IP Library Granted Patent US 9,410,059
Granted Patent B2
US 9,410,059 · App. 14/160,065 · Granted Aug 9, 2016

Wax treated article and method of making

Inventors: Chunjiang Fu (North Mankato, MN); Wajira Asanga Ratnayake Manamperi (Madelia, MN); Dan Dhuyvetter (Saint Peter, MN)
Assignee: Alltech, Inc.
C09D191/06B27N5/02B27N7/00C09D191/08Y10T428/13
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Quick Facts
Patent No.
US 9,410,059
App. No.
14/160,065
Granted
Aug 9, 2016
Kind
B2
Abstract

Water swellable articles are treated with wax by applying a molten wax to the article, the wax having a kinematic viscosity of between about 0.1 cSt to 20 cSt at 100° C., wherein the temperature of the article at the time of applying is about 40° C. to 200° C., with the proviso that the temperature is not less than 30° C. below the melting point of the wax. Using this method of treatment, swelling of the article in water is reduced by at least 25% compared to the same article treated with molten wax wherein the article is at ambient temperature at the time the wax is applied.

Claims (19)

1. A process for making a container, the process comprising:

placing a fiber mixture in a mold, the fiber mixture comprising a fiber and a binder, the fiber and the binder being biodegradable, edible, or both;

forming a self-supporting container by application of heat and pressure to the fiber mixture in the mold, the container having an interior container surface and exterior container surface;

removing the container from the mold;

upon removing the container from the mold, applying a molten wax to the container, the wax having a kinematic viscosity of between about 0.1 cSt to 20 cSt at 100° C., wherein the temperature of the container at the time of applying is about 40° C. to 200° C., with the proviso that the temperature is not less than 30° C. below the melting point of the wax; and

cooling the container to a temperature below the melting point of the wax.

2. The process of claim 1 wherein the fiber comprises wood fiber, straw, corn husks, sorghum stalks, soybean hulls, peanut hulls, or a combination of two or more thereof.

3. The process of claim 1 wherein the binder comprises soy flour.

4. The process of claim 1 wherein the container is coated on at least a portion of the exterior surface thereof.

5. The process of claim 1 wherein the container is coated on both the interior and exterior surfaces thereof.

6. The process of claim 4 wherein swelling of the container in water is reduced by at least 25% compared to a container having a wax coating wherein the temperature of the container at the time of applying the wax is ambient temperature.

7. The process of claim 1 further comprising bringing the container to the temperature of about 40° C. to 200° C. by pre-heating the container in an oven, by use of microwave radiation, or by use of infrared radiation.

8. The process of claim 1 wherein the temperature of the container at the time of applying is about 50° C. to 190° C., with the proviso that the temperature is not less than 20° C. below the melting point of the wax.

9. The process of claim 1 wherein the melting point of the wax is from 55° C. to 90° C.

10. The process of claim 1 further comprising pre-heating the wax to a temperature that is about 5° C. to 50° C. above the melting point of the wax at the time of the applying.

11. The process of claim 1 further comprising pre-heating the wax to a temperature that is about 15° C. to 30° C. above the melting point of the wax at the time of the applying.

12. The process of claim 1 wherein the applying comprises dipping the container in the molten wax.

13. The process of claim 1 wherein the applying comprises curtain coating the container with the molten wax.

14. The process of claim 1 wherein the container has a surface roughness R a of from 1 μm to 2 cm before the applying.

Assignments (8)
SECOND LIEN PATENT SECURITY AGREEMENT Recorded Nov 14, 2024
From: ALLTECH, INC.; RIDLEY USA INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
Reel/Frame 069357/0281 →
PATENT SECURITY AGREEMENT Recorded Dec 1, 2021
From: RIDLEY USA INC.
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 058292/0942 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS (10) Recorded Nov 30, 2021
From: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
To: RIDLEY USA INC.
Reel/Frame 058291/0994 →
RELEASE OF SECURITY INTEREST Recorded Oct 26, 2021
From: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
To: ALLTECH, INC.; RIDLEY USA INC.
Reel/Frame 057919/0761 →
ASSIGNMENT FOR SECURITY -- PATENTS Recorded May 18, 2020
From: ALLTECH, INC; RIDLEY USA, INC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
Reel/Frame 052694/0412 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE NAME PREVIOUSLY RECORDED ON REEL 032505 FRAME 0386. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Apr 20, 2016
From: FU, CHUNJIANG; MANAMPERI, WAJIRA ASANGA RATNAYAKE; DHUYVETTER, DAN
To: RIDLEY USA INC.
Reel/Frame 038475/0114 →
PATENT SECURITY AGREEMENT Recorded Apr 19, 2016
From: RIDLEY USA INC.
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 038464/0083 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 24, 2014
From: FU, CHUNJIANG; MANAMPERI, WAJIRA ASANGA RATNAYAKE
To: RIDLEY USA, INC.
Reel/Frame 032505/0386 →
Continuity (1)
Related Publication 20150203719A1 · Jul 23, 2015