IP Library Granted Patent US 9,399,309
Granted Patent B2
US 9,399,309 · App. 14/070,061 · Granted Jul 26, 2016

Methods for threading sinterable materials and related apparatus and systems

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Quick Facts
Patent No.
US 9,399,309
App. No.
14/070,061
Granted
Jul 26, 2016
Kind
B2
Abstract

Methods for threading ceramic materials, such as ceramic materials used for spinal implants or other biomedical implants. In some implementations, an expected rate of shrinkage of the block upon undergoing a firing process may be determined. A scaling factor may then be applied using the expected rate of shrinkage to select a tap having a size larger than a desired thread size. A green block may then be tapped with the selected tap to form a threaded opening in the green block. The block may be machined in order to remove cracks caused by the tapping process and/or to form the block into a desired shape/size. The green block may then be fired, which may result in a reduction of a size of the block and a size of the threaded opening.

Claims (60)

1. A method for threading a ceramic material, the method comprising the steps of:

inserting a ceramic powder into a mold;

compressing the ceramic powder into a block;

determining an expected rate of shrinkage of the block upon undergoing a firing process;

applying a scaling factor using the expected rate of shrinkage to select a tap having a size larger than a desired thread size;

tapping the block with the selected tap to form a threaded opening in the block;

machining the block by removing material from the block comprising cracks formed during the step of tapping the block, wherein the step of machining the block comprises:

identifying a thickness of a layer of material in at least one surface of the block comprising at least substantially all of the cracks formed during the step of tapping the block; and

removing the layer of material having the thickness so as to remove at least substantially all of the cracks formed during the step of tapping the block; and

firing the block, wherein the firing reduces a size of the block and reduces a size of the threaded opening, wherein the step of machining the block is performed before the step of firing the block, and wherein the step of tapping the block is performed before the step of firing the block.

2. The method of claim 1 , wherein the step of identifying a thickness comprises identifying a thickness of a layer of material in at least one surface of the block comprising all of the cracks formed during the step of tapping the block; and wherein the step of removing the layer comprises removing the layer of material having the thickness so as to remove all of the cracks formed during the step of tapping the block.

3. The method of claim 1 , wherein the ceramic powder comprises a silicon nitride ceramic powder.

4. The method of claim 1 , wherein the step of compressing the ceramic powder into a block comprises using a cold isostatic pressing process to compress the ceramic powder into the block.

5. The method of claim 1 , wherein the block comprises a spinal implant.

6. The method of claim 5 , wherein the step of tapping the block comprises tapping the block such that the threaded opening extends to a hollow interior of the spinal implant.

7. The method of claim 6 , further comprising removing material adjacent to the threaded opening within the hollow interior prior to the step of firing the block.

8. A method for manufacturing a spinal implant, the method comprising the steps of:

selecting a mold having a sufficient size larger than a desired size of a spinal implant so as to account for an expected shrink rate and further to account for an expected layer of cracking during a subsequent tapping process;

inserting a silicon nitride ceramic powder into the selected mold;

compressing the silicon nitride ceramic powder into a spinal implant block;

determining an expected shrink rate of the spinal implant block upon undergoing a firing process;

applying a scaling factor using the expected rate of shrinkage to select a tap having a size larger than a desired thread size, wherein the scaling factor is selected such that the selected tap has a size that is between about 19% and about 20% larger than the desired thread size;

tapping the spinal implant block with the selected tap to form a threaded opening in the spinal implant block, whereby cracks are formed in the spinal implant block from the tapping process;

identifying a thickness of a layer of material in at least one surface of the spinal implant block in which at least substantially all of the cracks formed during the step of tapping the spinal implant block are present;

removing the layer of material having the thickness so as to remove at least substantially all of the cracks formed during the step of tapping the spinal implant block; and

firing the spinal implant block after the step of removing the layer of material and after the step of tapping the spinal implant block, wherein the firing reduces a size of the spinal implant block and reduces a size of the threaded opening.

9. The method of claim 8 , wherein the step of identifying a thickness comprises identifying a thickness of a layer of material in at least one surface of the spinal implant block in which all of the cracks formed during the step of tapping the spinal implant block are present, and wherein the step of removing the layer comprises removing the layer of material having the thickness so as to remove all of the cracks formed during the step of tapping the spinal implant block.

10. A method for threading a sinterable material, the method comprising the steps of:

inserting a powder into a mold;

forming the powder into a green block;

determining an expected rate of shrinkage of the green block upon undergoing a firing process;

applying a scaling factor using the expected rate of shrinkage to select a tap having a size larger than a desired size of a threaded opening in the green block after firing;

tapping the green block with the selected tap to form a threaded opening in the green block;

identifying a thickness of a layer of material in at least one surface of the green block, the layer comprising at least substantially all cracks formed during the step of tapping the green block;

removing the layer of material having the thickness so as to remove at least substantially all of the cracks formed during the step of tapping the green block; and

firing the green block to form a finished block.

11. The method of claim 10 , wherein the step of forming the powder into a green block comprises:

forming a slurry comprising the powder; and

compressing the slurry into the green block.

12. The method of claim 11 , wherein the step of removing the layer of material comprises removing a layer of material having a thickness of about 1.0 mm to about 2.0 mm from the green block.

13. The method of claim 10 , further comprising machining the green block.

14. The method of claim 13 , wherein the step of identifying a thickness comprises identifying a thickness of a layer of material in at least one surface of the green block, the layer comprising all cracks formed during the step of tapping the green block, and wherein the step of removing the layer comprises removing the layer of material having the thickness so as to remove all of the cracks formed during the step of tapping the green block.

15. The method of claim 10 , further comprising machining the finished block.

16. The method of claim 10 , wherein the powder comprises a silicon nitride ceramic powder.

17. The method of claim 10 , wherein the finished block comprises a spinal implant.

18. The method of claim 17 , wherein the step of tapping the green block comprises tapping the green block such that the threaded opening extends to a hollow interior of the spinal implant.

19. The method of claim 18 , further comprising removing material adjacent to the threaded opening within the hollow interior prior to the step of firing the green block.

20. A method for threading a ceramic material, the method comprising the steps of:

inserting a ceramic powder into a mold;

compressing the ceramic powder into a block comprising a spinal implant;

determining an expected rate of shrinkage of the block upon undergoing a firing process;

applying a scaling factor using the expected rate of shrinkage to select a tap having a size larger than a desired thread size;

tapping the block with the selected tap to form a threaded opening in the block such that the threaded opening extends to a hollow interior of the spinal implant;

machining the block by removing material from the block comprising cracks formed during the step of tapping the block;

firing the block, wherein the firing reduces a size of the block and reduces a size of the threaded opening, and wherein the step of tapping the block is performed before the step of firing the block; and

removing material adjacent to the threaded opening within the hollow interior prior to the step of firing the block.

21. The method of claim 20 , wherein the step of machining the block comprises:

identifying a thickness of a layer of material in at least one surface of the block comprising at least substantially all of the cracks formed during the step of tapping the block; and

removing the layer of material having the thickness so as to remove at least substantially all of the cracks formed during the step of tapping the block.

22. The method of claim 20 , wherein the step of machining the block is performed before the step of firing the block.

Assignments (2)
CHANGE OF NAME Recorded May 16, 2019
From: AMEDICA CORPORATION
To: SINTX TECHNOLOGIES, INC.
Reel/Frame 050133/0014 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 4, 2014
From: MCENTIRE, BRIAN J.; THIRUGNANASAMBANDAM, PRABHAKAR
To: AMEDICA CORPORATION
Reel/Frame 032137/0071 →