IP Library Granted Patent US 8,865,705
Granted Patent B2
US 8,865,705 · App. 13/993,107 · Granted Oct 21, 2014

Benzimidazole respiratory syncytial virus inhibitors

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Quick Facts
Patent No.
US 8,865,705
App. No.
13/993,107
Granted
Oct 21, 2014
Kind
B2
Abstract

Benzimidazoles having inhibitory activity on RSV replication and having the formula the prodrugs, N-oxides, addition salts, quaternary amines, metal complexes and stereochemically isomeric forms thereof, compositions containing these compounds as active ingredient and processes for preparing these compounds and compositions.

Claims (29)

1. A compound represented by formula I, a prodrug, N-oxide, addition salt, quaternary amine, metal complex, or a stereochemically isomeric form thereof;

wherein

each X independently is C or N;

R 1 is H;

R 2 is selected from the group consisting of Br and Cl;

R 3 is —(CR 6 R 7 ) n —R 8 ;

R 4 is selected from the group consisting of H, C 3 -C 7 cycloalkyl, C 2 -C 10 alkenyl, —(CR 6 R 7 ) n —R 8 ; —CH 2 -p-Fluorophenyl, CH 2 CF 3 and —SO 2 CH 3 ;

R 5 is present where X is C, whereby each R 5 is selected, each independently, from the group consisting of H, C 1 -C 6 alkyl, C 1 -C 6 alkoxy, halogen, and CN;

R 5 is absent where X is N;

R 6 and R 7 are H;

R 8 is selected from the group consisting of H, OH, CF 3 , CHF 2 , F, Cl, SO 2 CH 3 , SO 2 C 3 -C 7 cycloalkyl, NR 6 SO 2 R 6 , SO 2 NR 6 R 7 , NR 6 SO 2 C 3 -C 7 cycloalkyl, CN, NR 6 R 7 , COOH, COOR 6 , CONR 6 R 7 , OCOC 1 -C 6 alkyl, CONR 6 SO 2 R 7 , CONH—R 6 —SO 2 R 7 , CONH—R 6 —SO 2 NR 6 R 7 CONR 6 SO 2 NR 6 R 7 , phtalimido or a 5 to 6 membered aliphatic or aromatic ring that optionally contains one or more heteroatoms selected from the group N, S, O;

n is an integer having a value from 1 to 6.

2. A compound according to claim 1 wherein

R 4 is selected from the group consisting of H, C 3 -C 7 cycloalkyl, C 2 -C 10 alkenyl, and —SO 2 CH 3 ;

R 8 is selected from the group consisting of H, OH, CF 3 , CHF 2 , F, SO 2 CH 3 , SO 2 C 3 -C 7 cycloalkyl, NR 6 SO 2 R 6 , SO 2 NR 6 R 7 , NR 6 SO 2 C 3 -C 7 cycloalkyl, CN, NR 6 R 7 .

3. A compound according to claim 1 wherein R 2 is Br.

4. A compound according to claim 1 wherein R 2 is Cl.

5. A compound according to claim 1 , wherein n is 2-4.

6. A compound according to claim 1 , wherein R 8 is selected from the group consisting of F, CN, OH, CF 3 and SO 2 CH 3 .

7. A compound according to claim 1 , wherein R 8 is selected from the group consisting of F, CN, OH, and SO 2 CH 3 .

8. A compound according to claim 1 , wherein R 4 is C 3 -C 7 cycloalkyl or CH 2 CF 3 .

9. A compound according to claim 1 , wherein R 4 is cyclopropyl or CH 2 CF 3 .

10. A compound according to claim 1 , wherein one X is N and the other X's are C.

11. A compound according to claim 10 , wherein the N is in para position to N—R 4 .

12. A compound according to claim 1 , wherein at most one R 5 is selected from the group consisting of C 1 -C 6 alkyl, C 1 -C 6 alkoxy, halogen, and CN.

13. A compound according to claim 1 , wherein all R 5 are H.

14. A compound according to claim 1 , wherein R 2 is Cl; one X is N and the other X's are C, wherein the N is in para position to N—R 4 ; and R 4 is cyclopropyl or CH 2 CF 3 .

15. A pharmaceutical composition comprising a pharmaceutically acceptable carrier, and as active ingredient a therapeutically effective amount of a compound as claimed in claim 1 .

16. A process for preparing a pharmaceutical composition as claimed in claim 15 , said process comprising intimately mixing a pharmaceutically acceptable carrier with a therapeutically effective amount of compound.

Assignments (8)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 24, 2015
From: JANSSEN R & D IRELAND
To: JANSSEN SCIENCES IRELAND UC
Reel/Frame 035496/0382 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 6, 2014
From: COOYMANS, LUDWIG PAUL
To: JANSSEN PHARMACEUTICA NV
Reel/Frame 033478/0224 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 6, 2014
From: DEMIN, SAMUEL DOMINIQUE; HU, LILI; JONKERS, TIM HUGO MARIA; RABOISSON, PIERRE JEAN-MARIE BERNARD; TAHRI, ABDELLAH; VENDEVILLE, SANDRINE MARIE HELENE
To: TIBOTEC BVBA
Reel/Frame 033478/0600 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2014
From: TIBOTEC BVBA
To: TIBOTEC PHARMACEUTICALS
Reel/Frame 033465/0931 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2014
From: DEMIN, SAMUEL DOMINIQUE; HU, LILI; JONCKERS, TIM HUGO MARIA; RABOISSON, PIERRE JEAN-MARIE BERNARD; TAHRI, ABDELLAH; VENDEVILLE, SANDRINE MARIE HELENE
To: TIBOTEC BVBA
Reel/Frame 033465/0314 →
CHANGE OF NAME Recorded Aug 5, 2014
From: TIBOTEC PHARMACEUTICALS
To: JANSSEN R&D IRELAND
Reel/Frame 033466/0066 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2014
From: COOYMANS, PAUL LUDWIG
To: JANSSEN PHARMACEUTICA NV
Reel/Frame 033465/0616 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2014
From: JANSSEN PHARMACEUTICA NV
To: TIBOTEC PHARMACEUTICALS
Reel/Frame 033465/0768 →