above the connectivity threshold.

9. The method of claim 8 , wherein the variation threshold screens subvolumes having variation in an upper ⅗ths of the distribution.

10. The method of claim 8 , wherein the connectivity threshold screens subvolumes having more than 10% disconnected porosity.

11. A system for analyzing a sample, comprising:

an electron microscope operable to produce an image of the sample;

a memory having software; and

one or more processors coupled to the memory to execute the software, the software causing the one or more processors to:

derive a three-dimensional pore/matrix model from the image;

measure a distribution of porosity-related parameter variation for the pore/matrix model as a function of subvolume size;

measure a pore connectivity-related parameter for the pore/matrix model as a function of subvolume size;

determining a reachable porosity for subvolumes in the model where the distribution of porosity-related parameter variation of the subvolumes is below a variation threshold and the pore connectivity-related parameter of the subvolumes is below a connectivity threshold;

adjusting either or both of the variation threshold or the connectivity threshold to determine the subvolumes offering a maximum reachable porosity; and

determining porosity and permeability values associated with the determined subvolumes.

12. The system of claim 11 , wherein the software further causes the one or more processors to determine an integral scale based at least in part on said distribution of porosity-related parameter variation as a function of subvolume size.

13. The system of claim 12 , wherein the software further causes the one or more processors to determine a percolation scale based at least in part on the connectivity-related parameter as a function of subvolume size.

14. The system of claim 11 , further comprising determining, by the processor, porosities possessed by the subvolumes and selecting a subvolume size offering a maximum reachable porosity range from the determined porosities by determining that at least one of an integral scale or a percolation scale are the same size to a dimension of the pore/matrix model.

15. The system of claim 11 , wherein the sample is a physical rock sample.

16. The system of claim 11 , wherein the distribution of porosity-related parameter variation is a distribution of standard deviation of porosity.

17. The system of claim 16 , wherein the software further causes the one or more processors to measure a distribution of standard deviation of pore surface to volume ratio.

18. The system of claim 11 , wherein as part of said determining a reachable porosity for subvolumes, the software causes the one or more processors to:

screen out subvolumes having porosity-related parameter variation above a given variation threshold;

screen out subvolumes having a connectivity-related parameter value above a given connectivity threshold.

19. The system of claim 18 , wherein the variation threshold screens subvolumes having variation in an upper ⅗ths of the distribution.

20. The system of claim 18 , wherein the connectivity threshold screens subvolumes having more than 10% disconnected porosity.

Assignments (6)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 6, 2018
From: INGRAIN, INC.
To: HALLIBURTON ENERGY SERVICES, INC.
Reel/Frame 047024/0084 →
RELEASE OF SECURITY INTEREST Recorded Jul 5, 2017
From: COMERICA BANK
To: INGRAIN, INC.
Reel/Frame 042900/0176 →
RELEASE OF SECURITY INTEREST Recorded Jul 5, 2017
From: GEMCAP LENDING I, LLC
To: INGRAIN, INC.
Reel/Frame 043090/0263 →
SECURITY INTEREST Recorded Sep 1, 2016
From: INGRAIN, INC.
To: GEMCAP LENDING I, LLC
Reel/Frame 039973/0886 →
SECURITY INTEREST Recorded Jan 23, 2015
From: INGRAIN, INC.
To: COMERICA BANK
Reel/Frame 034797/0255 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 21, 2013
From: DE PRISCO, GIUSEPPE; TOELKE, JONAS
To: INGRAIN, INC.
Reel/Frame 031057/0159 →
Continuity (2)
Provisional Application 61692541 · Aug 23, 2012
Related Publication 20140058676A1 · Feb 27, 2014