IP Library Granted Patent US 8,772,002
Granted Patent B1
US 8,772,002 · App. 14/212,251 · Granted Jul 8, 2014

Method for treatment of microorganisms during propagation, conditioning and fermentation using hops acid extracts and organic acid

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Quick Facts
Patent No.
US 8,772,002
App. No.
14/212,251
Granted
Jul 8, 2014
Kind
B1
Abstract

A method of reducing undesirable microorganism concentration, the method comprises (a) introducing a quantity of fermentable carbohydrate, sugar or cellulose to an aqueous system, (b) introducing a quantity of desirable microorganism to the aqueous system, (c) introducing a hops acid extract into the aqueous system and (d) introducing an organic acid solution into said system.

Claims (33)

1. A method of controlling undesirable microorganism concentration in an aqueous solution employed in a fermentation process, the method comprising the steps of:

(a) introducing a fermentable carbohydrate to the aqueous solution;

(b) introducing at least one yeast to the solution;

(c) introducing a hops acid extract into the solution; and

(d) introducing at least one organic acid into the solution;

wherein the organic acid is selected from the group consisting of citric acid, benzoic acid, propionic acid and their salts.

2. The method of claim 1 wherein the steps are performed sequentially.

3. The method of claim 1 wherein the organic acid comprises citric acid.

4. The method of claim 1 wherein the amount of hops acid extract in the aqueous solution comprises from 1 ppm to 100 ppm.

5. The method of claim 1 wherein the amount of hops acid extract in the aqueous solution comprises from 2 ppm to 70 ppm.

6. The method of claim 1 wherein the hops acid extract has a dosage of at least 0.5 ppm.

7. The method of claim 1 wherein the organic acid has a dosage of at least 100 ppm.

8. The method of claim 1 wherein the organic acid is citric acid or its salt and the ratio of hops acid extract to citric acid (or its salt) is from 1:10 to 1:6500.

9. A method of controlling undesirable microorganism concentration in an aqueous fluid solution employed in a fermentation process, the method comprising the steps of:

(a) introducing a fermentable carbohydrate to the aqueous system;

(b) introducing at least one desirable microorganism which is capable of fermenting carbohydrate to the aqueous system;

(c) introducing at least one hops acid extract into the aqueous system; and

(d) introducing at least one organic acid into the aqueous system;

wherein the organic acid is selected from the group consisting of citric acid, benzoic acid, propionic acid and their salts.

10. The method of claim 9 wherein the steps are performed sequentially.

11. The method of claim 9 wherein the organic acid comprises citric acid.

12. The method of claim 9 wherein the hops acid extract has a dosage in the aqueous system of at least 1 ppm to 100 ppm.

13. The method of claim 9 wherein the hops acid extract has a dosage in the aqueous system of at least 2 ppm to 70 ppm.

14. The method of claim 9 wherein the organic acid is citric acid or its salt and the ratio of hops acid extract to citric acid (or its salt) is from 1:10 to 1:6500.

15. The method of claim 9 wherein the organic acid is citric acid or its salt and wherein the hops acid extract has a dosage in the aqueous system of at least 2 ppm to 70 ppm and wherein the organic acid has a dosage of at least 100 ppm.

16. The method of claim 9 , wherein the organic acid has a dosage of at least 100 ppm.

17. The method of claim 9 wherein the desirable microorganism is selected from the group consisting of a yeast, a fungi, a bacteria or combination thereof.

18. A method of reducing residual byproduct of antibiotic in a fermentation process, the method comprising the steps of:

(a) introducing a fermentable carbohydrate to an aqueous system;

(b) introducing at least one yeast to said system;

(c) introducing at least one hops acid extract into said system; and

(d) introducing at least one organic acid into said system;

wherein the organic acid is selected from the group consisting of citric acid, benzoic acid, propionic acid and their salts.

Assignments (16)
SECURITY INTEREST Recorded Nov 14, 2025
From: CHEM-AQUA, INC.; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; NCH CORPORATION; NCH LIFE SCIENCES LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073570/0838 →
RELEASE OF SECURITY INTEREST Recorded Nov 14, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073564/0864 →
RELEASE OF 2023 NOTES PATENT SECURITY INTERESTS Recorded Oct 10, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073074/0198 →
SECURITY AGREEMENT (NOTES) Recorded Oct 10, 2025
From: DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073061/0885 →
SECURITY AGREEMENT (2024 NOTES) Recorded Jun 24, 2024
From: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 067824/0278 →
2023 NOTES PATENT SECURITY AGREEMENT Recorded Jul 7, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE GLOBAL CORPORATION
To: BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 064225/0170 →
SECURITY AGREEMENT (NOTES) Recorded Sep 14, 2022
From: SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A. AS COLLATERAL AGENT
Reel/Frame 061432/0821 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: GOLDMAN SACHS BANK USA
Reel/Frame 058102/0407 →
ABL PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: BANK OF AMERICA, N.A.
Reel/Frame 058102/0122 →
NOTES SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 058103/0066 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CITIBANK, N.A.
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058848/0636 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058856/0724 →
INTELLECTUAL PROPERTY SECOND LIEN SECURITY AGREEMENT RELEASE Recorded Jul 20, 2018
From: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 047058/0800 →
INTELLECTUAL PROPERTY FIRST LIEN SECURITY AGREEMENT RELEASE Recorded Jul 20, 2018
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 046594/0252 →
FIRST LIEN NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jul 20, 2018
From: SOLENIS TECHNOLOGIES, L.P.
To: CITIBANK, N.A., COLLATERAL AGENT
Reel/Frame 046595/0241 →
SECOND LIEN NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jul 20, 2018
From: SOLENIS TECHNOLOGIES, L.P.
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
Reel/Frame 046629/0213 →