IP Library Granted Patent US 9,113,643
Granted Patent B2
US 9,113,643 · App. 14/170,358 · Granted Aug 25, 2015

Process for the production of a liquid coffee concentrate

Inventors: Gertjan Heijman (Gouda, NL); Wilhelmus Johannes de Bruin (Almere, NL); Maarten Juriaan Verhoeven (Den Bosch, NL)
Assignee: Koninklijke Douwe Egberts B.V.
A23F5/46A23F5/24A23F5/26A23F5/28A23F5/285A23F5/50
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Quick Facts
Patent No.
US 9,113,643
App. No.
14/170,358
Granted
Aug 25, 2015
Kind
B2
Abstract

The present disclosure relates to a process for the production of a liquid coffee concentrate that has an improved storage stability at ambient temperature. The process comprises separating coffee extract resulting in a high aromatic coffee extract and a low aromatic coffee extract and subjecting the low aromatic coffee extract to a heat treatment and, optionally, a pH rising step.

Claims (44)

1. A process for the production of a liquid coffee concentrate with a pH of 4.8 to 6, the process comprising:

subjecting roasted, ground coffee to one or more extraction steps with water resulting in a coffee extract;

separating the coffee extract, either by fractionation during the extraction step(s) or by aroma recovery after the extraction step(s) resulting in a high aromatic coffee extract and a low aromatic coffee extract;

subjecting at least 50 v/v % of the low aromatic coffee extract to a heat treatment of at least 120° C. for at most 30 minutes;

concentrating at least the heat treated low aromatic coffee extract to form a concentrated low aromatic coffee extract;

combining at least the concentrated low aromatic coffee extract with the high aromatic coffee extract, thereby obtaining a liquid coffee concentrate, wherein the liquid coffee concentrate has a pH of 4.8 to 6.

2. The process of claim 1 , further comprising raising the pH of the low aromatic coffee extract after separating the coffee extract.

3. The process of claim 2 , comprising raising the pH of at least 50 v/v % of the low aromatic extract.

4. The process of claim 3 , comprising raising the pH of at least 50 v/v % of the low aromatic extract before or after the heat treatment but before the concentrating.

5. The process of claim 1 , wherein the heat treatment is conducted at a temperature of at least 135° C., for a time of at most 15 minutes.

6. The process of claim 1 , wherein the heat treatment is conducted from 120° C. to 200° C. for a time of 30 minutes to 10 seconds.

7. The process of claim 1 , wherein the heat treatment is conducted from 135° C. to 180° C. for a time of 15 minutes to 1 minute.

8. The process of claim 1 , wherein the heat treatment is conducted at about 150° C. for a time of about 5 minutes.

9. The process of claim 2 , wherein the pH is raised to a value of 5 to 10.

10. The process of claim 4 , wherein the pH is raised prior to the heat treatment.

11. The process of claim 10 , wherein the pH is raised to a value of 6 to 8.

12. The process of claim 4 , wherein the pH is raised after the heat treatment.

13. The process of claim 12 , wherein the pH is raised to a value of 5 to 7.

14. The process of claim 2 , wherein the pH is raised with an anion exchanger.

15. The process of claim 1 , wherein the process results in a hydrolysation of at least 150 mmoles acid/kg dry matter solids content in the liquid coffee extract.

16. A process for the production of a liquid coffee concentrate with a pH of 4.8 to 6, the process comprising:

subjecting roasted, ground coffee to one or more extraction steps with water resulting in a coffee extract;

separating the coffee extract by fractionation during the extraction step(s) resulting in a high aromatic coffee extract and a low aromatic coffee extract, wherein the low aromatic coffee extract comprises a second primary extract and a secondary extract;

subjecting at least part of the second primary extract to a heat treatment of at least 120° C. for at most 30 minutes, wherein the part of the second primary extract to be treated comprises at least 25 v/v % of the low aromatic coffee extract, resulting in a treated low aromatic coffee extract;

concentrating at least the treated low aromatic coffee extract, resulting in a concentrated low aromatic coffee extract; and

combining at least the concentrated low aromatic coffee extract with the high aromatic coffee extract, thereby obtaining a liquid coffee concentrate, wherein the liquid coffee concentrate has a pH of 4.8 to 6.

17. The process of claim 16 , further comprising raising the pH of the low aromatic coffee extract after separating the coffee extract.

18. The process of claim 17 , wherein the pH of at least part of the second primary extract is raised.

19. The process of claim 18 , wherein the pH of at least part of the second primary extract is raised before or after the heat treatment but before the concentrating.

20. The process of claim 16 , wherein the heat treatment is conducted at a temperature of at least 135° C., for a time of at most 15 minutes.

21. The process of claim 16 , wherein the heat treatment is conducted from 120° C. to 200° C. for a time of 30 minutes to 10 seconds.

22. The process of claim 16 , wherein the heat treatment is conducted from 135° C. to 180° C. for a time of 15 minutes to 1 minute.

23. The process of claim 16 , wherein the heat treatment is conducted at about 150° C. for a time of about 5 minutes.

24. The process of claim 17 , wherein the pH is raised to a value of 5 to 10.

25. The process of claim 19 , wherein the pH is raised prior to the heat treatment.

26. The process of claim 25 , wherein the pH is raised to a value of 6 to 8.

27. The process of claim 19 , wherein the pH is raised after the heat treatment.

28. The process of claim 27 , wherein the pH is raised to a value of 5 to 7.

29. The process of claim 17 , wherein the pH is raised with an anion exchanger.

30. The process of claim 16 , wherein the process results in a hydrolysation of at least 150 mmoles acid/kg dry matter solids content in the liquid coffee extract.

31. The process of claim 1 , wherein the heat treatment is conducted at a temperature of at least 150° C., for a time of at most 10 minutes.

32. The process of claim 2 , wherein the pH is raised with an anion exchange column.

33. The process of claim 16 , wherein the heat treatment is conducted at a temperature of at least 150° C., for a time of at most 10 minutes.

34. The process of claim 17 , wherein the pH is raised with an anion exchange column.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 20, 2014
From: HEIJMAN, GERTJAN; DE BRUIN, WILHELMUS JOHANNES; VERHOEVEN, MAARTEN JURIAAN
To: KONINKLIJKE DOUWE EGBERTS B.V.
Reel/Frame 032937/0375 →
Priority Claims (1)
EP 11176077 · Aug 1, 2011 · regional
Continuity (2)
Continuation PCTNL2012050543 · Aug 1, 2012
Related Publication 20140147562A1 · May 29, 2014