Asphalt oxidation technique
View Patent ↗The present invention relates to a method for oxidizing asphalt which comprises dispersing an oxygen containing gas throughout an asphalt flux in an oxidation zone while the asphalt flux is maintained at a temperature which is within the range of about 400° F. to 550° F., wherein the oxygen containing gas is introduced into the oxidation zone through a recycle loop. The recycle loop pumps asphalt flux from the oxidation zone and reintroduces the asphalt flux into the oxidation zone as oxygen enhanced asphalt flux. The recycle loop will typically include a pump which pulls the asphalt flux from the oxidation zone and which pumps the oxygen enhanced asphalt flux into the oxidation zone, and wherein the oxygen containing gas is injected into the recycle loop at a point before the asphalt flux enters into the pump.
1. A method for oxidizing asphalt which comprises dispersing an oxygen containing gas throughout an asphalt flux in an oxidation zone while the asphalt flux is maintained at a temperature which is within the range of about 400° F. to 550° F., wherein the oxygen containing gas is introduced into the oxidation zone through a recycle loop, wherein the recycle loop pumps asphalt flux from the oxidation zone and reintroduces the asphalt flux into the oxidation zone as an oxygen enhanced asphalt flux, wherein the recycle loop further includes a pump which pulls the asphalt flux from the oxidation zone and which pumps the oxygen enhanced asphalt flux into the oxidation zone, and wherein the oxygen containing gas is injected into the recycle loop at a point before the asphalt flux enters into the pump.
2. The method of claim 1 wherein an oxygen containing gas is injected into the recycle loop to produce the oxygen enhanced asphalt flux.
3. The method of claim 1 wherein the recycle loop pumps the asphalt flux from the oxidation zone and pumps the oxygen enhanced asphalt flux into the oxidation zone, and wherein the oxygen enhanced asphalt flux is pumped into the oxidation zone at a lower point in the oxidation zone than the point at which the asphalt flux is pumped from the oxidation zone.
4. The method of claim 3 wherein the oxygen containing gas is air.
5. The method of claim 4 wherein the air is enriched with oxygen.
6. The method of claim 1 wherein said method results in the production of industrial asphalt, wherein the industrial asphalt has a softening point which is within the range of 185° F. to 235° F., and wherein the industrial asphalt has a penetration value which is within the range of 15 dmm to 35 dmm.
7. The method of claim 1 wherein said method results in the production of industrial asphalt, wherein the industrial asphalt has a softening point which is within the range of 190° F. to 220° F., and wherein the industrial asphalt has a penetration value which is within the range of 15 dmm to 25 dmm.
8. The method of claim 1 wherein the asphalt flux is maintained at a temperature which is within the range of about 425° F. to about 525° F., and wherein the asphalt flux is maintained in the oxidation zone for a period of about 2 hours to about 8 hours.
9. The method of claim 8 wherein the asphalt flux is maintained in the oxidation zone for a period of about 3 hours to about 6 hours.
10. The method of claim 1 wherein the asphalt flux is maintained at a temperature which is within the range of about 450° F. to about 500° F., and wherein the asphalt flux is maintained in the oxidation zone for a period of about 3 hours to about 6 hours.
11. The method of claim 1 wherein the oxidation zone is a blow still.
12. The method of claim 1 wherein the oxidation is conducted in the presence of an air blowing catalyst.
13. The method of claim 1 wherein the oxygen enhanced asphalt flux is pumped into the oxidation zone at a higher point in the oxidation zone than the point at which the asphalt flux is pumped from the oxidation zone.
14. The method of claim 1 wherein said method is carried out as a batch process.