IP Library Granted Patent US 9,567,229
Granted Patent B2
US 9,567,229 · App. 14/184,401 · Granted Feb 14, 2017

Fumed silica

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Quick Facts
Patent No.
US 9,567,229
App. No.
14/184,401
Granted
Feb 14, 2017
Kind
B2
Abstract

Fumed silica having a BET surface area of 200±15 m2/g, a grindometer value of less than 30 μm and a median value by PCS of 65 to 85 nm is prepared by grinding a fumed silica having a surface area of 200±25 m2/g, and silicone rubber containing this silica.

Claims (18)

1. Hydrophilic milled fumed silica prepared by a process having no propensity to reagglomerate, comprising grinding fumed silica having a BET surface area of 200±25 m 2 /g and recovering a hydrophilic milled fumed silica that exhibits lower grindometer values and smaller median values than the starting fumed silica, wherein the hydrophilic milled fumed silica contains no hydrophobic fractions and has the following physicochemical data:

BET surface area

200 ± 15 m 2 /g

Grindometer value

less than 30 μm

Median value by PCS

65 to 85 nm

D50

12 to 14 weight distribution

Particle size span

5.260 to 34.70 nm

Particle size mean

11.5 to 13.5 nm.

2. A composition comprising silicone rubber and the hydrophilic milled fumed silica according to claim 1 .

3. Silicone rubber composition comprising 0.5% to 60% by weight of the hydrophilic milled fumed silica according to claim 1 .

4. The silicone rubber composition according to claim 3 which is vulcanized.

5. An article of manufacture made from the vulcanize silicone rubber composition of claim 4 .

6. The hydrophilic milled fumed silica according to claim 1 which has no particles in the range greater than 40 μm.

Assignments (2)
CHANGE OF NAME Recorded Mar 29, 2020
From: EVONIK DEGUSSA GMBH
To: EVONIK OPERATIONS GMBH
Reel/Frame 052254/0052 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 12, 2014
From: SCHOLZ, MARIO; ROCHNIA, MATTHIAS; MEYER, JÜRGEN
To: EVONIK DEGUSSA GMBH
Reel/Frame 032867/0955 →