IP Library Granted Patent US 9,034,287
Granted Patent B2
US 9,034,287 · App. 14/205,049 · Granted May 19, 2015

Catalyst compositions, articles, methods and systems

Inventors: Olga Gerlach (Ludwigshafen, DE); Andreas Sundermann (Bensheim, DE); Jeffrey B. Hoke (North Brunswick, NJ)
Assignee: BASF CORPORATION
B01J29/7415B01D53/945B01J23/42B01J23/44B01J29/7007B01J35/023B01J35/04B01J35/08B01J37/0215B01D2255/102B01D2255/2047B01D2255/2063B01D2255/2065B01D2255/20707B01D2255/2092B01D2255/30B01D2255/502B01D2255/504B01D2255/9202Y02T10/22
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Quick Facts
Patent No.
US 9,034,287
App. No.
14/205,049
Granted
May 19, 2015
Kind
B2
Abstract

Described are catalyst compositions, catalytic articles, exhaust gas treatment systems and methods that utilize the catalytic articles. The catalyst composition comprises a washcoat including a zeolite, refractory metal oxide support particles, and a platinum group metal supported on the refractory metal oxide support particles. Greater than 90% of the refractory metal oxide particles supporting PGM have a particle size greater than 1 μm and a d 50 less than 40 microns.

Claims (17)

1. A catalyst composition comprising a washcoat including a zeolite, refractory metal oxide support particles, and a platinum group metal supported on the refractory metal oxide support particles, wherein greater than 90% of the refractory metal oxide particles supporting PGM have a particle size greater than 1 μm and a d 50 less than 40 microns.

2. The catalyst composition of claim 1 , wherein greater than 95% of the refractory metal oxide particles supporting PGM have a particle size greater than 1 μm and a d 50 less than 40 microns.

3. The catalyst composition of claim 2 , where greater than 98% of the refractory metal oxide particles supporting PGM have a particle size greater than 1 μm and a d 50 less than 40 microns.

4. The catalyst composition of claim 1 , wherein the refractory metal oxide support particles are selected from alumina, silica-alumina, titania, titania-alumina, silicatitania, ceria, ceria-alumina, ceria-silica-alumina, manganese-alumina, and lanthanaalumina.

5. The catalyst composition of claim 4 , wherein the refractory metal oxide support particles are selected from alumina and silica-alumina.

6. The catalyst composition of claim 1 , wherein the CO light-off temperature of the catalyst composition after aging at 800° C. is at least 3° C. less than the light-off temperature of a catalyst composition comprising refractory metal oxide support particles and a platinum group metal supported on the refractory metal oxide support particles, wherein less than 90% of the refractory metal oxide support particles of the comparative catalyst composition have a particle size greater than 1 μm.

7. The catalyst composition of claim 6 , wherein the CO light-off temperature of the catalyst composition after aging at 800° C. is at least 5° C. less than the light-off temperature of a comparative catalyst composition comprising refractory metal oxide support particle and a platinum group metal supported on the refractory metal oxide support particles, wherein less than 90% of the refractory metal oxide support particles of the comparative catalyst composition have a particle size greater than 1 μm.

8. The catalyst composition of claim 7 , wherein the CO light-off temperature of the catalyst composition after aging at 800° C. is at least 7° C. less than the light-off temperature of a comparative catalyst composition comprising refractory metal oxide support particles and a platinum group metal supported on the refractory metal oxide support particles, wherein less than 90% of the refractory metal oxide support particles of the comparative catalyst composition have a particle size greater than 1 μm.

9. The catalyst composition of claim 1 , wherein the platinum group metal comprises platinum, palladium, or mixtures thereof.

10. The catalyst composition of claim 1 , wherein the zeolite is selected from the group consisting of faujasite, chabazite, clinoptilolite, mordenite, silicalite, zeolite X, zeolite Y, ultrastable zeolite Y, ZSM-5, ZSM-12, SSZ-13, SAPO-5, SAPO-37, offretite, Beta zeolite, and combinations thereof.

11. The catalyst composition of claim 10 , wherein the zeolite is Beta zeolite.

12. The catalyst composition of claim 10 , wherein the zeolite has a particle size distribution that is monomodal.

13. A catalytic article for the treatment of exhaust gas from an internal combustion engine containing hydrocarbons, carbon monoxide, and nitrogen oxides, the catalytic article comprising a carrier substrate having a length, an inlet end and outlet end, an oxidation catalyst material on the carrier, the oxidation catalyst material including an oxidation catalyst comprising a washcoat layer including the catalyst composition of claim 1 .

14. The catalytic article of claim 13 , wherein the catalytic article uses a single washcoat layer.

15. The catalytic article of claim 13 , wherein the internal combustion engine is a lean burn engine.

16. A method of treating exhaust gas from a lean burn engine containing hydrocarbons, carbon monoxide, and nitrogen oxides, the method comprising flowing the exhaust gas over the catalytic article of claim 13 .

17. A method of preparing a catalytic article including a zeolite, refractory metal oxide support particles, and a platinum group metal supported on the refractory metal oxide support particles, wherein greater than 90% of the refractory metal oxide particles supporting PGM have a particle size greater than 1 μm and a d 50 less than 40 microns, the method comprising impregnating refractory metal oxide support particles with a platinum group metal, spray drying the refractory metal oxide particles supporting PGM to increase the particle size, creating a slurry of the spray dried refractory metal oxide particles supporting PGM, adding the zeolite to the slurry to form a washcoat, and coating the washcoat on a substrate.

Assignments (2)
NUNC PRO TUNC ASSIGNMENT Recorded Aug 8, 2024
From: BASF CORPORATION
To: BASF MOBILE EMISSIONS CATALYSTS LLC
Reel/Frame 068518/0394 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 28, 2014
From: GERLACH, OLGA; SUNDERMANN, ANDREAS; HOKE, JEFFREY B.
To: BASF CORPORATION
Reel/Frame 032768/0909 →
Continuity (2)
Provisional Application 61779603 · Mar 13, 2013
Related Publication 20140271428A1 · Sep 18, 2014