IP Library Granted Patent US 9,889,541
Granted Patent B2
US 9,889,541 · App. 14/147,241 · Granted Feb 13, 2018

Polycrystalline diamond compacts and related methods

Inventors: Mohammad N. Sani (Orem, UT); Jair J. Gonzalez (Provo, UT); Andrew E. Dadson (Provo, UT); Debkumar Mukhopadhyay (Sandy, UT)
Assignee: US SYNTHETIC CORPORATION
B24D3/10B22F3/24B22F5/00B22F7/06B24D18/0009B24D18/0027C22C26/00Y10T428/12028Y10T428/12056Y10T428/24355Y10T428/30
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Quick Facts
Patent No.
US 9,889,541
App. No.
14/147,241
Granted
Feb 13, 2018
Kind
B2
Abstract

Embodiments of the invention relate to polycrystalline diamond compacts (“PDCs”) and methods of fabricating polycrystalline diamond tables and PDCs in a manner that facilitates removal of metal-solvent catalyst used in the manufacture of polycrystalline diamond tables of such PDCs.

Claims (17)

1. A polycrystalline diamond compact, comprising:

a substrate; and

a polycrystalline diamond table including a working surface and an opposing interfacial surface directly bonded to the substrate, the polycrystalline diamond table including bonded diamond grains defining a plurality of interstitial regions, the polycrystalline diamond table further including:

a first volume of the polycrystalline diamond table including the bonded diamond grains extending inwardly from the working surface;

a second volume of the polycrystalline diamond table including the bonded diamond grains extending inwardly from the interfacial surface;

a metal-solvent catalyst and at least one sacrificial material disposed in at least a portion of the plurality of interstitial regions;

wherein the at least one sacrificial material comprises a material different than that of the metal-solvent catalyst, the at least one sacrificial material including a plurality of sacrificial particles, at least one reaction product of the plurality of diamond grains and the plurality of sacrificial particles, or combinations thereof;

wherein the at least one sacrificial material is present in the first volume and the second volume of the polycrystalline diamond table in a pre-leaching concentration of greater than 0 weight % to about 5 weight % of the first volume and the second volume prior to leaching the first volume;

wherein the at least one sacrificial material is present in the first volume in a concentration such that the first volume exhibits a post-leaching concentration of the metal-solvent catalyst of less than 0.85 weight % of the first volume, and the second volume includes the pre-leaching concentration of the at least one sacrificial material, after leaching the first volume.

2. The polycrystalline diamond compact of claim 1 wherein the post-leaching concentration of the metal-solvent catalyst in the first volume is about 0.20 weight % to about 0.50 weight % after leaching.

3. The polycrystalline diamond compact of claim 1 wherein the post-leaching concentration of the metal-solvent catalyst in the first volume is about 0.50 weight % to about 0.78 weight %.

4. The polycrystalline diamond compact of claim 1 wherein the metal-solvent catalyst includes at least one member selected from the group consisting of iron, nickel, and cobalt.

5. The polycrystalline diamond compact of claim 1 wherein the at least one sacrificial material includes tungsten carbide.

6. The polycrystalline diamond compact of claim 1 wherein the pre-leaching concentration of the at least one sacrificial material is about 1 weight % to about 5 weight %.

7. The polycrystalline diamond compact of claim 1 wherein the pre-leaching concentration of the at least one sacrificial material is about 1.5 weight % to about 2.5 weight %.

8. The polycrystalline diamond compact of claim 1 wherein the first volume extends to a depth of about 50 μm to about 500 μm from the working surface.

9. The polycrystalline diamond compact of claim 1 wherein the first volume extends to a depth of at least about 200 μm from the working surface.

Assignments (4)
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: ACE DOWNHOLE, LLC; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; APERGY BMCS ACQUISITION CORP.; NORRISEAL-WELLMARK, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
Reel/Frame 060305/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: ACE DOWNHOLE, LLC; APERGY BMCS ACQUISITION CORP.; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 053790/0001 →
SECURITY AGREEMENT Recorded May 9, 2018
From: APERGY (DELAWARE) FORMATION, INC.; APERGY BMCS ACQUISITION CORP.; APERGY ENERGY AUTOMATION, LLC; HARBISON-FISCHER, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 046117/0015 →
Continuity (3)
Continuation 12608155 · Oct 29, 2009
Provisional Application 61109752 · Oct 30, 2008
Related Publication 20140115971A1 · May 1, 2014