IP Library Granted Patent US 9,062,227
Granted Patent B2
US 9,062,227 · App. 14/215,116 · Granted Jun 23, 2015

Paper sizing composition with salt of calcium (II) and organic acid, products made thereby, method of using, and method of making

Inventor: Michael F. Koenig (Paducah, KY)
Assignee: INTERNATIONAL PAPER COMPANY
C09D103/00Y10T428/24934D21H17/28D21H17/68D21H21/16D21H21/30D21H23/04D21H23/56B41M5/52B41M5/5218B41M5/5245B41M7/00C09J103/00
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Quick Facts
Patent No.
US 9,062,227
App. No.
14/215,116
Granted
Jun 23, 2015
Kind
B2
Abstract

A paper sizing composition is provided, which comprises a water-soluble salt of Ca(II) and at least one organic acid; and starch. Methods of making and using the composition, and methods of making and using the recording sheets which include the composition, are disclosed.

Claims (20)

1. A paper sizing composition, comprising: starch in an amount of from about 0.1 to about 75% by weight of the sizing composition; an optical brightening agent in an amount of from 0.1 to 100 lbs per 100 lbs of the sizing composition; and a water-soluble salt of Ca(II) and at least one organic acid in an amount of from about 0.1 to about 50% by weight of the sizing composition.

2. The composition of claim 1 , wherein the salt has a water solubility of greater than 0.002 grams salt/100 cc of water at 25° C.

3. The composition of claim 1 , wherein the organic acid has the formula RCOOH, wherein R is a hydrocarbon having 1-30 carbon atoms.

4. The composition of claim 1 , wherein the organic acid is zwitterionic or amphoteric.

5. The composition of claim 1 , wherein the salt is a salt having two identical organic acids.

6. The composition of claim 1 , wherein the salt is a complex salt having two or more different organic acids.

7. The composition of claim 1 , wherein the salt is calcium acetate, calcium formate, calcium proprionate, calcium lactate, calcium stearate, calcium tartrate, calcium gluconate, calcium citrate, calcium lactate gluconate, calcium 2-ethylbutanoate, calcium EDTA, calcium DTPA, calcium magnesium acetate, or a mixture thereof.

8. The composition of claim 1 , wherein the salt is calcium acetate, calcium formate, calcium proprionate, calcium lactate, calcium stearate, calcium tartrate, calcium gluconate, calcium citrate, calcium lactate gluconate, calcium 2-ethylbutanoate, calcium magnesium acetate, or a mixture thereof.

9. A method for making the composition of claim 1 , comprising contacting starch; optical brightening agent; and a water-soluble salt of Ca(II) and at least one organic acid to produce the composition of claim 1 .

10. A recording sheet, comprising: a paper substrate, comprising: a plurality of cellulosic fibers; and a paper sizing composition, comprising: starch in an amount of from about 0.1 to about 75% by weight of the sizing composition; an optical brightening agent in an amount of from 0.1 to 100 lbs per 100 lbs of the sizing composition; and a water-soluble salt of Ca(II) and at least one organic acid in an amount of from about 0.1 to about 50% by weight of the sizing composition.

11. The recording sheet of claim 10 , wherein the water soluble Ca(II) salt of the organic acid is present in an amount ranging from about 2 to about 100 lbs Ca(II) salt/ton of paper.

12. The recording sheet of claim 10 , wherein the water soluble Ca(II) salt is present in an amount ranging from about 0.02 g/m 2 to about 4 g/m 2 .

13. The recording sheet of claim 10 , wherein the starch is present in an amount ranging from about 5 to about 300 lbs/ton.

14. The recording sheet of claim 10 , wherein the dry pickup of the sizing composition ranges from 0.25 to 8 gsm.

15. The recording sheet of claim 10 , wherein the sizing composition is an internal sizing.

16. The recording sheet of claim 10 , wherein the sizing composition is an external sizing.

17. The recording sheet of claim 10 , wherein the sizing composition is an internal and an external sizing.

18. The recording sheet of claim 10 , comprising a printed image thereon.

19. A method for making a recording sheet, comprising: contacting: a paper substrate comprising a plurality of cellulosic fibers; and a composition, comprising: starch in an amount of from about 0.1 to about 75% by weight of the sizing composition; an optical brightening agent in an amount of from 0.1 to 100 lbs per 100 lbs of the sizing composition; and a water-soluble salt of Ca(II) and at least one organic acid in an amount of from about 0.1 to about 50% by weight of the sizing composition to produce a recording sheet.

20. A method, comprising forming an image with a printing apparatus on a surface of a recording sheet, said recording sheet comprising: a paper substrate comprising: a plurality of cellulosic fibers; and a composition, comprising: starch in an amount of from about 0.1 to about 75% by weight of the sizing composition; an optical brightening agent in an amount of from 0.1 to 100 lbs per 100 lbs of the sizing composition; and a water-soluble salt of Ca(II) and at least one organic acid in an amount of from about 0.1 to about 50% by weight of the sizing composition.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 2, 2024
From: GLOBAL HOLDINGS II, INC.
To: COBANK, ACB, AS ADMINISTRATIVE AGENT
Reel/Frame 068161/0057 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 11, 2022
From: INTERNATIONAL PAPER COMPANY
To: GLOBAL HOLDINGS II, INC.
Reel/Frame 059862/0110 →
SECURITY AGREEMENT Recorded Sep 29, 2021
From: GLOBAL HOLDINGS II, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 057686/0548 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 24, 2014
From: KOENIG, MICHAEL F
To: INTERNATIONAL PAPER COMPANY
Reel/Frame 032743/0880 →
Continuity (3)
Continuation 13295168 · Nov 14, 2011
Provisional Application 61414017 · Nov 16, 2010
Related Publication 20140220323A1 · Aug 7, 2014