IP Library Granted Patent US 9,821,291
Granted Patent B2
US 9,821,291 · App. 14/128,324 · Granted Nov 21, 2017

Material such as film, fiber, woven and nonwoven fabric with adsorbancy

Inventor: Willard E. Wood (Arden Hills, MN)
Assignee: CELLRESIN TECHNOLOGIES, LLC
B01J20/262B01D53/02B01D53/04B01D53/48B01J20/103B01J20/28011B01J20/28023B01J20/28057B01J20/321B01J20/3204B01J20/3212B01J20/3236B01J20/3248B01D53/52B01D2253/106B01D2253/112B01D2253/202B01D2253/25B01D2253/306B01D2255/20738B01D2257/304B01D2257/306B01D2257/706B01D2257/90B01D2259/4541Y10T428/1362Y10T442/2508
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Quick Facts
Patent No.
US 9,821,291
App. No.
14/128,324
Granted
Nov 21, 2017
Kind
B2
Abstract

Compositions that can be used to adsorb low concentration, of unwanted or target substances from a dynamic fluid stream or from an enclosed static vapor phase. Such adsorbency can be obtained with thermoplastic materials used in the form of bulk polymer or a film, fiber, web, woven fabric, non-woven fabric, sheet, packaging and other such structures including or surrounding the enclosed volume. The concentration should be reduced to non-offensive sensed limits or a limit that does not produce a biological response.

Claims (27)

1. An adsorbent comprising a nonwoven fabric having a coating, the coating comprising a solid surface, the solid surface comprising an interface with a gas or vapor phase, the solid surface comprising:

a. ferric hydroxide; and

b. an uncomplexed polyethylenimine

wherein the adsorbent is adapted for adsorbing unwanted or target substances from the gas or vapor phase.

2. The adsorbent of claim 1 , wherein the ferric hydroxide is the reaction product of a hydroxide reactant and a source of an Fe(III) compound.

3. The adsorbent of claim 1 , wherein the polyethylenimine has a molecular weight (M n ) of 800 to 1,000,000 and the adsorbent is substantially free of silica.

4. The adsorbent of claim 1 , wherein the polyethylenimine is free of substituents.

5. The adsorbent of claim 1 , wherein the polyethylenimine comprises an ethoxylated polyethylenimine.

6. The adsorbent of claim 1 , wherein there is about 1 to 85 wt % of the ferric hydroxide and 0.1 to 80 wt % of polyethylenimine based on solids content.

7. The adsorbent of claim 1 , wherein the ferric hydroxide is the decomposition product of an aqueous solution of a ferrate salt.

8. The adsorbent of claim 1 , wherein the fabric has a coated surface area of at least 0.1 m 2 g −1 .

9. The adsorbent of claim 1 , wherein the polyethylenimine has a molecular weight (M n ) of 800 to 1,000,000 and the adsorbent is free of silica.

10. The adsorbent of claim 1 , the adsorbent comprising about 0.1 to 35 wt % of the ferric hydroxide and 0.1 to 35 wt % of polyethylenimine based on the weight of the adsorbent.

11. The adsorbent of claim 1 , wherein the nonwoven fabric comprises a polyolefin or a polyester.

12. The adsorbent of claim 1 , wherein the fabric comprises a web having a thickness of about 0.01 to 1 mm.

13. The adsorbent of claim 1 , wherein the fabric comprises a polyester non-woven.

14. The adsorbent of claim 1 , wherein the fabric comprises a polyolefin non-woven.

15. A method of adsorbing unwanted or target substances from a dynamic gas or vapor phase with the adsorbent of claim 1 comprising a nonwoven fabric, the dynamic gas or vapor phase having a concentration of unwanted or target substances of less than 15 ppm, the method comprises:

i. positioning the adsorbent such that the dynamic gas or vapor phase is in contact with the adsorbent at a contact time of less than 1 second; and

ii. causing the concentration of the unwanted or target substance be reduced in the dynamic gas or vapor phase.

16. The method of claim 15 , wherein in the coating there is about 0.01 to 80 wt % of the ferric hydroxide and 0.01 to 80 wt % of the incomplexed polyethylenimine based on the solids content of the coating.

17. The method of claim 15 , wherein the nonwoven fabric comprises a web having a thickness of about 0.01 to 10 mm.

18. The method of claim 15 , wherein the nonwoven fabric comprises a polyester non-woven.

19. The method of claim 15 , wherein the nonwoven fabric comprises a polyolefin non-woven.

20. The adsorbent of claim 2 , wherein the source of the iron(III) compound is a ferric sulfate, ferric chloride, ferric nitrate, or any combination thereof.

21. A container comprising the adsorbent of claim 1 , wherein the container comprises the unwanted or target substances.

22. A face mask comprising one or more layers, wherein at least one of the one or more layers comprises the adsorbent of claim 1 .

Assignments (2)
CHANGE OF NAME Recorded Dec 4, 2020
From: CELLRESIN TECHNOLOGIES, LLC
To: VERDANT TECHNOLOGIES, LLC
Reel/Frame 054591/0969 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 4, 2014
From: WOOD, WILLARD E.
To: CELLRESIN TECHNOLOGIES, LLC
Reel/Frame 032348/0030 →
Priority Claims (1)
CA 2744780 · Jun 23, 2011 · national
Continuity (1)
Related Publication 20140334998A1 · Nov 13, 2014