IP Library Granted Patent US 10,390,552
Granted Patent B2
US 10,390,552 · App. 14/331,178 · Granted Aug 27, 2019

Highly refined cellulose-based gel

Inventors: Brock M. Lundberg (Osseo, WI); Alexander Scott Jasper (Eau Claire, WI)
A23L29/262A23L29/20
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Quick Facts
Patent No.
US 10,390,552
App. No.
14/331,178
Granted
Aug 27, 2019
Kind
B2
Abstract

A method forms a gel from a highly-refined cellulose by: providing a composition of highly refined cellulose fiber as at least about 0.5% weight/weight highly refined cellulose to water; adding at least one buffering agent to the composition to maintain the pH of the composition at a pH below 9.5; bringing the buffered composition to an elevated temperature such as a boil; stirring the buffered composition; and cooling the buffered composition to below 25° C. to form a gel, such as a stable gel.

Claims (30)

1. A method of forming a gel comprising from a highly refined cellulose comprising:

providing a composition of highly refined cellulose fiber as at least 0.5% weight/weight highly refined cellulose to water;

adding at least one buffering agent to the composition to maintain the pH of the composition at a pH below 9.5;

bringing the buffered composition to a boil;

stirring the buffered composition before cooling the buffered composition to form a gel; and

cooling the buffered composition to below 25° C. to form a gel.

2. The method of claim 1 wherein the at least one buffering agent maintains the pH of the composition between 4.0 and 8.0.

3. The method of claim 2 wherein the buffering agent comprises less than 1% by molecular percent of ammonium and less than 1% molecular percent of hydroxide and wherein the highly refined cellulose fiber is present as at least 0.5% weight/weight highly refined cellulose to water with no more than 1% pectin weight/weight highly refined cellulose.

4. The method of claim 1 wherein the gel is combined with a liquid to thicken the liquid and wherein the highly refined cellulose fiber is present as at least 0.5% weight/weight highly refined cellulose to water with no more than 1% pectin weight/weight highly refined cellulose.

5. A solid mass formed by the method of claim 1 .

6. The method of claim 1 wherein the at least one buffering agent maintains the pH of the composition between 4.0 and 9.0.

7. The method of claim 6 wherein the buffering agent comprises less than 1% by molecular percent of ammonium and less than 1% molecular percent of hydroxide.

8. The method of claim 7 wherein the gel is combined with a liquid to thicken the liquid.

9. The liquid mass formed by the method of claim 8 .

10. The method of claim 6 wherein the gel is combined with a liquid to thicken the liquid.

11. The liquid mass formed by the method of claim 10 .

12. The method of claim 1 wherein ester groups present in pectin from the highly refined cellulose are esterified during boiling, stirring and cooling to a degree of esterification of less than 50%.

13. The method of claim 12 wherein the gel is combined with a liquid to thicken the liquid.

14. A solid mass formed by the method of claim 12 .

15. The method of claim 12 wherein the gel is added to an edible liquid composition to form a combination and the combination is chilled to increase viscosity of the combination and wherein highly refined cellulose.

16. The increased viscosity combination formed by the method of claim 15 .

17. The method of claim 1 wherein the gel is added to an edible liquid composition to form a combination and the combination is chilled to increase viscosity of the combination.

18. The increased viscosity combination formed by the method of claim 17 .

19. A method of forming a gel comprising from a highly refined cellulose comprising:

providing a composition of highly refined cellulose fiber as at least 0.5% weight/weight highly refined cellulose to water with no more than 1% pectin weight/eight highly refined cellulose;

adding at least one buffering agent to the composition to maintain the pH of the composition at a pH below 9.5;

bringing the buffered composition to a boil;

stirring the buffered composition; and

cooling the buffered composition to below 25° C. to form a gel.

20. The method of claim 19 wherein stirring the buffered composition is performed before cooling the buffered composition to below 25° C. to form a gel.

Assignments (2)
MERGER AND CHANGE OF NAME Recorded Mar 10, 2017
From: FIBERSTAR BIO-INGREDIENT TECHNOLOGIES, INC.; FIBERSTAR, INC
To: FIBERSTAR, INC
Reel/Frame 041540/0070 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 14, 2014
From: LUNDBERG, BROCK M.; JASPER, ALEXANDER SCOTT
To: FIBERSTAR BIO-INGREDIENT TECHNOLOGIES, INC.
Reel/Frame 033319/0280 →
Continuity (2)
Provisional Application 61846007 · Jul 13, 2013
Related Publication 20150024108A1 · Jan 22, 2015