IP Library Granted Patent US 9,921,154
Granted Patent B2
US 9,921,154 · App. 14/099,750 · Granted Mar 20, 2018

Multiplexed digital assays

Inventors: Yann Jouvenot (Benicia, CA); Serge Saxonov (Oakland, CA); Simant Dube (Kirkland, WA); John Frederick Regan (San Mateo, CA)
Assignee: Bio-Rad Laboratories, Inc.
G01N21/64G06F19/12G06F19/18
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Quick Facts
Patent No.
US 9,921,154
App. No.
14/099,750
Granted
Mar 20, 2018
Kind
B2
Abstract

System, including methods and apparatus, for performing a multiplexed digital assay.

Claims (47)

1. A method of performing a multiplexed digital assay, the method comprising:

forming partitions that collectively contain R targets;

amplifying the R targets in the partitions;

collecting data representing amplification of each of the R targets in the partitions, all of the data being collected in fewer than R optical channels; and

determining a respective level of each of the R targets from the data, wherein each level is specific for a single target of the R targets, and wherein the level determined for at least one of the R targets is based in part on a partition count for a partition population positive for two of the R targets;

wherein the step of determining is based on at least R+2 identified partition populations.

2. The method of claim 1 , wherein R is at least three.

3. The method of claim 1 , wherein the data is collected in only two optical channels.

4. The method of claim 1 , wherein each optical channel represents a different waveband of emitted light.

5. The method of claim 1 , wherein each optical channel represents a different waveband of excitation light.

6. The method of claim 1 , wherein a different plurality of the partitions contains each different pair of the R targets.

7. The method of claim 1 , wherein at least 10% of the partitions contain a pair of the R targets.

8. The method of claim 1 , further comprising a step of identifying from the data a plurality of partition populations each positive for a different combination of the R targets.

9. The method of claim 1 , wherein the step of determining is based on at least 2R identified partition populations.

10. The method of claim 8 , wherein the step of identifying includes a step of resolving each partition population that is positive for exactly two of the R targets from each partition population that is positive for only one of the R targets.

11. A method of performing a multiplexed digital assay, the method comprising:

forming partitions that collectively contain R targets;

amplifying the R targets in the partitions;

collecting data representing amplification of each of the R targets in the partitions, all of the data being collected in fewer than R optical channels;

identifying from the data a plurality of partition populations each positive for a different combination of the R targets, wherein the step of identifying includes a step of resolving each partition population that is positive for exactly two of the R targets from each partition population that is positive for only one of the R targets; and

determining a respective level of each of the R targets from the data, wherein each level is specific for a single target of the R targets, and wherein the level determined for at least one of the R targets is based in part on a partition count for a partition population positive for two of the R targets.

12. The method of claim 11 , wherein R is at least three.

13. The method of claim 11 , wherein the data is collected in only two optical channels.

14. The method of claim 11 , wherein each optical channel represents a different waveband of emitted light.

15. The method of claim 11 , wherein a different plurality of the partitions contains each different pair of the R targets.

16. The method of claim 11 , wherein at least 10% of the partitions contain a pair of the R targets.

17. The method of claim 11 , wherein the step of determining is based on at least 2R identified partition populations.

18. A method of performing a multiplexed digital assay, the method comprising:

forming partitions that collectively contain R targets;

amplifying the R targets in the partitions;

collecting data representing amplification of each of the R targets in the partitions, all of the data being collected in fewer than R optical channels, wherein each optical channel represents a different waveband of excitation light; and

determining a respective level of each of the R targets from the data, wherein each level is specific for a single target of the R targets, and wherein the level determined for at least one of the R targets is based in part on a partition count for a partition population positive for two of the R targets.

19. A method of performing a multiplexed digital assay, the method comprising:

forming partitions that collectively contain R targets;

amplifying the R targets in the partitions;

collecting data representing amplification of each of the R targets in the partitions, all of the data being collected in fewer than R optical channels;

plotting the data such that partition populations containing different combinations of the R targets form a rectangular array, wherein the step of plotting is performed with respect to a pair of orthogonal axes, and wherein each partition population that is positive for only one of the R targets is arranged along a line that is at least generally parallel to one of the axes; and

determining a respective level of each of the R targets from the data, wherein each level is specific for a single target of the R targets, and wherein the level determined for at least one of the R targets is based in part on a partition count for a partition population positive for two of the R targets.

20. The method of claim 19 , wherein R is at least three.

21. The method of claim 19 , wherein the data is collected in only two optical channels.

22. The method of claim 19 , wherein each optical channel represents a different waveband of emitted light.

23. The method of claim 19 , wherein a different plurality of the partitions contains each different pair of the R targets.

24. The method of claim 19 , wherein at least 10% of the partitions contain a pair of the R targets.

25. The method of claim 19 , further comprising a step of identifying from the data a plurality of partition populations each positive for a different combination of the R targets.

26. The method of claim 25 , wherein the step of identifying includes a step of resolving each partition population that is positive for exactly two of the R targets from each partition population that is positive for only one of the R targets.

27. The method of claim 19 , wherein the step of determining is based on at least 2R identified partition populations.

28. The method of claim 19 , wherein the array is composed of a plurality of rows and columns, with each row and each column including at least two of the partition populations.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 2, 2018
From: JOUVENOT, YANN; SAXONOV, SERGE; REGAN, JOHN FREDERICK
To: BIO-RAD LABORATORIES, INC.
Reel/Frame 044824/0102 →
Continuity (8)
Continuation In Part 13424304 · Mar 19, 2012
Continuation In Part 13548062 · Jul 12, 2012
Provisional Application 61454373 · Mar 18, 2011
Provisional Application 61507082 · Jul 12, 2011
Provisional Application 61510013 · Jul 20, 2011
Provisional Application 61734296 · Dec 6, 2012
Related Publication 20140171341A1 · Jun 19, 2014
Related Publication 20170205345A9 · Jul 20, 2017