IP Library Granted Patent US 9,050,316
Granted Patent B2
US 9,050,316 · App. 14/306,756 · Granted Jun 9, 2015

Pharmaceutical-grade ferric organic compounds, uses thereof and methods of making same

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Quick Facts
Patent No.
US 9,050,316
App. No.
14/306,756
Granted
Jun 9, 2015
Kind
B2
Abstract

The present invention discloses a pharmaceutical-grade ferric organic compounds, including ferric citrate, which are soluble over a wider range of pH, and which have a large active surface area. A manufacturing and quality control process for making a pharmaceutical-grade ferric citrate that consistently complies with the established Manufacture Release Specification is also disclosed. The pharmaceutical-grade ferric organic compounds are suitable for treating disorders characterized by elevated serum phosphate levels.

Claims (23)

1. A method of treating hyperphosphatemia, comprising:

administering one or more tablets comprising ferric citrate and a pharmaceutically acceptable carrier to a subject, the tablets prepared from a form of ferric citrate having an intrinsic dissolution rate of at least 1.88 mg/cm 2 /min; wherein the tablets are administered to provide up to 30 grams of ferric citrate to the subject per day.

2. The method of claim 1 , wherein the subject has chronic kidney disease.

3. The method of claim 2 , wherein the chronic kidney disease is selected from early-stage chronic kidney disease and mid-stage chronic kidney disease.

4. The method of claim 2 , wherein the chronic kidney disease is late-stage chronic kidney disease.

5. The method of claim 2 , wherein the subject is undergoing dialysis.

6. The method of claim 5 , wherein the dialysis is selected from hemodialysis and peritoneal dialysis.

7. The method of claim 1 , wherein the tablets are administered to provide 4 grams to 15 grams of ferric citrate to the subject per day.

8. The method of claim 1 , wherein the tablets are administered to provide 2 grams to 12 grams of ferric citrate to the subject per day.

9. The method of claim 1 , wherein the tablets are administered to provide 2 grams, 4 grams or 6 grams of ferric citrate to the subject per day.

10. The method of claim 1 , wherein the tablets are administered to provide 1 gram of ferric citrate to the subject per day.

11. The method of claim 1 , wherein the tablets each comprise 500 mg of ferric citrate.

12. A method of treating metabolic acidosis, comprising: administering one or more tablets comprising ferric citrate and a pharmaceutically acceptable carrier to a subject, the tablets prepared from a form of ferric citrate having an intrinsic dissolution rate of at least 1.88 mg/cm 2 /min; wherein the tablets are administered to provide up to 30 grams of ferric citrate to the subject per day.

13. The method of claim 12 , wherein the subject has chronic kidney disease.

14. The method of claim 13 , wherein the chronic kidney disease is selected from early-stage chronic kidney disease and mid-stage chronic kidney disease.

15. The method of claim 13 , wherein the chronic kidney disease is late-stage chronic kidney disease.

16. The method of claim 15 , wherein the subject is undergoing dialysis.

17. The method of claim 16 , wherein the dialysis is selected from hemodialysis and peritoneal dialysis.

18. The method of claim 12 , wherein the tablets are administered to provide 4 grams to 15 grams of ferric citrate to the subject per day.

19. The method of claim 12 , wherein the tablets are administered to provide 2 grams to 12 grams of ferric citrate to the subject per day.

20. The method of claim 12 , wherein the tablets are administered to provide 2 grams, 4 grams or 6 grams of ferric citrate to the subject per day.

21. The method of claim 12 , wherein the tablets are administered to provide 1 gram of ferric citrate to the subject per day.

22. The method of claim 12 , wherein the tablets each comprise 500 mg of ferric citrate.

Assignments (18)
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jun 25, 2024
From: BIOPHARMA CREDIT PLC
To: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
Reel/Frame 067839/0134 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jan 29, 2024
From: BIOPHARMA CREDIT PLC
To: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
Reel/Frame 066377/0741 →
FIFTEENTH AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Jan 4, 2024
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 066205/0143 →
THIRTEENTH AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 29, 2023
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 063189/0065 →
TWELFTH AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Nov 29, 2022
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 062012/0561 →
ELEVENTH AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Aug 22, 2022
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 061297/0238 →
TENTH AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Jun 16, 2022
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 060529/0168 →
SECURITY INTEREST Recorded Dec 15, 2021
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 058399/0055 →
SEVENTH AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Sep 12, 2021
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 057474/0770 →
SIXTH AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Jun 11, 2021
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 056544/0468 →
FIFTH AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 30, 2021
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 055776/0491 →
FOURTH AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Dec 17, 2020
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 054793/0455 →
THIRD AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Sep 10, 2020
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 054173/0451 →
SECOND AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Sep 2, 2020
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 053671/0221 →
SECURITY INTEREST Recorded Apr 2, 2020
From: AKEBIA THERAPEUTICS, INC.; KERYX BIOPHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 052295/0662 →
NUNC PRO TUNC ASSIGNMENT Recorded Apr 1, 2015
From: KWOK, DAVID W.K.; STOYNOV, NIKOLAY MINTCHEV
To: PANION & BF BIOTECH INC.
Reel/Frame 035313/0813 →
NUNC PRO TUNC ASSIGNMENT Recorded Jul 22, 2014
From: GLOBOASIA, LLC
To: PANION & BF BIOTECH INC.
Reel/Frame 033366/0456 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 22, 2014
From: CHAN, KEITH; TOWN, WINSTON
To: GLOBOASIA, LLC
Reel/Frame 033366/0251 →