IP Library Granted Patent US 8,927,098
Granted Patent B2
US 8,927,098 · App. 14/020,358 · Granted Jan 6, 2015

Hard coating film

Inventors: Soon-Hwa Jung (Daejeon, KR); Heon Kim (Daejeon, KR); Yeong-Rae Chang (Daejeon, KR); Hye-Min Kim (Daejeon, KR)
Assignee: LG Chem, Ltd.
C09D105/16C08B37/0012C08B37/0015C08G83/007C08G63/08C08L83/04C08G18/71C08G18/8116C09D175/04C09D175/14C09D175/16C08G18/4277C08J7/047C08J2333/12
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Quick Facts
Patent No.
US 8,927,098
App. No.
14/020,358
Granted
Jan 6, 2015
Kind
B2
Abstract

The present invention relates to a hard coating film including a hard coating layer comprising: a crosslinked product of (a) a polyrotaxane compound including a macrocycle to which a lactone-based compound is bonded, wherein a (meth)acrylate-based compound is introduced at the end of the lactone-based compound at a ratio of 40 mol % to 70 mol %, a linear molecule penetrating the macrocycle, and blocking groups arranged at both ends of the linear molecule and preventing the macrocycle from escaping; and (b) a binder resin.

Claims (33)

1. A hard coated substrate comprising a substrate and a hard coating layer a hard coating layer comprising: a crosslinked product of (a) a polyrotaxane compound comprising a macrocycle to which a lactone-based compound is bonded, wherein a (meth)acrylate-based compound is introduced at the end of the lactone-based compound at a ratio of 40 mol % to 70 mol %, a linear molecule penetrating the macrocycle, and blocking groups arranged at both ends of the linear molecule and preventing the macrocycle from escaping; and (b) a binder resin.

2. The hard coated film according to claim 1 ,

wherein a ratio of the (meth)acrylate-based compound introduced at the end of the lactone-based compound is 45 mol % to 65 mol %.

3. The hard coated film according to claim 1 ,

wherein the macrocycle includes at least one selected from the group consisting of α-cyclodextrin, β-cyclodextrin, and γ-cyclodextrin.

4. The hard coated film according to claim 1 ,

wherein the lactone-based compound is bonded to the macrocycle by a direct bond or a C1-10 linear or branched oxyalkylene group.

5. The hard coated film according to claim 1 ,

wherein a residue of the lactone-based compound includes a functional group of the following Chemical Formula 1:

wherein, in Chemical Formula 1, m is an integer of from 2 to 11, and n is an integer of from 1 to 20.

6. The hard coated film according to claim 1 ,

wherein the (meth)acrylate-based compound is bonded to the residue of the lactone-based compound through a direct bond, a urethane bond, an ether bond, a thioester bond, or an ester bond.

7. The hard coated film according to claim 1 ,

wherein the residue of the (meth)acrylate-based compound includes a functional group of the following Chemical Formula 2:

wherein, in Chemical Formula 2, R 1 is hydrogen or a methyl, and R 2 is a C1-12 linear or branched alkylene group, a C4-20 cycloalkylene group, or a C6-20 arylene group.

8. The hard coated film according to claim 1 ,

wherein the linear molecule is a polyoxyalkylene-based compound or a polylactone-based compound.

9. The hard coated film according to claim 1 ,

wherein the linear molecule has a weight average molecular weight of 1000 to 50,000.

10. The hard coated film according to claim 1 ,

wherein the blocking group includes at least one functional group selected from the group consisting of dinitrophenyl, cyclodextrin, adamantane, trityl, fluorescein, and pyrene groups.

11. The hard coated film according to claim 1 ,

wherein the polyrotaxane compound has a weight average molecular weight of 100,000 to 800,000.

12. The hard coated film according to claim 1 ,

wherein the binder resin is selected from the group consisting of a polysiloxane-based resin, a (meth)acrylate-based resin, and a urethane (meth)acrylate-based resin, a mixture thereof, and a copolymer thereof.

13. The hard coated film according to claim 1 ,

wherein the hard coating layer has pencil hardness of 5H or more under a load of 1 kg.

14. The hard coated film according to claim 1 ,

further comprising inorganic microparticles dispersed in a crosslinked product of the (a) polyrotaxane compound and the (b) binder resin.

15. The hard coated film according to claim 1 ,

wherein the hard coating layer has a thickness of 1 to 300 μm.

16. The hard coated film according to claim 1 ,

wherein the substrate is a polymer resin substrate.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 24, 2025
From: LG CHEM, LTD.
To: XINMEI FONTANA HOLDING (HONG KONG) LIMITED
Reel/Frame 070608/0517 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 23, 2025
From: LG CHEM, LTD
To: XINMEI FONTANA HOLDING (HONG KONG) LIMITED
Reel/Frame 070609/0245 →
ADDRESS CHANGE Recorded Nov 19, 2024
From: LG CHEM, LTD.
To: LG CHEM, LTD.
Reel/Frame 069389/0264 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 6, 2013
From: JUNG, SOON-HWA; KIM, HEON; CHANG, YEONG-RAE; KIM, HYE-MIN
To: LG CHEM, LTD.
Reel/Frame 031153/0679 →
Priority Claims (5)
KR 10-2012-0056284 · May 25, 2012 · national
KR 10-2012-0056285 · May 25, 2012 · national
KR 10-2012-0056286 · May 25, 2012 · national
KR 10-2012-0056287 · May 25, 2012 · national
KR 10-2013-0059517 · May 27, 2013 · national
Continuity (2)
Continuation PCTKR2013004605 · May 27, 2013
Related Publication 20140079937A1 · Mar 20, 2014