IP Library Granted Patent US 9,322,013
Granted Patent B2
US 9,322,013 · App. 14/189,969 · Granted Apr 26, 2016

Magnetic separation of algae

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Quick Facts
Patent No.
US 9,322,013
App. No.
14/189,969
Granted
Apr 26, 2016
Kind
B2
Abstract

Described herein are methods and systems for harvesting, collecting, separating and/or dewatering algae using iron based salts combined with a magnetic field gradient to separate algae from an aqueous solution.

Claims (9)

1. A method comprising:

adding an iron salt to an algae culture in aqueous solution, wherein the iron salt is selected from the group consisting of FeSO 4 ; FeBr 2 ; FeBr 3 ; FeCl 2 ; FeCl 3 ; FeF 2 ; FeF 3 ; FeI 2 ; FeMoO 4 ; (NH 4 ) 2 Fe(SO 4 ) 2 .6H 2 O; C 20 H 20 Cl 2 FeN 4 ; FeCl 2 .4H 2 O; C 6 H 5 FeO 7 ; FeF 3 .3H 2 O; Fe(NO 3 ) 3 .9H 2 O; Fe(C 2 O 4 ).2H 2 O; Fe 2 (C 2 O 4 ) 3 .6H 2 O; FePO 4 .4H 2 O; Fe 4 (P 2 O 7 ) 3 ; FeSO 4 .7H 2 O; Fe(BF 4 ) 2 .6H 2 O; K 4 Fe(CN) 6 .3H 2 O and a combination of two or more thereof, and the iron salt in the aqueous solution is at a concentration of from 100 μM to 1000 μM;

culturing the algae in the aqueous solution with iron salt for at least 24 hours; and

exposing the aqueous solution comprising the cultured algae and the iron salt to a magnetic field gradient generated by a permanent magnet having sufficient strength to separate the algae from the aqueous solution, whereby the method results in the algae being separated from the aqueous solution.

2. The method of claim 1 , wherein the iron salt in the aqueous solution comprises FeSO 4 or FeSO 4 .7H 2 O.

3. The method of claim 1 , wherein the magnetic field gradient is at least about 500 Tesla/meter.

4. The method of claim 3 , wherein the magnetic field gradient is at least about 1000 Tesla/meter.

5. The method of claim 1 , wherein the algae comprises a wild-type algae or a transgenic algae.

6. The method of claim 5 , wherein the algae comprises Tetraselmis striata.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 6, 2018
From: LOS ALAMOS NATIONAL SECURITY, LLC
To: TRIAD NATIONAL SECURITY, LLC
Reel/Frame 047438/0511 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 21, 2016
From: NATH, PULAK; TWARY, SCOTT
To: LOS ALAMOS NATIONAL SECURITY, LLC
Reel/Frame 038049/0501 →
CONFIRMATORY LICENSE Recorded Nov 27, 2015
From: LOS ALAMOS NATIONAL SECURITY
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 037149/0728 →