IP Library Granted Patent US 9,321,034
Granted Patent B2
US 9,321,034 · App. 14/199,270 · Granted Apr 26, 2016

Aqueous dispersion liquid and coating material, film, and product using the same

Inventors: Kayo Nakano (Yokohama, JP); Akira Sato (Yokohama, JP); Yasuhiro Shirakawa (Yokohama, JP); Keiichi Fuse (Yokohama, JP); Shinya Kasamatsu (Yokohama, JP); Akito Sasaki (Yokohama, JP)
Assignees: KABUSHIKI KAISHA TOSHIBA; TOSHIBA MATERIALS CO., LTD.
B01J23/30A61L2/232B01J23/34B01J23/6527B01J23/687B01J23/888B01J31/34B01J35/004B01J35/023B01J37/0219B82Y30/00C01G41/02C09C1/00C09D5/00C09D5/1618C09D7/1216C09D7/1266C09D7/1275C09D7/1283B01D53/864B01D2255/20776B01D2255/802B01D2257/702C01P2004/61C01P2004/62C01P2004/64C01P2006/12C01P2006/22C08K3/22
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Quick Facts
Patent No.
US 9,321,034
App. No.
14/199,270
Granted
Apr 26, 2016
Kind
B2
Abstract

In one embodiment, an aqueous dispersion liquid contains at least one particles selected from tungsten oxide particles and tungsten oxide composite particles. A mean primary particle diameter (D50) of the particles is in the range of 1 nm to 400 nm. In the aqueous dispersion liquid, concentration of the particles is in the range of 0.1 mass % to 40 mass %, and pH is in the range of 1.5 to 6.5. The aqueous dispersion liquid excels in dispersibility of particles and capable of maintaining good liquidity for a long period.

Claims (34)

1. A photocatalytic material, comprising:

a substrate; and

a photocatalytic film, formed on the substrate, containing particles selected from the group consisting of tungsten oxide particles and tungsten oxide composite particles,

wherein a mean primary particle diameter (D50) of the particles is from 1 nm to 400 nm,

wherein the tungsten oxide composite contains at least one metal element selected from transition metal elements and aluminum, or a compound including at least one metal element selected from transition metal elements and aluminum, in a range of 0.001 mass% to 50 mass% as an amount of the metal element, balanced by tungsten oxide,

wherein, when a surface state of the particles in the photocatalytic film is observed by a fourier-transform infrared absorption spectroscopy, an absorption peak based on hydroxyl exists in a vicinity of 3700 cm −1 of an absorption spectrum obtained by the fourier-transform infrared absorption spectroscopy, and

wherein the photocatalytic film exhibits photocatalytic performance when visible light is irradiated, wherein the tungsten oxide which constitutes the particles has a crystal structure, and

wherein the crystal structure includes a mixture of a monoclinic crystal of tungsten trioxide, a triclinic crystal of tungsten trioxide, and a rhombic crystal of tungsten trioxide.

2. The photocatalytic material according to claim 1 ,

wherein the photocatalytic film contains at least one selected from the group consisting of a zeolite, an activated carbon, and a porous ceramic.

3. The photocatalytic material according to claim 1 .

wherein the metal element is at least one element selected from the group consisting o titanium, zirconium, manganese, iron, palladium, platinum, copper, silver, aluminum, and cerium.

4. The photocatalytic material according to claim 1 ,

wherein the tungsten oxide composite contains the metal element or the compound in a range of 0.01 mass% to 2 mass% as the amount of the metal element.

5. The photocatalytic material according to claim 1 ,

wherein the substrate comprises at least one selected from the group consisting of a glass, a ceramic, a plastic, a resin, a paper, a fiber, a metal, and a wood.

6. The photocatalytic material according to claim 1 ,

wherein the substrate comprises a fiber.

7. The photocatalytic material according to claim 1 ,

wherein the mean primary particle diameter (D50) of the particles is from 2.7 nm to 75nm.

8. The photocatalytic material according to claim 1 ,

wherein the photocatalytic film contains at least one binder component selected from the group consisting of an inorganic binder and an organic binder.

9. The photocatalytic material according to claim 1 ,

wherein the photocatalytic film has a thickness of from 2nm to 1000 nm.

10. The photocatalytic material according to claim 1 ,

wherein the photocatalytic film has a thickness of from 2nm to 400 nm.

11. The photocatalytic material according to claim 10 ,

wherein the crystal structure includes a mixture of the monoclinic crystal and the triclinic crystal or a mixture of the monoclinic crystal, the triclinic crystal, and the rhombic crystal.

12. The photocatalytic material according to claim 1 ,

wherein the photocatalytic film is formed by applying an aqueous dispersion liquid including the particles and an aqueous dispersion medium on a substrate, and

wherein a concentration of the particles in the aqueous dispersion liquid is in a range of 0.1 mass% to 40 mass%, and pH of the aqueous dispersion liquid is in a range of 1.5 to 6.5.

13. The photocatalytic material according to claim 1 ,

wherein the photocatalytic film is formed by applying a coating material comprising an aqueous dispersion liquid including the particles and an aqueous dispersion medium, and at least one binder component selected from an inorganic binder and an organic binder on the substrate, and

wherein a concentration of the particles in the aqueous dispersion liquid is in a range of 0.1 mass% to 40 mass%, and pH of the aqueous dispersion liquid is in a range of 1.5 to 6.5.

Assignments (3)
NUNC PRO TUNC ASSIGNMENT Recorded Feb 19, 2026
From: KABUSHIKI KAISHA TOSHIBA
To: TOSHIBA MATERIALS CO. LTD.
Reel/Frame 074940/0511 →
CHANGE OF NAME Recorded Feb 19, 2026
From: TOSHIBA MATERIALS CO. LTD.
To: NITERRA MATERIALS CO., LTD.
Reel/Frame 074941/0803 →
CHANGE OF ADDRESS Recorded Feb 19, 2026
From: KABUSHIKI KAISHA TOSHIBA
To: KABUSHIKI KAISHA TOSHIBA
Reel/Frame 074941/0846 →
Priority Claims (2)
JP 2008-054139 · Mar 4, 2008 · national
JP 2008-106891 · Apr 16, 2008 · national
Continuity (4)
Division 13592741 · Aug 23, 2012
Division 12874664 · Sep 2, 2010
Continuation PCTJP2009000984 · Mar 4, 2009
Related Publication 20140187412A1 · Jul 3, 2014