Methods of fabricating a polycrystalline diamond compact
View Patent ↗Embodiments relate to PDCs, methods of fabricating PDCs, and applications for such PDCs. In an embodiment, a PDC includes a substrate and a pre-sintered PCD table including an interfacial surface that is bonded to the substrate. The pre-sintered PCD table may be substantially free of leaching by-products in a region at least proximate to the interfacial surface. In an embodiment, a method of fabricating a PDC includes providing an at least partially leached PCD including an interfacial surface. The method includes removing at least some leaching by-products from the at least partially leached PCD table. After removing the at least some leaching by-products, the method includes bonding the interfacial surface of the at least partially leached PCD table to a substrate to form a PDC.
1. A method, comprising:
providing an at least partially leached polycrystalline diamond table;
subjecting the at least partially leached polycrystalline diamond table to a non-ambient pressure and an elevated temperature effective to remove at least some leaching by-products from the at least partially leached polycrystalline diamond table;
after removing the at least some leaching by-products,
infiltrating the at least partially leached polycrystalline diamond table with an infiltrant;
bonding the at least partially leached polycrystalline diamond table to a substrate to form a polycrystalline diamond compact; and
leaching a portion of the infiltrant from the infiltrated polycrystalline diamond table to which the substrate is bonded.
2. The method of claim 1 wherein the non-ambient pressure is a pressure less than ambient pressure.
3. The method of claim 1 wherein the non-ambient pressure is partial vacuum.
4. The method of claim 1 wherein the non-ambient pressure is partial vacuum and the elevated temperature is at least about 600° C. and less than about 700° C.
5. The method of claim 1 wherein subjecting the at least partially leached polycrystalline diamond table to a non-ambient pressure and an elevated temperature effective to remove at least some leaching by-products from the at least partially leached polycrystalline diamond table includes heating the at least partially leached polycrystalline diamond table under partial vacuum conditions.
6. The method of claim 5 wherein heating the at least partially leached polycrystalline diamond table under partial vacuum conditions includes heating the at least partially leached polycrystalline diamond table at a temperature sufficient to sublimate the at least some leaching by-products.
7. The method of claim 1 wherein the at least some leaching by-products include at least one of an oxide or a salt.
8. The method of claim 1 , further comprising:
reducing a non-planarity of an interfacial surface of the at least partially leached polycrystalline diamond table prior to bonding the at least partially leached polycrystalline diamond table to the substrate;
wherein bonding the at least partially leached polycrystalline diamond table to a substrate to form a polycrystalline diamond compact includes bonding the interfacial surface of the at least partially leached polycrystalline diamond table to the substrate.
9. The method of claim 8 wherein reducing a non-planarity of the interfacial surface of the at least partially leached polycrystalline diamond table prior to bonding the at least partially leached polycrystalline diamond table to the substrate includes substantially planarizing the interfacial surface to a flatness of about 0.00050 inch to about 0.0010 inch.
10. The method of claim 8 wherein reducing a non-planarity of the interfacial surface of the at least partially leached polycrystalline diamond table prior to bonding the at least partially leached polycrystalline diamond table to the substrate occurs prior to removing the at least some leaching by-products from the at least partially leached polycrystalline diamond table.
11. The method of claim 8 wherein reducing a non-planarity of the interfacial surface of the at least partially leached polycrystalline diamond table prior to bonding the at least partially leached polycrystalline diamond table to the substrate occurs after removing the at least some leaching by-products from the at least partially leached polycrystalline diamond table.
12. The method of claim 1 wherein leaching a portion of the infiltrant from the infiltrated polycrystalline diamond table to which the substrate is bonded includes leaching the infiltrant to a selected leach depth of about 50 μm to about 500 μm.
13. The method of claim 12 , further comprising removing at least some leaching by-products generated during the leaching the portion of the infiltrant.
14. The method of claim 1 wherein the acts of infiltrating and bonding are performed in a high-pressure/high-temperature process.
15. The method of claim 1 wherein the infiltrant includes at least one of iron, cobalt, or nickel.
16. The method of claim 1 wherein the substrate includes the infiltrant.
17. A method, comprising:
providing an at least partially leached polycrystalline diamond table;
subjecting the at least partially leached polycrystalline diamond table to a non-ambient pressure and an elevated temperature effective to remove at least some leaching by-products from the at least partially leached polycrystalline diamond table;
after removing the at least some leaching by-products, in a high-pressure/high-temperature process,
infiltrating the at least partially leached polycrystalline diamond table with an infiltrant from a substrate to be bonded to the at least partially leached polycrystalline diamond table; and
bonding the at least partially leached polycrystalline diamond table to the substrate to form a polycrystalline diamond compact; and
leaching a portion of the infiltrant from the infiltrated polycrystalline diamond table to a selected depth.
18. The method of claim 17 wherein the non-ambient pressure is a pressure less than ambient pressure.
19. The method of claim 17 wherein the non-ambient pressure is partial vacuum.
20. The method of claim 17 wherein the non-ambient pressure is partial vacuum and the elevated temperature is at least about 600° C. and less than about 700° C.
21. The method of claim 17 , further comprising:
reducing a non-planarity of an interfacial surface of the at least partially leached polycrystalline diamond table prior to bonding the at least partially leached polycrystalline diamond table to the substrate;
wherein bonding the at least partially leached polycrystalline diamond table to the substrate to form a polycrystalline diamond compact includes bonding the interfacial surface of the at least partially leached polycrystalline diamond table to the substrate.