IP Library Granted Patent US 8,883,206
Granted Patent B2
US 8,883,206 · App. 14/286,856 · Granted Nov 11, 2014

Pharmaceutical composition and administrations thereof

Inventors: Eleni Dokou (Cambridge, MA); Shahla Jamzad (Belmont, MA); John P. Caesar, Jr. (Lancaster, MA); Majed Fawaz (Foxboro, MA); Laura Das (Charlestown, MA); Chong-Hui Gu (Weban, MA); Patricia Nell Hurter (Harvard, MA); Meghna Jai Israni (Boston, MA); Meghan M. Johnston (Wakefield, MA); Dragutin Knezic (Watertown, MA); Andrew G. Kuzmission (Shrewsburg, MA); HongRen Wang (Lexington, MA)
Assignee: Vertex Pharmaceuticals Incorporated
C07D215/56A61K9/1623A61K9/2009A61K9/1652A61K9/1617A61K9/2054A61K9/1611A61K9/2013A61K9/2018
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Quick Facts
Patent No.
US 8,883,206
App. No.
14/286,856
Granted
Nov 11, 2014
Kind
B2
Abstract

The present invention relates to pharmaceutical compositions containing a solid dispersion of N-[2,4-Bis(1,1-dimethylethyl)-5-hydroxyphenyl]-1,4-dihydro-4-oxoquinoline-3-carboxamide including formulations of the solid dispersions into powders, granules and mini-tablets, methods for manufacturing and processing the powders, granules and mini-tablets, and methods for treating cystic fibrosis employing the pharmaceutical composition.

Claims (17)

1. A pharmaceutical composition consisting of:

about 35 wt % of a solid dispersion by weight of the composition, wherein the dispersion comprises about 80 wt % of substantially amorphous or amorphous N-[2,4-Bis(1,1-dimethylethyl)-5-hydroxyphenyl]-1,4-dihydro-4-oxoquinoline-3-carboxamide by weight of the dispersion, about 19.5 wt % of HPMCAS by weight of the dispersion, and about 0.5 wt % SLS by weight of the dispersion;

about 13.5 wt % of mannitol by weight of the composition;

about 41 wt % of lactose by weight of the composition;

about 2 wt % of sucralose by weight of the composition;

about 6 wt % of croscarmellose sodium by weight of the composition;

about 1 wt % of colloidal silicon dioxide by weight of the composition; and

about 1.5 wt % of magnesium stearate by weight of the composition.

2. The pharmaceutical composition of claim 1 , wherein the pharmaceutical composition is a unit dose form comprising one or a plurality of granules, pellets, particles or mini-tablets, and wherein the unit dose form comprises from about 1 mg to about 100 mg of substantially amorphous or amorphous N-[2,4-Bis(1,1-dimethylethyl)-5-hydroxyphenyl]-1,4-dihydro-4-oxoquinoline-3-carboxamide.

3. The pharmaceutical composition of claim 2 , wherein the unit dose form comprises about 50 mg of substantially amorphous or amorphous N-[2,4-Bis(1,1-dimethylethyl)-5-hydroxyphenyl]-1,4-dihydro-4-oxoquinoline-3-carboxamide.

4. The pharmaceutical composition of claim 2 , wherein the unit dose form comprises about 75 mg of substantially amorphous or amorphous N-[2,4-Bis(1,1-dimethylethyl)-5-hydroxyphenyl]-1,4-dihydro-4-oxoquinoline-3-carboxamide.

5. The pharmaceutical composition of claim 2 , wherein the unit dose form comprises from about 25 to about 40 mini-tablets.

6. The pharmaceutical composition of claim 2 , wherein the solid dispersion is present in an amount of about 35 percent by weight of the pharmaceutical composition and the unit dose form comprises from about 26 mini-tablets.

7. The pharmaceutical composition of claim 6 , wherein the unit dose form comprises about 50 mg of substantially amorphous or amorphous N-[2,4-Bis(1,1-dimethylethyl)-5-hydroxyphenyl]-1,4-dihydro-4-oxoquinoline-3-carboxamide.

8. The pharmaceutical composition of claim 2 , wherein the solid dispersion is present in an amount of about 35 percent by weight of the pharmaceutical composition and the unit dose form comprises about 39 mini-tablets.

9. The pharmaceutical composition of claim 8 , wherein the unit dose form comprises about 75 mg of substantially amorphous or amorphous N-[2,4-Bis(1,1-dimethylethyl)-5-hydroxyphenyl]-1,4-dihydro-4-oxoquinoline-3-carboxamide.

10. The pharmaceutical composition of claim 5 , wherein the mini-tablet has a shape that is cylinder-like, oval-like, cone-like, sphere-like, ellipsis-like, polygon-like or combinations thereof, wherein the mini-tablet has as its longest dimension or diameter a length of about 2 mm.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded Oct 14, 2016
From: MACQUARIE US TRADING LLC
To: VERTEX PHARMACEUTICALS INCORPORATED; VERTEX PHARMACEUTICALS (SAN DIEGO) LLC
Reel/Frame 040357/0001 →
SECURITY INTEREST Recorded Jul 10, 2014
From: VERTEX PHARMACEUTICALS INCORPORATED; VERTEX PHARMACEUTICALS (SAN DIEGO) LLC
To: MACQUARIE US TRADING LLC
Reel/Frame 033292/0311 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 18, 2014
From: DOKOU, ELENI; JAMZAD, SHAHLA; CAESAR, JOHN P.; DAS, LAURA; FAWAZ, MAJED; GU, CHONG-HUI; HURTER, PATRICIA NELL; ISRANI, MEGHNA JAI; JOHNSTON, MEGHAN M.; KNEZIC, DRAGUTIN; KUZMISSION, ANDREW G.; WANG, HONGREN
To: VERTEX PHARMACEUTICALS INCORPORATED
Reel/Frame 033131/0962 →
Continuity (4)
Continuation 13779654 · Feb 27, 2013
Provisional Application 61603882 · Feb 27, 2012
Provisional Application 61710352 · Oct 5, 2012
Related Publication 20140255483A1 · Sep 11, 2014