IP Library Granted Patent US 9,153,782
Granted Patent B2
US 9,153,782 · App. 13/978,013 · Granted Oct 6, 2015

Method for producing organic light-emitting element, organic display panel, organic light-emitting device, method for forming functional layer, ink, substrate, organic light-emitting element, organic display device, and inkjet device

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Quick Facts
Patent No.
US 9,153,782
App. No.
13/978,013
Granted
Oct 6, 2015
Kind
B2
Abstract

To provide a method of efficiently manufacturing an organic light-emitting element with excellent light-emitting characteristics by application, the method includes: preparing ink and filling an inkjet device having an ink ejection nozzle with ink; preparing a substrate having a base layer including a first electrode; and positioning the inkjet device above the substrate, and causing the inkjet device to eject a drop of the ink onto the base layer, wherein, in the preparation of the ink, a value Z denoting a reciprocal of the Ohnesorge number Oh determined by density ρ (g/dm 3 ), surface tension γ (mN/m), and viscosity η (mPa·s) of the ink and a diameter r (mm) of the ink ejection nozzle satisfies Formula 1, in the ejection of the drop of the ink, speed V (m/s) of the ejected drop satisfies Formula 2, and the value Z and the speed V (m/s) satisfy Formula 3.

Claims (45)

1. A method of manufacturing an organic light-emitting element, comprising:

preparing ink including functional material as a material for a functional layer and a solvent dissolving the functional material, and filling an inkjet device having an ink ejection nozzle with the ink, the functional material having a weight-average molecular weight equal to or greater than 200,000 and equal to or less than 250,000;

preparing a substrate having a base layer including a first electrode;

positioning the inkjet device above the substrate, and causing the inkjet device to eject a drop of the ink onto the base layer of the substrate;

forming the functional layer by drying the ink ejected onto the base layer of the substrate; and

forming a second electrode above the functional layer, wherein

in the preparation of the ink, when a value Z denotes a reciprocal of the Ohnesorge number Oh determined by density ρ (g/dm 3 ), surface tension γ (mN/m), and viscosity η (mPa·s) of the ink and a diameter r (mm) of the ink ejection nozzle, the value Z is within a range of Formula 1,

in the ejection of the drop of the ink, speed V (m/s) of the ejected drop of the ink is within a range of Formula 2, and

the value Z and the speed V (m/s) satisfy Formula 3:

1≦ Z≦ 30;

where Z=1/Ohnesorge number Oh;

1/Ohnesorge number Oh =( r ·ρ·γ) 1/2 /η  (Formula 1);

3≦ V≦ 6  (Formula 2); and

V≦− 1.18Ln( Z )+7.52  (Formula 3).

2. The method of manufacturing the organic light-emitting element of claim 1 , wherein

the value Z is two or more and is ten or less, and

the speed V is 3 m/s or more and is 5 m/s or less.

3. The method of manufacturing the organic light-emitting element of claim 1 , wherein

the density ρ of the ink is 858 g/dm 3 or more and is 969 g/dm 3 or less, the surface tension γ of the ink is 28.2 mN/m or more and is 33.9 mN/m or less,

the viscosity η of the ink is 0.9 mPa·s or more and is 18.6 mPa·s or less, and

the diameter r of the ink ejection nozzle is 0.02 mm or more and is 0.03 mm or less.

4. The method of manufacturing the organic light-emitting element of claim 1 , wherein

in the preparation of the substrate, the substrate has a plurality of openings corresponding to respective pixel units and includes a plurality of banks each formed above the base layer to partition adjacent pixel units, and

in the ejection of the drop of the ink, drops of the ink are ejected onto the base layer in regions corresponding to the openings between the banks.

5. A method of forming a functional layer, comprising:

preparing ink including functional material as a material for the functional layer and a solvent dissolving the functional material, and filling an inkjet device having an ink ejection nozzle with the ink, the functional material having a weight-average molecular weight equal to or greater than 200,000 and equal to or less than 250,000;

preparing a substrate on which the functional layer is to be formed;

positioning the inkjet device above the substrate, and causing the inkjet device to eject a drop of the ink onto the substrate; and

forming the functional layer by drying the ink ejected onto the substrate; and, wherein

in the preparation of the ink, when a value Z denotes a reciprocal of the Ohnesorge number Oh determined by density ρ (g/dm 3 ), surface tension γ (mN/m), and viscosity η (mPa·s) of the ink and a diameter r (mm) of the ink ejection nozzle, the value Z is within a range of Formula 1,

in the ejection of the drop of the ink, speed V (m/s) of the ejected drop of the ink is within a range of Formula 2, and

the value Z and the speed V (m/s) satisfy Formula 3:

1≦ Z≦ 30;

where Z=1/Ohnesorge number Oh;

1/Ohnesorge number Oh =( r ·ρ·γ) 1/2 /η)  (Formula 1);

3≦ V≦ 6  (Formula 2); and

V≦− 1.18Ln( Z )+7.52  (Formula 3).

6. The method of forming the functional layer of claim 5 , wherein

the value Z is two or more and is ten or less, and

the speed V is 3 m/s or more and is 5 m/s or less.

7. The method of forming the functional layer of claim 5 , wherein

the density ρ of the ink is 858 g/dm 3 or more and is 969 g/dm 3 or less,

the surface tension γ of the ink is 28.2 mN/m or more and is 33.9 mN/m or less,

the viscosity η of the ink is 0.9 mPa·s or more and is 18.6 mPa·s or less, and

the diameter r of the ink ejection nozzle is 0.02 mm or more and is 0.03 mm or less.

Assignments (6)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 18, 2025
From: JDI DESIGN AND DEVELOPMENT G.K.
To: MAGNOLIA BLUE CORPORATION
Reel/Frame 072039/0656 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 31, 2024
From: JOLED, INC.
To: JDI DESIGN AND DEVELOPMENT G.K.
Reel/Frame 066382/0619 →
CORRECTION BY AFFIDAVIT FILED AGAINST REEL/FRAME 063396/0671 Recorded Jun 12, 2023
From: JOLED, INC.
To: JOLED, INC.
Reel/Frame 064067/0723 →
SECURITY INTEREST Recorded Apr 20, 2023
From: JOLED, INC.
To: INCJ, LTD.
Reel/Frame 063396/0671 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 12, 2015
From: PANASONIC CORPORATION
To: JOLED INC
Reel/Frame 035187/0483 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 11, 2013
From: NANNO, HIROTAKA; ISHINO, SHINICHIRO; MASUDA, TOMOKI; KAWANAMI, YUKO; MATSUSUE, NORIYUKI
To: PANASONIC CORPORATION
Reel/Frame 031178/0905 →