IP Library Granted Patent US 9,216,906
Granted Patent B2
US 9,216,906 · App. 14/140,516 · Granted Dec 22, 2015

Method for manufacturing aluminum nitride powder

Inventors: Yang-Kuao Kuo (Taoyuan County, TW); Yung-Han Huang (Taoyuan County, TW); Cheng-Hung Shih (Taoyuan County, TW); Lea-Hwung Leu (aoyuan County, TW)
Assignee: NATIONAL CHUNG SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY
C01B21/072C01B21/0722C01B21/0726
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Quick Facts
Patent No.
US 9,216,906
App. No.
14/140,516
Granted
Dec 22, 2015
Kind
B2
Abstract

A method for manufacturing aluminum nitride powder includes steps of: preparing a polymer powder, a wood powder having grain size similar with that of the polymer powder, and an alumina powder; and mixing the polymer powder, the wood powder and the alumina powder uniformly and forming granules to be carried out a single-replacement reaction by exposing the granules in a nitrogen-containing atmosphere at a temperature of 1680-1850° C.

Claims (8)

1. A method for manufacturing aluminum nitride powder comprising steps of:

preparing a polymer powder, a wood powder, a carbon black and an alumina powder;

mixing the polymer powder, the wood powder, the carbon black and the alumina powder uniformly and forming granules;

performing a single-replacement reaction by exposing the granules in a nitrogen-containing atmosphere at a temperature of 1680-1850° C., such that carbon atoms of the granules act as a medium for replacement reaction, and most of oxygen atoms are separated from alumina via crystal vibration and replaced by nitrogen atoms to form the aluminum nitride powder; and

performing a decarbonization treatment to remove carbon by providing an oxygen-containing gas flowing through the aluminum nitride powder at a temperature of 600-800° C.;

wherein a weight ratio of the polymer powder and the wood powder is in a range of 0.15:1 to 0.42:1.

2. The method for manufacturing aluminum nitride powder as claimed in claim 1 , wherein the polymer powder is polyvinyl butyral (PVB).

3. The method for manufacturing aluminum nitride powder as claimed in claim 1 , wherein the granules is obtained by binding the polymer powder, the wood powder, the carbon black and the alumina powder together via a spray granulation process.

Assignments (2)
CHANGE OF NAME Recorded Apr 17, 2015
From: CHUNG-SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY, ARMAMENTS BUREAU, M.N.D.
To: NATIONAL CHUNG SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY
Reel/Frame 035453/0341 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 25, 2013
From: KUO, YANG-KUAO; HUANG, YUNG-HAN; SHIH, CHENG-HUNG; LEU, LEA-HWUNG
To: CHUNG-SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY, ARMAMENTS BUREAU, M.N.D
Reel/Frame 031846/0828 →
Continuity (1)
Related Publication 20150175421A1 · Jun 25, 2015