IP Library Granted Patent US 9,701,876
Granted Patent B2
US 9,701,876 · App. 14/069,653 · Granted Jul 11, 2017

Reactive roofing adhesive

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Quick Facts
Patent No.
US 9,701,876
App. No.
14/069,653
Granted
Jul 11, 2017
Kind
B2
Abstract

A two-part adhesive includes an A side, a B side, at least one of a polyurethane prepolymer and a diisocyanate, at least one polyol, at least one catalyst, and at least one chain extender. The two-part adhesive may include an adhesion promoter.

Claims (26)

1. A two-part adhesive having an A side and a B side, the two-part adhesive comprising:

at least one of a polyurethane prepolymer and a diisocyanate present in the A side;

not more than two polyols present in the B side, wherein the weight ratio of the two polyols is at least 4:1;

at least one catalyst present in the B side;

a blowing agent present in an amount of less than 1 wt % of the B side; at least on adhesion promoter in at least one of the A side or the B side in an amount of about 10% to 50% by weight of the two-part adhesive and

wherein the A side and the B side of the two part adhesive are mixed in a volumetric ratio of 1:1 and the two part adhesive has a heat aged T-peel breakaway strength of at least about 1 pli.

2. The two-part adhesive of claim 1 , wherein

the at least one of a polyurethane prepolymer and a diisocyanate is present in the A side in an amount of 100% by weight of the A side composition;

a first polyol of the two polyols present in the B side in an amount from about 75% to about 89.73% by weight of the B side composition;

a second polyol of the two polyols is present in the B side in an amount from about 4% to about 19%;

the at least one catalyst is present in the B side in an amount from about 0.5% to about 5% by weight of the B side composition; and

the blowing agent is present in in an amount of 0.25% by weight of the two-part adhesive.

3. The two-part adhesive of claim 1 further comprising at least one adhesion promoter in at least one of the A side and the B side.

4. The two-part adhesive of claim 1 wherein the at least one of a polyurethane prepolymer and a diisocyanate is a prepolymer.

5. The two-part adhesive of claim 1 wherein the two polyols includes at least one of a multifunctional polyether polyol and a polyester polyol.

6. The two-part adhesive of claim 1 wherein the two polyols includes at least one of a polyether diol and a polyester diol.

7. The two-part adhesive of claim 1 wherein the at least one catalyst is a diazole.

8. The two-part adhesive of claim 1 wherein the at least one catalyst is an imidazole.

9. The two-part adhesive of claim 1 wherein the at least one catalyst is a 1-methylimidazole.

10. The two-part adhesive of claim 1 wherein the at least one catalyst is 2,2-dimorphorlinodiethylether.

11. The two-part adhesive of claim 1 wherein the at least one catalyst is a quaternary ammonium salt.

12. The two-part adhesive of claim 1 wherein the B side composition and the A side composition are pumpable.

13. The two-part adhesive of claim 1 wherein the B side composition and the A side composition are sprayable.

14. The two-part adhesive of claim 1 wherein the two-part adhesive has an application range from about 0° F. to about 190° F.

15. The two-part adhesive of claim 1 wherein the two-part adhesive composition has a balance of cure speed, adhesion strength, and tack.

16. The two part adhesive of claim 3 wherein the at least one adhesion promoter is selected from the group consisting of chlorinated paraffins and chlorinated polyolefins.

Assignments (9)
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS (TERM LOAN) Recorded Feb 15, 2023
From: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
To: H.B. FULLER COMPANY; H.B. FULLER CONSTRUCTION PRODUCTS INC.; ROYAL ADHESIVES AND SEALANTS, LLC; ADCO PRODUCTS, LLC
Reel/Frame 062761/0884 →
RCF SECURITY AGREEMENT Recorded Oct 25, 2017
From: H.B. FULLER COMPANY; H.B. FULLER CONSTRUCTION PRODUCTS INC.; ROYAL ADHESIVES AND SEALANTS, LLC; ADCO PRODUCTS, LLC
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 044616/0700 →
TERM LOAN SECURITY AGREEMENT Recorded Oct 25, 2017
From: H.B. FULLER COMPANY; H.B. FULLER CONSTRUCTION PRODUCTS INC.; ROYAL ADHESIVES AND SEALANTS, LLC; ADCO PRODUCTS, LLC
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 044616/0671 →
RELEASE OF SECURITY INTEREST IN PATENT COLLATERAL AT REEL/FRAME NO. 36018/0518 (FIRST LIEN) Recorded Oct 20, 2017
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
To: ADCO PRODUCTS, LLC
Reel/Frame 044568/0878 →
RELEASE OF SECURITY INTEREST IN PATENT COLLATERAL AT REEL/FRAME NO. 036018/0710 (SECOND LIEN) Recorded Oct 20, 2017
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
To: ADCO PRODUCTS, LLC
Reel/Frame 044570/0064 →
FIRST LIEN PATENT SECURITY AGREEMENT Recorded Jun 24, 2015
From: ADCO PRODUCTS, LLC
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
Reel/Frame 036018/0518 →
SECOND LIEN PATENT SECURITY AGREEMENT Recorded Jun 24, 2015
From: ADCO PRODUCTS, LLC
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
Reel/Frame 036018/0710 →
CONVERSION Recorded Oct 21, 2014
From: ADCO PRODUCTS, INC.
To: ADCO PRODUCTS, LLC
Reel/Frame 034029/0660 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 8, 2014
From: MILLER, JOHN WILLIAM; SNOWWHITE, PAUL
To: ADCO PRODUCTS, INC.
Reel/Frame 031914/0116 →