IP Library Granted Patent US 9,552,958
Granted Patent B2
US 9,552,958 · App. 14/189,506 · Granted Jan 24, 2017

Alignment marking for rock sample analysis

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Quick Facts
Patent No.
US 9,552,958
App. No.
14/189,506
Granted
Jan 24, 2017
Kind
B2
Abstract

A method for using a Focused Ion Beam and/or Scanning Electron Microscope (FIB/SEM) for etching one or more alignment markers on a rock sample, the one or more alignment markers being etched on the rock sample using the FIB/SEM. The one or more alignment markers may further be deposited with a platinum alloy or other suitable compositions for increasing alignment marker visibility.

Claims (42)

1. A method of analyzing a rock sample in one or more analysis devices, the method comprising:

installing the rock sample in the one or more analysis devices;

identifying a localized region of interest and a global region of interest encompassing the localized region of interest on the rock sample in the one or more analysis devices;

performing global marking by aligning the rock sample to the global region of interest in the one or more analysis devices for marking and etching one or more global of alignment markers on the rock sample relative to the global region of interest using the one or more analysis devices; and

performing localized marking by aligning the rock sample to the localized region of interest encompassed in the global region in the one or more analysis devices for marking and etching one or more localized of alignment markers on the rock sample relative to the localized region of interest using the one or more analysis devices.

2. The method of claim 1 , wherein aligning the rock sample for marking comprises aligning the rock sample using an optical microscope as one of the one or more analysis devices.

3. The method of claim 1 , wherein aligning the rock sample for marking comprises aligning the rock sample using a scanning electron microscope as one of the one or more analysis devices.

4. The method of claim 1 , wherein etching the alignment markers on the rock sample comprises etching the alignment markers using a focused ion beam as one of the one or more analysis devices.

5. The method of claim 4 , wherein etching the alignment markers on the rock sample comprises etching a depth of the alignment markers between 1 um and 3 um.

6. The method of claim 1 , wherein etching the alignment markers on the rock sample comprises etching one or more of a vertical bar, a horizontal bar, a circle, a point, a crossed bar, a numeral, and a symbol.

7. The method of claim 1 , further comprising filling the alignment markers with a material.

8. The method of claim 7 , wherein the alignment markers are filled with metal.

9. The method of claim 7 , further comprising polishing the rock sample.

10. The method of claim 1 , wherein the alignment markers indicate a directional orientation of the rock sample.

11. The method of claim 1 , further comprising removing the rock sample from the one or more analysis devices for further handling.

12. The method of claim 11 , further comprising:

reinstalling the rock sample in the one or more analysis devices after further handling;

aligning the rock sample to the global region of interest in the analysis device using the one or more global alignment markers.

13. The method of claim 12 , further comprising

locating the localized region of interest with the one or more global alignment markers;

aligning the rock sample to the localized region of interest with the one or more of localized alignment markers; and

analyzing the localized region of interest with the one or more analysis devices.

14. A method of analyzing a rock sample in one or more analysis devices, the method comprising:

installing the rock sample in the one or more analysis devices;

identifying a region of interest on the rock sample using the one or more analysis devices;

using the one or more analysis devices to place one or more alignment markers on the rock sample to facilitate location of the region of interest;

removing the rock sample from the one or more analysis devices for further handling;

reinstalling the rock sample in the one or more analysis devices after further handling; and

aligning the rock sample to the region of interest in the one or more analysis devices using the one or more alignment markers.

15. The method of claim 14 , wherein using the one or more analysis devices to place the one or more alignment markers on the rock sample comprises placing one or more global elements and one or more local elements of the one or more alignment markers.

16. The method of claim 15 , wherein the one or more local elements are contained in a local region defined by the one or more global elements.

17. The method of claim 15 , wherein reinstalling the rock sample in the one or more analysis devices after further handling and aligning the rock sample to the region of interest in the one or more analysis devices using the one or more alignment markers comprises:

locating the region of interest globally with the one or more global elements;

aligning the rock sample locally to the region of interest with the one or more local elements; and

analyzing the region of interest with the one or more analysis devices.

18. The method of claim 14 , wherein the one or more analysis devices comprises one or more of an optical microscope, a scanning electron microscope, and a focused ion beam.

19. The method of claim 14 , wherein using the one or more analysis devices to place the one or more alignment markers on the rock sample to facilitate location of the region of interest comprises giving the one or more alignment markers with a depth between 1 -μm and 3 -μm.

20. The method of claim 14 , wherein using the one or more analysis devices to place the one or more alignment markers on the rock sample to facilitate location of the region of interest comprises indicating a directional orientation of the rock sample with the one or more alignment markers.

21. The method of claim 14 , wherein using the one or more analysis devices to place the one or more alignment markers on the rock sample to facilitate location of the region of interest comprises placing one or more of a vertical bar, a horizontal bar, a circle, a point, a crossed bar, a numeral, and a symbol for the one or more alignment markers.

22. The method of claim 14 , wherein removing the rock sample from the one or more analysis devices for further handling comprises filling the one or more alignment markers with a material.

23. The method of claim 22 , wherein the alignment markers are filled with metal.

24. The method of claim 14 , wherein removing the rock sample from the one or more analysis devices for further handling comprises polishing the rock sample.

Assignments (7)
SECURITY INTEREST Recorded Apr 7, 2025
From: STRATUM RESERVOIR (US), LLC,; STRATUM RESERVOIR, LLC,; STRATUM RESERVOIR (ISOTECH), LLC,; STRATUM RESERVOIR INTERMEDIATE, LLC,; STRATUM RESERVOIR (US) INTERNATIONAL HOLDINGS, INC.
To: WOODFOREST NATIONAL BANK
Reel/Frame 070749/0681 →
SECURITY INTEREST Recorded Jun 7, 2022
From: STRATUM RESERVOIR INTERMEDIATE, LLC; STRATUM RESERVOIR (US), LLC; STRATUM RESERVOIR, LLC; STRATUM RESERVOIR (ISOTECH), LLC; STRATUM RESERVOIR (US) INTERNATIONAL HOLDINGS, INC.
To: WOODFOREST NATIONAL BANK
Reel/Frame 060120/0735 →
NOTICE OF TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS Recorded May 18, 2022
From: JPMORGAN CHASE BANK, N.A.
To: STRATUM RESERVOIR (US), LLC
Reel/Frame 060116/0242 →
GRANT OF SECURITY INTEREST IN PATENT RIGHTS Recorded May 20, 2019
From: STRATUM RESERVOIR (US), LLC
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 049234/0650 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 1, 2019
From: WEATHERFORD TECHNOLOGY HOLDINGS, LLC; WEATHERFORD U.S, L.P.; WEATHERFORD/LAMB, INC.
To: STRATUM RESERVOIR (US), LLC
Reel/Frame 049046/0032 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 24, 2016
From: WEATHERFORD/LAMB, INC.
To: WEATHERFORD TECHNOLOGY HOLDINGS, LLC
Reel/Frame 039531/0320 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 25, 2014
From: HOOGHAN, KULTARANSINGH N.
To: WEATHERFORD/LAMB, INC.
Reel/Frame 032295/0130 →