IP Library Granted Patent US 9,865,870
Granted Patent B2
US 9,865,870 · App. 14/122,559 · Granted Jan 9, 2018

Batteries with nanostructured electrodes and associated methods

Inventors: M. Grant Norton (Pullman, WA); Uttara Sahaym (Pullman, WA); Sarah Miller (Evanston, IL)
Assignee: WASHINGTON STATE UNIVERSITY
H01M4/387C25D1/003C25D1/006H01M4/02H01M4/04H01M4/0438H01M4/0452H01M4/0461H01M4/1395H01M4/38H01M4/66H01M4/8605H01M4/8626H01M10/04C25D3/30C25D5/18C25D21/12H01M4/134H01M10/0525H01M2004/021
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Quick Facts
Patent No.
US 9,865,870
App. No.
14/122,559
Granted
Jan 9, 2018
Kind
B2
Abstract

Several embodiments related to batteries having electrodes with nanostructures, compositions of such nanostructures, and associated methods of making such electrodes are disclosed herein. In one embodiment, a method for producing an anode suitable for a lithium-ion battery comprising preparing a surface of a substrate material and forming a plurality of conductive nanostructures on the surface of the substrate material via electrodeposition without using a template.

Claims (13)

1. A method for producing an anode suitable for a lithium-ion battery, the method comprising:

preparing a surface of a substrate material;

forming a plurality of conductive nanostructures on the surface of the substrate material via electro-deposition without using a template; and

controlling at least one of the operating conditions of the electrodeposition based on a target profile for the plurality of conductive nanostructures formed on the surface of the substrate, the target profile including the conductive nanostructures forming a plurality of freestanding structures, wherein the electro-deposition is preceded by soaking the substrate in an electrolyte, the soaking time being controlled based on a target area coverage density for the plurality of conductive nanostructures formed on the surface of the substrate.

2. The method of claim 1 wherein forming a plurality of conductive nanostructures includes forming a plurality of conductive nanostructures on the surface of the substrate material via electrodeposition without using a template at a temperature greater than about 40° C.

3. The method of claim 1 wherein forming a plurality of conductive nanostructures includes forming a plurality of conductive nanoneedles on the surface of the substrate material via electrodeposition without using a template.

4. The method of claim 1 wherein forming a plurality of conductive nanostructures includes forming a plurality of tin (Sn) nanoneedles on the surface of the substrate material via electrodeposition without using a template.

5. The method of claim 1 wherein forming a plurality of conductive nanostructures includes forming a plurality of tin (Sn) nanoneedles on the surface of the substrate material via electrodeposition without using a template, and wherein the substrate material includes copper with surface copper oxide (Cu2O).

6. The method of claim 1 , wherein preparing a surface of a substrate material includes at least one of:

polishing the substrate;

treating the substrate with a basic solution; or

treating the substrate with an acidic solution.

7. The method of claim 1 , wherein the soaking the substrate in an electrolyte includes soaking the substrate in sodium stannate solution.

Assignments (4)
RELEASE OF SECURITY INTEREST IN PATENTS, RECORDED ON JANUARY 29, 2019 AT REEL 048373 FRAME 0217 Recorded Sep 22, 2025
From: CRESTLINE DIRECT FINANCE, L.P., AS COLLATERAL AGENT
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 072936/0464 →
RELEASE OF SECURITY INTEREST Recorded Jul 31, 2019
From: CRESTLINE DIRECT FINANCE, L.P.
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 049924/0794 →
SECURITY INTEREST Recorded Jan 29, 2019
From: EMPIRE TECHNOLOGY DEVELOPMENT LLC
To: CRESTLINE DIRECT FINANCE, L.P.
Reel/Frame 048373/0217 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 1, 2014
From: WASHINGTON STATE UNIVERSITY RESEARCH FOUNDATION
To: WASHINGTON STATE UNIVERSITY
Reel/Frame 033445/0961 →
Continuity (2)
Provisional Application 61493822 · Jun 6, 2011
Related Publication 20140315085A1 · Oct 23, 2014