IP Library Granted Patent US 10,094,027
Granted Patent B2
US 10,094,027 · App. 14/108,064 · Granted Oct 9, 2018

Self-cleaning substrates and methods for making the same

Inventors: Jay A. Kahn (Houston, TX); Grant Nintzel (Alpharetta, GA); Yves Biehlmann (Pfaffenheim, FR); Craig Belnap (Johns Creek, GA); Clinton Zediak (Tarentum, PA); John Keener (Freeport, PA); James Bell (Monroeville, PA); Albert L. Askin (Lower Burrell, PA); Paula L. Kolek (Tarentum, PA); Jean Ann Skiles (Gibsonia, PA)
Assignee: ARCONIC INC.
C23C28/00B05D5/08C09D5/1618C09D5/1693C23C26/00B05D1/28B05D7/56B05D2202/25
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Quick Facts
Patent No.
US 10,094,027
App. No.
14/108,064
Granted
Oct 9, 2018
Kind
B2
Abstract

A methods, apparatus and compositions for producing colored, self-cleaning substrates by roll coating are provided. The roll coated, colored, self-cleaning substrates retain the predetermined color and a predetermined gloss of the colored coating, thereby facilitating their use in architectural applications. The roll coated, colored, self-cleaning substrates may be iridescent-free.

Claims (25)

1. A method comprising:

(a) first roll coating an inorganic barrier coating liquid onto at least a portion of an initial colored sheet product, wherein the inorganic barrier coating liquid is in the form of an aqueous solution;

(i) wherein the initial colored sheet product comprise an organic layer disposed on a base material;

(ii) wherein the initial colored sheet product comprises a predetermined color and a predetermined gloss;

(b) first converting the inorganic barrier coating liquid into an inorganic barrier layer, thereby producing an intermediate product, wherein, after the first converting step, the inorganic barrier layer is located on at least a portion of the organic layer, and wherein, after the first converting step, the intermediate product retains the predetermined color and retains the predetermined gloss of the initial colored sheet product;

(c) second roll coating a self-cleaning coating liquid onto at least a portion of the inorganic barrier layer, wherein the self-cleaning coating liquid is an aqueous-based liquid consisting essentially of water, titanium dioxide particles, silica and optional surfactant, and wherein the second roll coating step comprises uniformly applying the self-cleaning coating liquid to the inorganic barrier layer; and

(d) second converting the self-cleaning coating liquid into a self-cleaning layer, thereby producing a final sheet product, wherein, after the second converting step, the self-cleaning layer is located on at least a portion of the inorganic barrier layer, and wherein, after the second converting step, the final sheet product retains the predetermined color and retains the predetermined gloss of the initial colored sheet product, and wherein the final sheet product is iridescent free.

2. The method of claim 1 , wherein the base material is steel-based.

3. The method of claim 1 , wherein the base material is aluminum-based.

4. The method of claim 1 , wherein the base material is titanium-based.

5. The method of claim 1 , wherein the base material is non-metallic based.

6. The method of claim 5 , wherein the base material comprises at least one of a plastic and a glass.

7. The method of claim 1 , wherein the base material comprises a mixture of metals and non-metallic materials.

8. The method of claim 7 , wherein the base material comprises metal sheets sandwiching a polymeric sheet.

9. The method of claim 7 , wherein the base material comprises non-metallic materials sandwiching a metal material.

10. The method of claim 1 , wherein the inorganic barrier coating liquid is in the form of an aqueous solution comprising silica.

11. The method of claim 10 , comprising:

agitating the aqueous-based self-cleaning coating liquid inside a coating reservoir; and

applying the aqueous-based self-cleaning coating liquid to the inorganic barrier layer.

12. The method of claim 11 , wherein the agitating step comprises continuous agitation.

13. The method of claim 1 , wherein the organic layer is a colored layer.

14. The method of claim 1 , wherein the organic layer comprises polymeric-based materials.

15. The method of claim 1 , wherein, after the second converting step (d), the titanium dioxide particles are uniformly dispersed throughout the self-cleaning layer.

16. The method of claim 1 , wherein the inorganic barrier layer has a thickness of from 0.1 to 1.0 microns.

17. The method of claim 1 , wherein the inorganic barrier layer has a thickness of from 0.2 to 1.0 microns.

Assignments (14)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 10, 2025
From: ARCONIC TECHNOLOGIES LLC
To: ARCONIC CORPORATION
Reel/Frame 072848/0511 →
RELEASE OF SECURITY INTEREST Recorded Aug 22, 2023
From: U.S. BANK NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
To: ARCONIC TECHNOLOGIES LLC
Reel/Frame 064661/0283 →
RELEASE OF SECURITY INTEREST Recorded Aug 22, 2023
From: DEUTSCHE BANK AG NEW YORK BRANCH
To: ARCONIC TECHNOLOGIES LLC
Reel/Frame 064661/0409 →
NOTICE OF GRANT OF SECURITY INTEREST (ABL) IN INTELLECTUAL PROPERTY Recorded Aug 18, 2023
From: ARCONIC TECHNOLOGIES LLC
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 064641/0798 →
NOTICE OF GRANT OF SECURITY INTEREST IN INTELLECTUAL PROPERTY (FIRST LIEN) Recorded Aug 18, 2023
From: ARCONIC TECHNOLOGIES LLC
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION
Reel/Frame 064641/0781 →
SECURITY INTEREST Recorded May 14, 2020
From: ARCONIC TECHNOLOGIES LLC
To: DEUTSCHE BANK AG NEW YORK BRANCH
Reel/Frame 052672/0425 →
RELEASE OF SECURITY INTEREST Recorded May 14, 2020
From: JPMORGAN CHASE BANK, N.A.
To: ARCONIC TECHNOLOGIES LLC
Reel/Frame 052671/0850 →
SECURITY INTEREST Recorded May 14, 2020
From: ARCONIC TECHNOLOGIES LLC
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 052671/0937 →
PATENT SECURITY AGREEMENT Recorded Mar 31, 2020
From: ARCONIC TECHNOLOGIES LLC
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 052272/0669 →
SECURITY INTEREST Recorded Mar 26, 2020
From: ARCONIC TECHNOLOGIES LLC
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 052235/0826 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 23, 2020
From: ARCONIC INC.
To: ARCONIC TECHNOLOGIES LLC
Reel/Frame 052204/0580 →
MERGER Recorded Mar 16, 2020
From: ARCONIC INC.
To: ARCONIC INC.
Reel/Frame 052167/0298 →
CHANGE OF NAME Recorded Nov 11, 2016
From: ALCOA INC.
To: ARCONIC INC.
Reel/Frame 040599/0309 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 17, 2013
From: KAHN, JAY A.; NINTZEL, GRANT; BIEHLMANN, YVES; BELNAP, CRAIG; ZEDIAK, CLINTON; KEENER, JOHN; BELL, JAMES; ASKIN, ALBERT L.; KOLEK, PAULA L.; SKILES, JEAN ANN
To: ALCOA INC.
Reel/Frame 031798/0573 →
Continuity (3)
Continuation 12569673 · Sep 29, 2009
Provisional Application 61230953 · Aug 3, 2009
Related Publication 20140106074A1 · Apr 17, 2014