IP Library Granted Patent US 9,410,076
Granted Patent B2
US 9,410,076 · App. 14/065,701 · Granted Aug 9, 2016

Wellbore servicing methods and compositions comprising degradable polymers

Inventors: B. Raghava Reddy (The Woodlands, TX); Janette Cortez (Kingwood, TX); James William Ogle (Spring, TX)
Assignee: Halliburton Energy Services, Inc.
C09K8/74C09K8/035
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Quick Facts
Patent No.
US 9,410,076
App. No.
14/065,701
Granted
Aug 9, 2016
Kind
B2
Abstract

A method of servicing a wellbore comprising providing a degradable polymer and a delayed action construct within a portion of a wellbore, a subterranean formation or both; wherein the delayed action construct comprises (i) a degradation accelerator comprising an alkanolamine, an oligomer of aziridine, a polymer of azridine, a diamine, or combinations thereof, (ii) a solid support, and (iii) an encapsulating material; and placing the wellbore servicing fluid comprising the degradable polymer and delayed action construct into the wellbore, the subterranean formation or both.

Claims (24)

1. A method of servicing a wellbore comprising:

providing a first component comprising a degradable polymer and a second component

comprising a delayed action construct within a portion of a wellbore, a subterranean formation or both;

wherein the delayed action construct comprises (i) a degradation accelerator comprising an oligomer of aziridine (ii) a solid support, and (iii) an encapsulating material; and

placing the wellbore servicing fluid comprising the degradable polymer and delayed action construct into the wellbore, the subterranean formation or both.

2. The method of claim 1 wherein the oligomer of aziridine is selected from the group consisting of: a linear aziridine oligomer, a branched aziridine oligomer, any derivatives thereof, and any combination thereof.

3. The method of claim 1 wherein the oligomer of aziridine comprises a compound characterized by Formula II:

where n may range from about 2 to about 100 and R 3 comprises a primary amine.

4. The method of claim 1 wherein the oligomer of aziridine comprises a compound characterized by Formula III:

where m ranges from about 2 to about 100 and R 4 comprises a methyl group.

5. The method of claim 1 wherein the oligomer of aziridine comprises a compound characterized by Formula IV:

where the repeating units occur in a total amount of about (x+y) wherein the total value of (x+y) ranges from about 2 to about 50.

6. The method of claim 1 wherein the degradation accelerator is present in the well bore servicing fluid in an amount of from about 0.1 wt. % to about 50 wt. % based on the total weight of the wellbore servicing fluid.

7. The method of claim 1 wherein the degradable polymer comprises a polymer selected from the group consisting of: a poly(lactide).

8. The method of claim 1 wherein the solid support comprises a particulate porous material.

9. The method of claim 8 wherein the particulate porous material is selected from the group consisting of: diatomaceous earth, silica, alumina, a metal salt of an alumino-silicate, a clay, hydrotalcite, a styrenedivinylbenzene-based material, a cross-linked polyalkylacrylate ester, a cross-linked modified starch, and any combination thereof.

10. The method of claim 1 wherein the encapsulating material is selected from the group consisting of: a crosslinked polyurethane.

11. The method of claim 1 wherein the degradation accelerator is spray coated onto the solid support.

12. A method of servicing a wellbore comprising:

providing a degradable polymer and a delayed action construct within a portion of a wellbore, a subterranean formation or both;

wherein the delayed action construct comprises (i) a degradation accelerator comprises an oligomer of aziridine, (ii) a solid support, and (iii) an encapsulating material;

wherein the oligomer of aziridine comprises a compound characterized by Formula VI:

where m ranges from about 2 to 100 and R 4 comprises a methyl group; and

placing the wellbore servicing fluid comprising the degradable polymer and delayed action construct into the wellbore, the subterranean formation or both.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 29, 2013
From: REDDY, B. RAGHAVA; CORTEZ, JANETTE; OGLE, JAMES WILLIAM
To: HALLIBURTON ENERGY SERVICES, INC.
Reel/Frame 031500/0136 →
Continuity (2)
Continuation In Part 13660740 · Oct 25, 2012
Related Publication 20140116704A1 · May 1, 2014