IP Library Granted Patent US 9,464,016
Granted Patent B2
US 9,464,016 · App. 14/124,671 · Granted Oct 11, 2016

Catechol derivatives for treatment of oxidative stress diseases

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Quick Facts
Patent No.
US 9,464,016
App. No.
14/124,671
Granted
Oct 11, 2016
Kind
B2
Abstract

Methods of treating or suppressing oxidative stress disorders affecting normal electron flow in the cells, including mitochondrial diseases, impaired energy processing disorders, neurodegenerative diseases, diseases of aging and diseases caused by reactive oxygen species are disclosed, as well as compounds useful in the methods of the invention, such as such as catechol or ortho-quinone derivatives of Formula (I).

Claims (72)

1. A compound of Formula I:

where X is selected from the group consisting of:

where the * indicates the point of attachment of X to the rest of the molecule;

each bond indicated by a dashed line is independently double or single;

m is 0 or 1;

n is 1 to 10;

R 1 , R 2 and R 3 are independently selected from the group consisting of hydrogen, C 1 -C 6 -alkyl, C 1 -C 6 -haloalkyl, and halogen;

R 4 is OH and R 5 is hydrogen; or R 4 and R 5 are both hydrogen; and

R 6 is hydrogen, C 1 -C 6 -alkyl, —C(O)C 1 -C 6 -alkyl or —C(O)aryl;

or a salt, a stereoisomer, a mixture of stereoisomers, a solvate or a hydrate thereof.

2. The compound of claim 1 , having the formula Ia:

where,

each bond indicated by a dashed line is independently double or single;

m is 0 or 1;

n is 1 to 4;

R 1 , R 2 and R 3 are independently selected from the group consisting of hydrogen, C 1 -C 6 -alkyl, C 1 -C 6 -haloalkyl, and halogen;

R 4 is OH and R 5 is hydrogen; or R 4 and R 5 are both hydrogen;

or a salt, a stereoisomer, a mixture of stereoisomers, a solvate or a hydrate thereof.

3. The compound of claim 1 , having the Formula Ib:

where,

each bond indicated by a dashed line is independently double or single;

m is 0 or 1;

n is 1 to 4;

R 1 , R 2 and R 3 are independently selected from the group consisting of hydrogen, C 1 -C 6 -alkyl, C 1 -C 6 -haloalkyl, and halogen;

R 4 is OH and R 5 is hydrogen; or R 4 and R 5 are both hydrogen;

or a salt, a stereoisomer, a mixture of stereoisomers, a solvate or a hydrate thereof.

4. The compound of claim 1 , where m is 1 and n is 1-4.

5. The compound of claim 1 , where m is 0 and n is 1-4.

6. The compound of claim 1 , where R 4 and R 5 are both hydrogen.

7. The compound of claim 1 , where R 4 is OH and R 5 is hydrogen.

8. A pharmaceutical composition comprising the compound of claim 1 and a pharmaceutically acceptable excipient.

9. The compound of claim 1 , wherein the compound is selected from the group consisting of:

4-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)benzene-1,2-diol;

4-(3-hydroxy-3,7,11,15,19-pentamethylicosa-6,10,14,18-tetraen-1-yl)benzene-1,2-diol;

4-(3-hydroxy-3,7,11-trimethyldodeca-6,10-dien-1-yl)benzene-1,2-diol;

4-(3-hydroxy-3,7-dimethyloct-6-en-1-yl)benzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-3,5,6-trimethylbenzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-3,5-dimethylbenzene-1,2-diol;

5-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-3,4-dimethylbenzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-3,6-dimethylbenzene-1,2-diol;

5-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-3-methylbenzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-5-methylbenzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-3-methylbenzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadecyl)benzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadecyl)-3,5,6-trimethylbenzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadecyl)-3,5-dimethylbenzene-1,2-diol;

5-(3-hydroxy-3,7,11,15-tetramethylhexadecyl)-3,4-dimethylbenzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadecyl)-3,6-dimethylbenzene-1,2-diol;

5-(3-hydroxy-3,7,11,15-tetramethylhexadecyl)-3-methylbenzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadecyl)-5-methylbenzene-1,2-diol;

4-(3-hydroxy-3,7,11,15-tetramethylhexadecyl)-3-methylbenzene-1,2-diol;

4-(3,7,11,15-tetramethylhexadecyl)benzene-1,2-diol;

3,4,6-trimethyl-5-(3,7,11,15-tetramethylhexadecyl)benzene-1,2-diol;

3,4-dimethyl-5-(3,7,11,15-tetramethylhexadecyl)benzene-1,2-diol;

3,6-dimethyl-4-(3,7,11,15-tetramethylhexadecyl)benzene-1,2-diol;

3,5-dimethyl-4-(3,7,11,15-tetramethylhexadecyl)benzene-1,2-diol;

4-methyl-5-(3,7,11,15-tetramethylhexadecyl)benzene-1,2-diol;

3-methyl-5-(3,7,11,15-tetramethylhexadecyl)benzene-1,2-diol;

3-methyl-4-(3,7,11,15-tetramethylhexadecyl)benzene-1,2-diol;

3-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)benzene-1,2-diol;

3-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-4,5,6-trimethylbenzene-1,2-diol;

6-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-3,4-dimethylbenzene-1,2-diol;

3-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-4,5-dimethylbenzene-1,2-diol;

3-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-4,6-dimethylbenzene-1,2-diol;

3-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-4-methylbenzene-1,2-diol;

3-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-5-methylbenzene-1,2-diol;

3-(3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)-6-methylbenzene-1,2-diol;

3-(3-hydroxy-3,7,11,15,19-pentamethylicosa-6,10,14,18-tetraen-1-yl)benzene-1,2-diol;

3-(3-hydroxy-3,7,11-trimethyldodeca-6,10-dien-1-yl)benzene-1,2-diol; and

3-(3-hydroxy-3,7-dimethyloct-6-en-1-yl)benzene-1,2-diol;

or a stereoisomer, mixture of stereoisomers, solvate, or hydrate thereof.

10. The compound of claim 1 , wherein the compound is selected from the group consisting of: 4-(6E,10E)-3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)benzene-1,2-diol; and 3-((6E,10E)-3-hydroxy-3,7,11,15-tetramethylhexadeca-6,10,14-trien-1-yl)benzene-1,2-diol.

Assignments (5)
TERMINATION AND RELEASE OF PATENT SECURITY AGREEMENT @ REEL 061803 AND FRAME 0878 Recorded Oct 20, 2023
From: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
To: PTC THERAPEUTICS, INC.
Reel/Frame 065303/0163 →
SECURITY INTEREST Recorded Oct 28, 2022
From: PTC THERAPEUTICS, INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 061803/0878 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 15, 2019
From: BIOELECTRON TECHNOLOGY CORPORATION
To: PTC THERAPEUTICS, INC.
Reel/Frame 051041/0478 →
CHANGE OF NAME Recorded Feb 8, 2017
From: EDISON PHARMACEUTICALS, INC.
To: BIOELECTRON TECHNOLOGY CORPORATION
Reel/Frame 041660/0644 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 19, 2014
From: MOLLARD, PAUL; PFISTER, GLORIA
To: EDISON PHARMACEUTICALS, INC.
Reel/Frame 032249/0619 →