IP Library Granted Patent US 9,181,415
Granted Patent B2
US 9,181,415 · App. 14/325,584 · Granted Nov 10, 2015

Acetylated derivatives of castor oil and their blends with epoxidized fatty acid esters

Inventors: Bharat I. Chaudhary (Princeton, NJ); Beate Sczekalla (Halle, DE); Michael Meerbote (Gutenberg, DE); Yang Cheng (Midland, MI)
Assignee: Dow Global Technologies LLC
C08K5/1515C08K5/0016C08K5/10C08K5/11H01B3/443Y10T428/1355Y10T428/2933Y10T428/31699
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Quick Facts
Patent No.
US 9,181,415
App. No.
14/325,584
Granted
Nov 10, 2015
Kind
B2
Abstract

The present disclosure is directed to acetylated castor components and compositions including the same. The acetylated castor component may be an acetylated castor oil and/or an acetylated castor wax. The acetylated castor component may be blended with an epoxidized fatty acid ester. The present acetylated castor components and blends find advantageous application as a plasticizer.

Claims (13)

1. A polymeric composition comprising:

(A) a polyvinyl chloride resin; and

(B) a plasticizer composition comprising

50 wt % of an acetylated castor wax having a hydroxyl number of 0, the acetylated castor wax is present in the plasticizer composition and the amount of acetylated castor wax is based on the weight of the plasticizer composition;

50 wt % of an epoxidized soybean oil, based on the weight of the plasticizer composition;

wherein the plasticizer composition has a solution temperature of 140° C. to 200° C. and the polymeric composition is phthalate-free and has a tensile elongation retention greater than 30% after 168 hours heat aging at 136° C. as measured on dog bones cut from 30 mil thick plaques in accordance with ASTM D638.

2. The polymeric composition of claim 1 , wherein the acetylated castor wax has a viscosity from 100 mPa·s to less than 2000 mPa·s as measured in accordance with ASTM D334 at 25° C.

3. The polymeric composition of claim 1 , wherein the acetylated castor wax has an iodine number of 0 to less than 40 g I 2 /100 g.

4. The polymeric composition of claim 1 , wherein the acetylated castor wax comprises 40-95 wt % acetylated glyceryl trihydroxystearate.

5. The polymeric composition of claim 1 , wherein the acetylated castor wax has an acid number from about 0 mg KOH/g to about 8 mg KOH/g.

6. The polymeric composition of claim 1 , wherein the composition is a plaque having a tensile strength retention greater than about 70% after 168 hours heat aging at 113° C.

7. The polymeric composition of claim 1 , wherein the acetylated castor wax has a viscosity from 100 mPa·s to less than 2000 mPa·s as measured in accordance with ASTM D334 at 25° C. and an iodine number of 0 to less than 40 g I 2 /100 g.

8. The polymeric composition of claim 7 comprising 63.9 wt % of the polyvinyl chloride and 27.3 wt % of the plasticizer composition, and further comprising 8.8 wt % of an additive, based on the weight of the polymeric composition.

Assignments (2)
CORRECTIVE ASSIGNMENT TO CORRECT THE CONVEYING PARTY DATA NAME PREVIOUSLY RECORDED AT REEL: 037300 FRAME: 0728. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF NAME. Recorded Apr 21, 2017
From: AMS RESEARCH CORPORATION
To: AMS RESEARCH, LLC
Reel/Frame 042308/0630 →
CHANGE OF NAME Recorded Dec 15, 2015
From: AMS RESEARCH CORPATION
To: AMS RESEARCH, LLC
Reel/Frame 037300/0728 →
Continuity (3)
Continuation 13498745
Provisional Application 61247383 · Sep 30, 2009
Related Publication 20140323622A1 · Oct 30, 2014