IP Library Granted Patent US 10,548,904
Granted Patent B2
US 10,548,904 · App. 14/045,311 · Granted Feb 4, 2020

Monolithic intravaginal rings comprising progesterone and methods of making and uses thereof

Inventors: Salah U. Ahmed (New City, NY); Jiaxiang Tsao (Nanuet, NY); Anu Mahashabde (Kendall Park, NJ); Diane D. Harrison (Villanova, PA)
Assignee: FERRING B.V.
A61K31/57A61F6/08A61K9/0036A61K47/34A61K47/44B29C45/0001B29C45/7207B29K2083/00B29K2105/0035B29L2031/753
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Quick Facts
Patent No.
US 10,548,904
App. No.
14/045,311
Granted
Feb 4, 2020
Kind
B2
Abstract

The present invention relates to monolithic intravaginal rings comprising progesterone, methods of making, and uses thereof. The intravaginal rings comprise progesterone, a polysiloxane elastomer, and a pharmaceutically acceptable hydrocarbon or glycerol esters of a fatty acid.

Claims (26)

1. A method for supplementation or replacement of corpus luteal function, the method comprising administering progesterone to a subject by a monolithic intravaginal ring comprising a polysiloxane elastomer and a pharmaceutically acceptable hydrocarbon or glycerol ester of a fatty acid, or a polysiloxane elastomer and a pharmaceutically acceptable oil, in amounts that are effective to maintain a serum progesterone level of about 6 ng/mL to about 10 ng/mL over a 7-day period of use after administration to the subject;

wherein the polysiloxane elastomer is present in an amount of about 55% to about 90% by total weight of the ring;

wherein the pharmaceutically acceptable hydrocarbon or glycerol ester of a fatty acid or the pharmaceutically acceptable oil is present in an amount of about 1% to about 10% by total weight of the ring;

wherein the progesterone is present in an amount of about 15% to about 30% by total weight of the ring.

2. The method of claim 1 , wherein the polysiloxane elastomer is dimethylpolysiloxane elastomer.

3. The method of claim 1 , wherein the polysiloxane elastomer is a dimethylpolysiloxane elastomer, and wherein the ratio by weight of progesterone to elastomer is about 1:1 to about 1:10, the progesterone is homogeneously dispersed in the elastomer, and the ratio of progesterone to hydrocarbon or glycerol esters of a fatty acid is about 1:0.1 to about 1:100.

4. The method of claim 2 , wherein the intravaginal ring comprises:

(a) about 15% to about 25% by weight of the progesterone;

(b) about 70% to about 80% by weight of the dimethylpolysiloxane elastomer; and

(c) about 1% to about 10% by weight of the pharmaceutically acceptable hydrocarbon or glycerol esters of a fatty acid or the pharmaceutically acceptable oil,

wherein the progesterone is homogeneously dispersed in the elastomer.

5. The method of claim 1 , wherein the intravaginal ring releases progesterone at a steady rate over a 7-day period of use.

6. The method of claim 1 , wherein the intravaginal ring releases about 11 mg to about 15 mg progesterone per day at a steady state rate over a 7-day period of use.

7. The method of claim 1 , wherein the pharmaceutically acceptable oil is mineral oil.

8. The method of claim 1 , wherein the intravaginal ring comprises the progesterone, the dimethylpolysiloxane elastomer, and the pharmaceutically acceptable oil, in a ratio by weight of about 4:15:1, respectively, wherein the progesterone is homogeneously dispersed in the elastomer.

9. A method for treating a luteal phase defect or supporting embryo implantation and early pregnancy in a patient in need thereof, the method comprising administering progesterone to a vaginal and/or urogenital tract of a subject, in amounts that are effective to maintain a serum progesterone level of about 6 ng/mL to about 10 ng/mL over a 7-day period of use, wherein said progesterone is administered by a monolithic intravaginal ring comprising a polysiloxane elastomer and a pharmaceutically acceptable hydrocarbon or glycerol ester of a fatty acid or a polysiloxane elastomer and a pharmaceutically acceptable oil, wherein:

the polysiloxane elastomer is present in an amount of about 55% to about 90% by total weight of the ring;

the pharmaceutically acceptable hydrocarbon or glycerol ester of a fatty acid or the pharmaceutically acceptable oil is present in an amount of about 1% to about 10% by total weight of the ring; and

the progesterone is present in an amount of about 15% to about 30% by total weight of the ring.

10. The method according to claim 1 , said method further comprising replacing the monolithic intravaginal ring about 7 days after administration to the subject.

11. The method according to claim 1 , wherein the subject is a woman with progesterone deficiency.

12. The method of claim 2 , wherein the intravaginal ring consists of:

(a) about 15% to about 25% by weight of the progesterone;

(b) about 70% to about 80% by weight of the dimethylpolysiloxane elastomer; and

(c) about 1% to about 10% by weight of the pharmaceutically acceptable hydrocarbon or glycerol esters of a fatty acid or the pharmaceutically acceptable oil,

wherein the progesterone is homogeneously dispersed in the elastomer.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 8, 2016
From: FERRING INTERNATIONAL CENTER S.A.
To: FERRING B.V.
Reel/Frame 037925/0316 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE'S NAME PREVIOUSLY RECORDED ON REEL 037051 FRAME 0471. ASSIGNOR(S) HEREBY CONFIRMS THE TO DELETE [FERRING B.V] AND INSERT FERRING INTERNATIONAL CENTER S.A. Recorded Mar 4, 2016
From: TEVA WOMEN'S HEALTH, INC.
To: FERRING INTERNATIONAL CENTER S.A.
Reel/Frame 038002/0842 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 16, 2015
From: TEVA WOMEN'S HEALTH, INC.
To: FERRING B.V.
Reel/Frame 037051/0471 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 4, 2013
From: AHMED, SALAH U.; TSAO, JIAXIANG; MAHASHABDE, ANU; HARRISON, DIANE D.
To: DURAMED PHARMACEUTICALS, INC.
Reel/Frame 031717/0440 →
CHANGE OF NAME Recorded Dec 4, 2013
From: DURAMED PHARMACEUTICALS, INC.
To: TEVA WOMEN'S HEALTH, INC.
Reel/Frame 031765/0383 →