IP Library Granted Patent US 9,682,878
Granted Patent B2
US 9,682,878 · App. 14/197,034 · Granted Jun 20, 2017

Sodium nitrite oxidation of hydrogen sulfide

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Quick Facts
Patent No.
US 9,682,878
App. No.
14/197,034
Granted
Jun 20, 2017
Kind
B2
Abstract

A method for treating hydrogen sulfide in a solution includes providing the solution containing hydrogen sulfide. The method also includes adding sodium nitrite to the solution in an amount suitable to react with the hydrogen sulfide and treat the hydrogen sulfide.

Claims (21)

1. A method for removing hydrogen sulfide from water, wherein the water comprises hydrogen sulfide, comprising:

adding sodium nitrite to the water in an amount suitable to react with the hydrogen sulfide in the water and remove hydrogen sulfide from the water, wherein the sodium nitrite is added at a mole ratio to hydrogen sulfide in the water from about 1:3 to about 2:3, wherein a concentration of the hydrogen sulfide in the water is about 5,000 mg/liter to about 25,000 mg/liter; and

adding a pH buffer periodically to the water to maintain a pH of the water between about 7.0 to about 9.0 and to remove free ammonia from the water.

2. The method of claim 1 , wherein the step of adding a pH buffer periodically to the water maintains a pH of the water between about 7.0 to about 8.5.

3. The method of claim 1 , wherein the step of adding a pH buffer periodically to the water maintains a pH of the water at about 8.0.

4. The method of claim 1 , wherein the step of adding a pH buffer periodically to the water maintains a pH of the water between about 7.0 to about 8.0.

5. The method of claim 1 , wherein the water is disposed in a tank.

6. The method of claim 1 wherein the step of adding a pH buffer periodically comprises adding the pH buffer to the water about every hour to maintain a pH of the water between about 7.0 to about 9.0.

7. The method of claim 1 , wherein the step of adding a pH buffer periodically comprises adding pH buffer to the water about every hour for about a three hour segment, beginning after about the second hour after a first addition of the pH buffer.

8. A method for removing hydrogen sulfide from water, wherein the water comprises hydrogen sulfide, comprising:

(A) adding sodium nitrite to the water in an amount suitable to react with the hydrogen sulfide in the water and remove hydrogen sulfide from the water;

(B) blowing a gas onto the water to remove ammonia formed by a reaction of sodium nitrite and the hydrogen sulfide, wherein a concentration of the hydrogen sulfide in the water is about 5,000 mg/liter to about 25,000 mg/liter; and

(C) adding a pH buffer periodically to the water to maintain a pH of the water between about 7.0 to about 9.0 and to remove free ammonia from the water.

9. The method of claim 8 , wherein the gas is blown by a compressor.

10. The method of claim 8 , wherein the gas comprises nitrogen.

11. The method of claim 8 , wherein the gas comprises air.

12. The method of claim 8 , wherein the step of adding a pH buffer periodically to the water maintains a pH of the water between about 7.0 to about 8.5.

13. The method of claim 8 , wherein the step of adding a pH buffer periodically to the water maintains a pH of the water at about 8.0.

14. The method of claim 8 , wherein the step of adding a pH buffer periodically to the water maintains a pH of the water between about 7.0 to about 8.0.

15. The method of claim 8 wherein the step of adding a pH buffer periodically comprises adding the pH buffer to the water about every hour to maintain a pH of the water between about 7.0 to about 9.0.

16. The method of claim 8 , wherein the step of adding a pH buffer periodically comprises adding pH buffer to the water about every hour for about a three hour segment, beginning after about the second hour after a first addition of the pH buffer.

Assignments (7)
MERGER Recorded Mar 15, 2025
From: CR3 ZYMEFLOW, INC.
To: ZYMEFLOW, INC.
Reel/Frame 070523/0169 →
MERGER Recorded Mar 13, 2025
From: TRISTAR GLOBAL ENERGY SOLUTIONS, INC.
To: CR3 ZYMEFLOW, INC.
Reel/Frame 070508/0396 →
MERGER Recorded Mar 12, 2025
From: UNITED LABORATORIES INTERNATIONAL, LLC
To: TRISTAR GLOBAL ENERGY SOLUTIONS, INC.
Reel/Frame 070491/0243 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 5, 2017
From: SNYDER, KENNETH J., JR.; FROST, JACK G.
To: UNITED LABORATORIES INTERNATIONAL, LLC
Reel/Frame 042253/0978 →
SECURITY INTEREST Recorded Jan 5, 2015
From: UNITED LABORATORIES INTERNATIONAL, LLC; GLOBAL VAPOR CONTROL, INC.
To: ABACUS FINANCE GROUP, LLC, AS AGENT
Reel/Frame 034631/0429 →
RELEASE OF SECURITY INTEREST Recorded Jan 5, 2015
From: TEXAS CAPITAL BANK, NATIONAL ASSOCIATION
To: UNITED LABORATORIES INTERNATIONAL, LLC
Reel/Frame 034634/0719 →
SECURITY INTEREST Recorded Oct 16, 2014
From: UNITED LABORATORIES INTERNATIONAL, LLC
To: TEXAS CAPITAL BANK, NATIONAL ASSOCIATION
Reel/Frame 033960/0530 →